Red Electroluminescence and Photoluminescence from Novel Binuclear Europium Complex with Squaric Acid Ligand

Organic electroluminescent devices (OELDs) have attracted much attention for several years because of their potential application in large area, multi-colored flat panel displays1-5. The green organic EL display using Alq3 as emitter was commercialized in 19976. However, red-emitting OELD with excellent properties has not been well developed. In order to realize practical full-color OELDs, it is considered very important to develop red and blue emitting materials with excellent propert…     

A Novel Mo—Doped Compound with Graphite—Like Structure：[H3O]2V3O8

1 INTRUDUCTION During the last few years, there has been much effort paid to the synthesis of new transition-metal oxides that might be active hosts for intercalation reactions. Vanadium and molybdenum in higher oxidation states with higher reacting ability tend to form polynuclear, anionic metal-oxygen clusters with an extraordinary variety of the relevant topology and electronic structures[1~3]. The preparation of the corresponding clusters is of special interest for different aspects …     

The Reaction Of Metal Trialkyls With Benzo[H]Quinolin-10-ol

IntroductionThechemistryoforganoaluminum,organogalliumandorganoindiumcomplexeshasattractedmuchat'tentionduenotonlytotheirinterestingstructuralandchemicalpropertiesbutalsotheirapplicationinsemiconductormaterialsl-5.InthecourseofourstudiesonexploringvolatileMOCVDprecursorsthathavethepropertiesoflowertoxicityandhigherstability,wehaverecentlyreportedonthesynthesisandcharacterizationofintermolecularadducts'-',novelbondingmodecomplexes",',andthecomplexesinwhichN/Omixed-donorcrownethersasligands'l'…     

随机Richlet级数的增长性

本文构造了全平面上的无限级Dirirchlet级数,使得它对型函数的增长性与一个已知的不同分布随机Dirichlet的增长性相同,从而通过前者增长性与指数,系数的关系可研究后者的增长性.     

基于微分算子的边缘检测法在基因芯片图像识别中的应用

一种基于梯度算子和拉普拉斯算子检测医学基因芯片荧光数字图像边缘的方法．数字图像经过图像增强等预处理以后，突出了我们感兴趣的数字图像特征，根据数字图像灰度变化的趋势，用灰度变化的一阶导数(梯度算子)检测图象中的边缘区域；用灰度变化的二阶导数确定图像边缘的中心位置．最后根据某些预定的准则把满足这些准则的象素组成一条边缘．     

ISOVALEROYL OXOKADSURANE,A NOVEL DIBENZOCYCLOOCTADIENE LIGNAN POSSESSING A SPIROBENZOPURANOID SKELETON

Isovaleroyl oxokadsurane, a novel dibenzocyclooctadiene lignan pos-sessing a spirobenzofuranoid skeleton was isolated from the stems of Kadsura coccinea.Its structure and relative configuration were determined by X-ray diffraction analysis.     

热释电激光能量计

本文通过求解热传导方程分析了几种脉冲辐射作用下热释电信号的解析表达式。用简化模型和数值计算两种方法着重讨论了在近似激光脉冲辐射作用下，信号电压的规律性。得到了峰值电压正比于激光能量的条件和结论。介绍了PLEM-1型激光能量计的原理结构、电路和性能，并对仪器误差进行了初步分析。     

Optimal adaptive generalized Pólya urn design for multi-arm clinical trials

A class of optimal adaptive multi-arm clinical trial designs is proposed based on an extended generalized Pólya urn (GPU) model. The design is applicable to both the qualitative and quantitative responses and achieves, asymptotically, some pre-specified optimality criterion. Such criterion is specified by a functional of the response distributions and is implemented through the relationship between the design matrix and its first eigenvector. The asymptotic properties of the design are studied using the existing methods on GPU. Some examples for commonly used clinical designs are given as illustration.     

HR——500ⅡA型自动温控红外热熔机整机结构设计

以红外热源的辐射热来热熔镀在印制电路板上的锡铅合金,具有很多的优点.本文着重对实施这一热熔工艺的专用设备——红外热熔机的整机造型、人机关系、各主要部件的功能和结构设计,作了较为详细的分析.