等温平台石墨炉原子吸收光谱法测定高纯镍中痕量杂质锑

利用石墨炉原子吸收法，在等温平台条件下直接测定高纯镍中的痕量杂质锑，对石墨炉加热程序中的干燥时间、灰化温度及原子化温度进行了优化，同时考察了介质酸度的影响。试验表明，基体镍对锑的测定有显著的影响，为此进行了标准系列基体匹配。该法的特征质量为6．6pg；相对标准偏差为6．5％；加标回收率为100％-103％。     

差分跳频系统对抗初探

以CHESS系统为例,介绍了差分跳频通信系统的基本原理,对其抗常规有意干扰的性能作了简要分析;在此基础上,初步探索了对CHESS系统进行侦察干扰的方法,并在计算机上对干扰效果进行了仿真比较。     

四能级原子系统中量子相干增强的Kerr非线性效应的研究

应用密度矩阵方程计算了四能级原子系统中三阶非线性极化率随信号光和探针光频率失谐的变化关系。结果表明，由于量子干涉对信号光强度的敏感性，使四能级原子介质的交叉Kerr非线性作用大大增强，与三能级系统相比，四能级原子介质的Kerr非线性系数可增强两个数量级。     

因特网防御DoS攻击技术评述Ⅰ--攻击分类与特征·包过滤·攻击检测与防御

概述了因特网上DoS攻击的相应分类及基本特征，评述了包过滤、攻击检测及防御技术的最新成果．前一部分介绍了入口过滤、基于路由的过滤网和有效源地址强制协议．后一方面主要讨论了适合于检测攻击包的技术，介绍了新近提出的频谱分析方法和泛滥检测系统．简要评述了已有的防御SYN泛滥攻击的技术措施，介绍了Cisco的TCP拦截技术，提出了改进策略．     

Numerical analysis of the rotating viscous flow approaching a solid sphere

A numerical simulation is performed to investigate the flow induced by a sphere moving along the axis of a rotating cylindrical container filled with the viscous fluid. Three‐dimensional incompressible Navier–Stokes equations are solved using a finite element method. The objective of this study is to examine the feature of waves generated by the Coriolis force at moderate Rossby numbers and that to what extent the Taylor–Proudman theorem is valid for the viscous rotating flow at small Rossby number and large Reynolds number. Calculations have been undertaken at the Rossby numbers (R_o) of 1 and 0.02 and the Reynolds numbers (R_e) of 200 and 500. When R_o=O(1), inertia waves are exhibited in the rotating flow past a sphere. The effects of the Reynolds number and the ratio of the radius of the sphere and that of the rotating cylinder on the flow structure are examined. When R_o ? 1, as predicted by the Taylor–Proudman theorem for inviscid flow, the so‐called ‘Taylor column’ is also generated in the viscous fluid flow after an evolutionary course of vortical flow structures. The initial evolution and final formation of the ‘Taylor column’ are exhibited. According to the present calculation, it has been verified that major theoretical statement about the rotating flow of the inviscid fluid may still approximately predict the rotating flow structure of the viscous fluid in a certain regime of the Reynolds number. Copyright © 2004 John Wiley & Sons, Ltd.     

Linearized and rational approximation method for solving non‐linear Burgers' equation

A new numerical method called linearized and rational approximation method is presented to solve non‐linear evolution equations. The utility of the method is demonstrated for the case of differentiation of functions involving steep gradients. The solution of Burgers' equation is presented to illustrate the effectiveness of the technique for the solution of non‐linear evolution equations exhibiting nearly discontinuous solutions. Copyright © 2004 John Wiley & Sons, Ltd.     

用SY87721实现城域网波分复用系统的多业务接入

为了使城域网的DWDM（密集波分复用）系统可以接入多种信号速率和格式，以满足用户的要求，首先介绍了一种波长转换板的设计方法，使用SY87721自适应提取28Mbit／s～2.7Gbit/s之间任意速率信号的时钟，其次介绍了SY87721提取时钟的工作原理、与单片机和CPLD（复杂可编程逻辑器件）的接口方式、对寄存器的配置和读出方式。最后介绍了使用参考时钟测量接入信号频率的方法，这会在系统维护时带来较大的方便。     

Interactions of Eu3+ and Am3+ with humic acid extracted from soil of Yongkwang in the Okchon Basin of the Korean Peninsula

Summary The stability constants of Eu³⁺ and Am³⁺ with the site specific humic acid (YKHA) have been determined. The humic acid has been extracted from the soil of Yongkwang area belonging geologically to the Okchon Basin of the Korean Peninsula, where the nuclear power plant is located. The total carboxylate capacity, the acidity constant (pKa), and the binding constants with Eu³⁺ and Am³⁺ have been determined for humic acid.     

A Mossbauer study of the magnetic coupling in iron phosphorous trisulfides

The polycrystalline sample of layered compound FePS_3 has been investigated by using M?ssbauer spectroscopy (12K to 300K), magnetic susceptibility measurements, x-ray diffraction and FTIR spectroscopy. The antiferromagnetic order exists below T_N=120.5±1K. The M?ssbauer spectra below T_N indicate that the magnetization axis is perpendicular to the layer of FePS_3, and the divalent iron cations are in their high spin configurations. By fitting the hyperfine field parameters near the Néel temperature, we obtain information on the nature of magnetic interactions in the material. The results show that the magnetic coupling can be treated by the two-dimensional Ising model, and it can be interpreted on the basis of a crystal-field effect.