Microwave-assisted extraction of quercetin and acid degradation of its glycosides in Psidium guajava leaves.

Microwave-assisted extraction (MAE) and microwave-assisted hydrolysis (MAAH) were developed for the sample preparation of guava leaves prior to GC determination of quercetin and its glycosides. Ethanol was selected as the solvent. The optimum MAE temperature, particle size, solvent volume and MAE time are 120 degrees C, 40 - 60 mesh, 20 mL and 5 min, respectively; the optimum MAAH temperature and time, HCl concentration, solvent are 100 degrees C, 5 min, 1.2 mol L(-1) HCl and ethanol, respectively.     

Concentrations of hazardous heavy metals in environmental samples collected in Xiamen, China, as determined by vapor generation non-dispersive atomic fluorescence spectrometry.

Non-dispersive atomic fluorescence spectrometry (NDAFS) coupled with vapor generation (VG) sample introduction was applied to the determination of the concentrations of hazardous heavy metals, such as arsenic, cadmium, lead and mercury, in seawater, soils and total airborne particulate matter (PM) collected around the Xiamen area in China. Almost 100% sample introduction efficiency was achieved by using thiourea and ascorbic acid for the pre-reduction of As(V) to As(III), K3Fe(CN)6 and tartaric acid for pre-oxidation of Pb(II) to Pb(IV), and masking the interferences arising from the co-existing transition metals to As, Cd, Hg and Pb during their vapor generation process. Moreover, a novel sample pretreatment device was developed to avoid the loss of mercury, lead, cadmium and arsenic during sample pretreatment. With such methods, the detection limit (DL) of arsenic, cadmium, lead and mercury was down to 0.08, 0.03, 0.05, 0.01 ng mL(-1) (3sigma), respectively. The relative standard deviations (RSD, n = 11) for arsenic, cadmium, lead and mercury at 10 ng mL(-1) were 0.9%, 1.6%, 1.3% and 2.0%, respectively. The concentrations of hazardous heavy metals in the environmental samples collected in Xiamen, China are in the range from 0.02 +/- 0.001 ng mL(-1) in seawater to 15.3 +/- 0.2 microg g(-1) in soils. Besides flame/GF-AAS and ICP-AES/MS, VG-NDAFS should be another choice for the determination of hazardous heavy metals in environmental samples.     

Exact evaluation of laser linewidth requirements for optical PSKhomodyne communication systems with balanced PLL receivers

The power penalty induced by imperfect phase recovery in PSK homodyne communication systems with balanced phase-locked loop receivers are exactly evaluated. Optimum phase deviations between the mark-state and the space-state bits are used in this study. This study for the first time shows the imperfect-phase-recovery-induced power penalty as a function of laser linewidth with optimum phase deviations considered. It can be estimated from the theoretical result that an optimal balanced PLL receiver requires the laser linewidth as Δν⩽1.15×10^-6× (bit rate) in contrast to the previous reported one Δν⩽5.88×10^-6× (bit rate). We also point out here that the previously reported laser linewidth requirement was wrongly estimated     

Towards a generalized TLM algorithm for solving arbitraryreciprocal and nonreciprocal planar structures

A generalized transmission line matrix (TLM) algorithm is developed in the frequency domain to tackle arbitrary both reciprocal and nonreciprocal anisotropic waveguiding problems. In particular, the modeling issue for arbitrary planar structures is stressed in this work. A new three-dimensional (3-D) condensed node is used to consider the effect of both electric and magnetic constitutive tensors. Various results indicate how the modal dispersive behavior can be manipulated by changing not only the anisotropic characteristics of the substrate, but also the strip/slot geometry as well as the magnitude and orientation of the applied static magnetic field. The present algorithm is useful for CAD and simulation of a large class of gyrotropic waveguide-based microwave and millimeter-wave circuits     

Characterization of ultrashort optical pulses with third-harmonic-generation based triple autocorrelation

We present a method to obtain complete information of femtosecond pulses. By measuring triple-optical autocorrelation directly with third-harmonic generation, without spectral information, a temporal pulse shape can be obtained by analytical calculation without direction-of-time ambiguity. Combining the resulting optical pulse shape with its corresponding optical spectrum, the exact phase and color variations in time can all be recovered with a Gerchberg-Saxton algorithm through an iterative calculation with an O(n) complexity.     

An experimental study of dynamic tensile properties of glass fiber at low-temperatures

Tensile impact experiments of EC8.0−24×7 glass fiber bundles at different low temperaturesT(14°C, −40°C and −10°C) and strain rates ɛ were carried out, and complete stress-strain curves were obtained. Within the range of the experiment temperatures and strain rates, it is found that the initial modulusE, the ultimate strength σ_max and the unstable strain ɛ _b of the glass fiber bundles all increase with ɛ at an identicalT. At an identical ɛ, with the decrease ofT, E and σ_max increase; but ɛ _b increases when 10°C>T>−40°C and decreases when −40°C>T>−100°C. The strain-rate- and temperature-dependent bimodal Weibull statistical constitutive theory was adopted for the statistical analysis of the experimental results, and the Weibull parameters of single fiber were obtained. The results show that the bimodal Weibull distribution function is suitable to represent the strength distribution of the glass fiber at low temperature and different strain rates. The differences in the mechanical properties between EC8.0−24×7 and EC5.5−12 ×14 glass fiber bundles were also discussed. Project supported by the National Natural Science Foundation of China (No. 19772058).     

Erds方程的全等解

本文运用初等方法给出了Erds方程的所有全等解.     

Tri-band frequency selective surface with circular ring elements

Theoretical analysis, physical reasonings, and experimental verifications are presented for a frequency selective surface with circular ring elements. Both double-screen and single-screen designs are generated for a tri-band system that reflects the X-band signal while transmitting through the S- and Ku-band signals. In these designs, the dielectric loading effect is used to reduce ring size and element spacing and thus avoid the grating lobe problem. The circular ring element is very insensitive to a large variation of the RF incident angle     

90°分束偏光镜光强分束比研究

给出了90°分束偏光镜的e,o光光强分束比的计算公式,以及光强分束比随光波长的变化曲线;在6328Å测得的光强分束比与计算值是一致的。     

淀积条件对GDa—SiNx薄膜电学特性的影响

本文讨论了用辉光放电法制备氮化硅薄膜时衬底温度、射频功率和气体流量比对薄膜的电导率、介电常数和击穿强度的影响。通过优化生长条件，制备了优质非晶氮化硅薄膜，其介电常数为７．５、击穿强度为５．５ＭＶ／ｃｍ、电导率为１０－１３（Ωｃｍ）－１。