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31.
Sandberg RL Paul A Raymondson DA Hädrich S Gaudiosi DM Holtsnider J Tobey RI Cohen O Murnane MM Kapteyn HC Song C Miao J Liu Y Salmassi F 《Physical review letters》2007,99(9):098103
We present the first experimental demonstration of lensless diffractive imaging using coherent soft x rays generated by a tabletop soft-x-ray source. A 29 nm high harmonic beam illuminates an object, and the subsequent diffraction is collected on an x-ray CCD camera. High dynamic range diffraction patterns are obtained by taking multiple exposures while blocking small-angle diffraction using beam blocks of varying size. These patterns reconstruct to images with 214 nm resolution. This work demonstrates a practical tabletop lensless microscope that promises to find applications in materials science, nanoscience, and biology. 相似文献
32.
Motivated by our desire to understand the biophysical mechanisms underlying the swimming of sperm in the non-Newtonian fluids of the female mammalian reproductive tract, we examine the swimming of filaments in the nonlinear viscoelastic upper convected Maxwell model. We obtain the swimming velocity and hydrodynamic force exerted on an infinitely long cylinder with prescribed beating pattern. We use these results to examine the swimming of a simplified sliding-filament model for a sperm flagellum. Viscoelasticity tends to decrease swimming speed, and changes in the beating patterns due to viscoelasticity can reverse swimming direction. 相似文献
33.
Electrochemical Vicinal Difluorination of Alkenes: Scalable and Amenable to Electron‐Rich Substrates
Sayad Doobary Alexi T. Sedikides Henry P. Caldora Darren L. Poole Alastair J. J. Lennox 《Angewandte Chemie (International ed. in English)》2020,59(3):1155-1160
Fluorinated alkyl groups are important motifs in bioactive compounds, positively influencing pharmacokinetics, potency and conformation. The oxidative difluorination of alkenes represents an important strategy for their preparation, yet current methods are limited in their alkene‐types and tolerance of electron‐rich, readily oxidized functionalities, as well as in their safety and scalability. Herein, we report a method for the difluorination of a number of unactivated alkene‐types that is tolerant of electron‐rich functionality, giving products that are otherwise unattainable. Key to success is the electrochemical generation of a hypervalent iodine mediator using an “ex‐cell” approach, which avoids oxidative substrate decomposition. The more sustainable conditions give good to excellent yields in up to decagram scales. 相似文献
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Henry T. Kalinoski Leonard O. Hargiss 《Journal of the American Society for Mass Spectrometry》1992,3(2):150-158
Direct injection from a capillary supercritical fluid chromatography system was used as an inlet technique for chemical ionization (CI) and low energy collision-induced dissociation (CID) mass spectrometry of a series of low volatility nonionic surfactant mixtures. Characteristic fragment ions produced by CID for various classes of nonionic surfactant molecules were found to depend greatly on the structure of the surfactant hydrophobe. This was the case even when the charge on the molecule appeared localized away from the hydrophobe. Numerous decomposition pathways are suggested by the fragment ions produced. The use of direct supercritical fluid injection as an inlet technique does not appear to influence adversely the ability to produce cm mass spectra. Direct supercritical fluid introduction allows CI to be compared with other ionization mechanisms more commonly used for multifunctional, low volatility samples. 相似文献
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Daewook Kim Heejoo Choi Trenton Brendel Henry Quach Marcos Esparza Hyukmo Kang Yi-Ting Feng Jaren N.Ashcraft Xiaolong Ke Tianyi Wang Ewan S.Douglas 《光电进展(英文版)》2021,4(6):20-43
Significant optical engineering advances at the University of Arizona are being made for design,fabrication,and con-struction of next generation astronomical te... 相似文献
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A tournament T on any set X is a dyadic relation such that for any x, y ∈ X (a) (x, x) ? T and (b) if x ≠ y then (x, y) ∈ T iff (y, x) ? T. The score vector of T is the cardinal valued function defined by R(x) = |{y ∈ X : (x, y) ∈ T}|. We present theorems for infinite tournaments analogous to Landau's necessary and sufficient conditions that a vector be the score vector for some finite tournament. Included also is a new proof of Landau's theorem based on a simple application of the “marriage” theorem. 相似文献
40.
Morvan Salez Pascal Febvre William R. Mcgrath Bruce Bumble Henry G. Leduc 《International Journal of Infrared and Millimeter Waves》1994,15(2):349-368
A waveguide SIS heterodyne receiver using a Nb/AlOX/Nb junction has been built for astronomical observations of molecular transitions in the frequency range 600 GHz - 635 GHz, and has been successfully used at the Caltech Submillimeter Observatory (CSO). We report double sideband (DSB) receiver noise temperatures as low as 245 K at 600 GHz -610 GHz, and near 300 K over the rest of the bandwidth. These results confirm that SIS quasiparticle mixers work well at submillimeter-wave frequencies corresponding to photon energies of at least 90% of the superconductor energy gap. In addition, we have systematically investigated the effect on the receiver performance of the overlap between first-order and second-order photon steps of opposite sign at these frequencies. The receiver noise increases by as much as 40% in the region of overlap. We infer potential limitations for operating submillimeter-wave Nb/AlOx/Nb mixers. 相似文献