The local ultraconvergence of high‐order finite element method for second‐order elliptic problems with constant coefficients over a rectangular partition

In this article, we will discuss the local ultraconvergence of high‐degree finite element method based on a rectangular partition for the second‐degree elliptic problem with constant coefficients in Ω ? ?² , u( y ) = 0 on ?Ω . Based on suitable regularity, ultraconvergence of the displacement of the extrapolated kth (k ≥ 3) degree finite element solution has been obtained by an extrapolation technique. Finally, numerical experiments are applied to demonstrate our theoretical findings.     

碳原子的再分布对铂上高质量单层石墨烯生长的影响

二维材料石墨烯以其独特的性质显示出在众多领域的应用潜力。化学气相淀积(CVD)作为最有效的生长单层石墨烯的方法得以良好发展。但在CVD方法中,频繁出现的多层石墨烯“点”严重影响单层石墨烯的有效面积,进而限制了石墨烯在很多场景中的应用。本文通过引入一个新的阶段-再分布阶段,使得在分解阶段溶解在铂片中的碳原子重新分布,进而减少了多层石墨烯“点”的数目。单层石墨烯的平均面积增加到16000μm₂,较未引入再分布阶段的单层面积增大了八倍。最后,拉曼光谱仪的测试结果说明了新方法下生长的石墨烯的高质量特征。     

以车代磨加工柱塞喷涂层的工艺性能研究

针对柱塞喷涂重熔后磨削加工用时长,效率低,严重影响产品生产周期这一瓶颈问题,本文介绍了一种安全可靠、简单可行的新工艺方法,并通过这种以车代磨新工艺方法的探究和工艺参数的验证与实施,缩短了喷涂柱塞的加工周期,大幅度的提高了加工效率,很好地解决了喷涂柱塞加工周期长,效率低这一生产瓶颈问题。既提高了喷涂柱塞的产品质量,又极大的降低了加工成本,也为喷涂层这种高硬度材料的高效硬加工进行了很有意义的探索,并有很好的推广价值。     

高速传输系统用低损耗单模光纤的研究

介绍了国际上低损耗单模光纤的研究进展,从理论上分析了低损耗单模光纤实现的技术途径。通过对石英玻璃物理特性的研究,探索出石英玻璃光纤的退火工艺,以降低光纤的内应力从而降低光纤的衰减。采用自主知识产权的专利技术制造的光纤在1 310、1 550和1 625nm波长的衰减典型值分别为0.320、0.182和0.195dB/km。该光纤的技术指标优于ITU-T国际标准和GB/T规定的光纤指标值。     

电信运营商大数据应用浅析

在大数据时代,电信运营商如果不能挖掘出数据的价值可能彻底被管道化。当前大数据成为运电信营商向创新经营和精细化运营转型的强大推动力。剖析了电信运营商大数据应用的意义、优势、存在问题,并在此基础上提出了电信运营商大数据应用建议。     

基于TD-LTE技术实现企业客户视频传输业务的研究与应用

随着社会安全意识的提高,政府、企业集团客户视频监控传输类需求呈现快速的上升趋势,尽管视频传输业务在有线通信资源满足的条件下已经有较为成熟的解决方案,但是在无法铺设有线管道或现有管线资源无法满足的场景如河坝、山区等仍然面临很大的设计实施困难,尚未形成有效的解决措施。针对以上问题,结合TD-LTE无线通信的传输特点,研究了通过TD-LTE无线通信方式实现集团客户视频传输业务的方法,并结合TD-LTE无线通信的特点给出了相应的解决方案。     

Synthesis and Herbicidal Activity of [(Substituted Phenoxyacetoxy) (Substituted Phenyl)Methyl](Methyl) Phosphinates Containing Fluorine

Abstract

A series of [(substituted phenoxyacetoxy)(substituted phenyl)methyl](methyl)phos- phinates containing fluorine were designed and synthesized. All the synthesized compounds were identified by elemental analysis, IR, ¹H NMR, mass spectrometry. O-methyl [(2-fluorophenoxyacetoxy)(2,4-dichlorophenyl)methyl](methyl)phosphinate was further analyzed by X-ray single-crystal diffraction. Their herbicidal activity against a set of weed species was examined. Some of the compounds showed potential herbicidal activity, which provided some indications for further studies on structure modification.

Supplemental materials are available for this article. Go to the publisher's online edition of Phosphorus, Sulfur, and Silicon and the Related Elements to view the free supplemental file.     

Two Thiourea-based Colorimetric Sensors for Anions: Structure and Binding Study

Two colorimetric thiourea-based chemsensors with two relatively rigid arms, 2A and 2B, were synthesized. Their binding abilities with halide anions, AcO^?, [Formula: See Text] were studied by UV-Vis spectroscopy in DMSO. The two sensors showed a notable selective color response to F^? anion from colorless to green-yellow in recognition. The structures of the two sensors and their binding behaviors are discussed. The association constants were calculated by nonlinear fittings of 1:1, 1:2 or 1:1 to 1:2.     

Moisture absorption and diffusion in an underfill encapsulant at T > T g and T < T g

Moisture absorption and diffusion behavior of an underfill material used for electronic packaging with a glass transition temperature (T _g) slightly above room temperature have been investigated by the sorption thermogravimetric analysis technique. It has been found that moisture diffusion in this material follows the Fick’s diffusion model, and moisture absorption–desorption is reversible and repeatable. Based on moisture-induced mass gain versus time curve, the diffusion constant can be determined. It was found that below T _g, moisture diffusivity exhibits an Arrhenius temperature dependence, which changes to a different Arrhenius temperature dependence as the temperature increases to T > T _g. The change in diffusivity from T < T _g to T > T _g is accompanied by a significant decrease in the energy barrier for moisture diffusion. Results shed light on the change in moisture diffusion in polymer-based materials in the glassy and the rubbery state.