纳米金/β-环糊精复合修饰碳糊电极测定亚硝酸盐

本文研究了亚硝酸盐(NO_2~-)在纳米金和β-环糊精复合修饰碳糊电极(AuNPs-β-CD/CPE)上的电化学行为。实验结果表明,与裸CPE相比,AuNPs-β-CD/CPE对NO_2~-的电化学氧化有显著的促进作用,其氧化峰电流显著增加。同时用循环伏安法(CV)、计时电流法(CA)测定了NO_2~-在AuNPs-β-CD/CPE上的电极反应动力学参数,用线性扫描伏安法(LSV)法测得NO_2~-氧化峰电流与其浓度在6.0×10-6~8.0×10-3 mol·L-1范围内呈良好的线性关系,检出限(S/N=3)为5.7×10-7 mol·L-1。将该传感器应用于水样的检测,相对标准偏差在0.15%~1.40%之间,回收率达99.3%~104.0%,检测结果符合定量测定要求。     

有限CN-p-群

每个子群都C-正规的有限群称为CN-群.本文首先给出二元生成的CN-p-群的完全分类.在此基础上得到CN-p-群的结构:当p为奇素数时,有限群G为CNp-群当且仅当G的每个元都平凡地作用在Φ(G)上;有限群G为CN-2-群当且仅当对任意给定的a∈G,都有对任意g∈Φ(G),g~a=g或者对任意g∈Φ(G),g~a=g~(-1).最后给出两个CN-p-群的直积是CN-p-群的判定条件.     

1stOpt软件在蔗糖水解实验教学中的应用

将1stOpt软件用于物理化学实验蔗糖水解反应速率常数的测定中，在无需严格记录反应开始时间和测定反应终了旋光度的情况下，通过非线性拟合无需编程及公式变换就可以简单方便准确地得到反应速率常数，避免了传统数据处理方法所带来的人为误差，可以补充和改进物理化学实验的教学。     

Differential equation dynamical system based assessment model in GNSS interoperability

With the development of Global Navigation Satellite System (GNSS),the idea of GNSS interoperability is born and has become the focus of study in the field of satellite navigation.The popularity for GNSS to augment the interoperability with the existing ones necessitates the study of the assessment algorithm of this idea.In this paper,an assessment algorithm for interoperability comprehensive benefits based on the differential equation dynamical system is discussed.There are two important aspects in GNSS tha...     

An optimized distributed fiber Bragg grating sensing system based on optical frequency domain reflectometry

In this paper,the waveforms in time domain and frequency domain of two kinds of optical frequency domain reflectometry (OFDR) sensing systems are compared,which use common fiber Bragg grating (FBG) and...     

鲁棒声学事件检测综述

声学事件是指一段单一完整并能够引起人们感知注意的短时连续声音信号,而声学事件检测是指对这些声学事件进行识别。随着便携式摄像机与视频网站的迅猛发展,基于内容的声学事件检测在各领域的应用日趋广泛,例如个性化多媒体搜索、数字图书馆、网络管理与信息安全等。近年来,尽管研究者们提出了很多声学事件检测方法,但是由于采集设备、采集环境与传输条件等的千差万别,新环境下的音频数据日趋繁杂,使得类内数据差异较大且类间数据易混,从而导致传统识别方法的性能急剧下降,因此迫切需要研究当前环境下的鲁棒声学事件检测方法。     

利用显微拉曼光谱技术鉴别印文形成时间的应用研究

采用激光显微拉曼光谱技术,选择10种不同品牌和型号的印泥(油)盖印印文的历时性样本,利用印文拉曼光谱中的1089 cm~(-1)和1235 cm~(-1)处特征峰的相对面积值(I)分析纸张、温度、热老化因素对印文形成时间的影响,探讨盖印时间与峰面积相对值(I)的关系。结果表明,I值随时间呈现规律性变化,尤其在近期内盖印印文的变化规律明显,适用于印文形成时间的鉴别,是一种准确、无损的检验方法。     

直升机导航设备的现状与发展

概述了直升机导航设备的重要性，介绍了目前直升机导航设备的国内外应用情况， 分析了直升机载导航设备的发展方向。     

Optimization of frequency characteristics for SAW device using apodization weighting method

To calibrate the tracing performance of the thirty meter telescope(TMT)tertiary mirror,for the special requirement of the TMT,the laser tracker is used to verify the motion.Firstly,the deviation is divided into two parts,namely,the repeatable error and the unrepeatable part.Then,based on the laser tracker,the mearturement and evalutation methods of the rigid body motion for the mirror are established,and the Monte Carol method is used to determine the accuracy of the mothod.Lastly,the mothod is applied to the turn table of a classical telescope and the residual error is about 4 arc second.The work of this paper will guide the next desgin and construction work of the thirty meter telescope tertiary mirror.     

Photonic envelope detection and fiber transmission of 24 GHz IR-UWB signal based on phase modulation

A novel scheme for photonic envelope detection and fiber transmission of 24 GHz impulse radio ultra-wideband(IRUWB) signal is proposed based on phase modulator(PM). In the system, an optics assisted envelope detection unit(OAEDU) is used for filtering one of the first sidebands at the output of PM, then this narrow band optical signal transfers over single-mode fiber(SMF), and the envelope of 24 GHz IR-UWB signal is obtained after photodetection(PD) and low pass filter(LPF). The numerical simulation results show that the combination of PM and OAEDU can alleviate the fiber chromatic dispersion(CD) effectively. The proposed system may provide a simple and cost-effective solution for IR-UWB receiver.