Determination of mepiquatchloride in animal and plant matrices by ion chromatography with conductivity detection

Summary A new residue method, based on ion chromatography, for the determination of trace amounts of the ionic plant growth regulator mepiquatchloride is described. The method is adapted to plant and animal matrices and does not require any derivatization steps. This new technique provides higher recoveries of the analyte, better reproducibility and increased speed than the previous method. The limit of determination is 0.05 mg/kg.     

Millimeter wave beams diffracted from reflecting gratings

According to the angular-spectrum method, a radiation beam of an antenna horn in the Fresnal region is decomposed into the plane waves with the fast Fourier transform algorithm and the waves diffracted from a reflection grating are superposed as a diffracted beam. Compared with the reflected beam from the same size mirror, the radiation half width of the diffracted beam from a grating is narrower and its lateral shape is shift. These performances have been experimentally verified at Ka-band by: (1). The relative diffraction efficiencies in the first order with two triangular gratings which is put along propagating direction of a beam produced by a conical lens-horn. (2). H-plane lateral width with power—3dB lapsed of the focus beam from a grating and a mirror in a grating spectrometer for millimeter waves (25–100 GHz).     

苯对N,N-二甲基甲酰胺化合物~1H NMR的影响研究

本文研究了N,N-二甲基甲酰胺(DMF)在四氯化碳和苯混合溶剂中的~1H NMR。观察到N,N-二甲基甲酰胺(DMF)分子中两个甲基和混合溶剂中苯的共振吸收峰的化学位移随苯的摩尔分数增加而逐渐移向高场,而且两个甲基共振吸收峰向高场移动的程度不同,α甲基较β甲基为甚。DMF分子中两个甲基和混合溶剂中苯的化学位移可以用线性方程表示(δ=A+Bx),这里x是混合溶剂中苯的摩尔分数。相关系数R接近于-1。     

铝酸锶铕的合成与发光的研究

本文详细报导4(SrEu)O·7Al2O3.磷光体的合成及激活剂Eu2+离子浓度、硼酸、五氧化二磷等对磷光体发光强度,发射光谱和激发光谱的影响.讨论了不同Eu2+离子之间的能量传递.测量了不同Eu2+浓度下磷光体的荧光寿命和长余辉特性.     

正交小波包的构造

本文给出尺度因子ａ＝４时正交小波包的构造，推广了［２，４］引入的正交小波包，并给出相应的分解与再构造算法．本文引入的正交小波包具有保持信号ｆ∈Ｌ^２的线性相位，也讨论了尺度因子ａ＝ｋ（ｋ∈Ｚ，ｋ≥２）正交小波的构造     

LiNbO3:Fe晶体中调制双光束耦合衍射效率的测定

通过对LiNbO₃:Fe晶体中双光束耦合中的任一束光强进行低频调制,其衍射效率比无调制时提高两倍多(由30％提高到76％)。用运动光栅理论解释了这一实验结果。 关键词：     

热辐射驱动烧蚀平面金靶的数值定标定律

利用一维辐射流体力学编码数值研究了辐射烧蚀波在平面金靶中的传播情况,并在常温边界条件下得到了辐射流、烧蚀压、质量烧蚀率和特征等离子体密度的定标定律。     

高压陡脉冲信号测量系统的补偿

本文针对高压陡脉冲测量过程中由于对地电容引起的波形畸变,介绍了一种电感补偿方法,这种补偿回路简便、可靠,可使测量系统的方波响应得到明显的改善。     

经纬仪二轴正交调整方法

本文叙述了经纬仪二轴正交调整的四种方法,其中对偏反射镜法作了理论分析。     

Trefftz,collocation, and other boundary methods—A comparison

In this article we survey the Trefftz method (TM), the collocation method (CM), and the collocation Trefftz method (CTM). We also review the coupling techniques for the interzonal conditions, which include the indirect Trefftz method, the original Trefftz method, the penalty plus hybrid Trefftz method, and the direct Trefftz method. Other boundary methods are also briefly described. Key issues in these algorithms, including the error analysis, are addressed. New numerical results are reported. Comparisons among TMs and other numerical methods are made. It is concluded that the CTM is the simplest algorithm and provides the most accurate solution with the best numerical stability. © 2006 Wiley Periodicals, Inc. Numer Methods Partial Differential Eq, 2007