单丁基磷酸酯的合成与表征

本文报道用三氯氧磷酯化、水解方法制备单丁基磷酸酯，用红外、核磁共振，质谱等方法对其结构进行了分析与表征。     

基于辛几何理论的非均匀媒质中电磁波传播问题的研究

本文提出了一种利用辛几何理论求解非均匀媒质中电磁波传播问题的新方法,首先引入新的波向量空间与原来的物理空间共同构成辛空间,将物理空间中波的传播问题提升为辛空间中的Ｌａｇｒａｎｇｅ子流形的问题,并通过适当的投影变换可以处理电磁波在非均匀媒质中传播的焦散问题。     

馈源阵面排列对偏置多波束天线特性的影响

以３７单元馈源阵为例,就用于卫星移动通信系统中的偏置多波束天线进行分析探讨：在原有两种馈源阵阵面排列形式的基础上,又提出了第三种排列形式,即馈源阵的球面排列形式,并对这三种形式下偏置多波束天线的远场特征进行了计算比较,得出了一些有益的结论;另外,将馈源阵阵面适当地偏离焦点也可使多波束天线的远场特性得以改善。     

一种A da95分布计算的实现模型

在研究 Ａｄａ９５ 分布计算语义的基础上,提出了一个支持 Ａｄａ９５ 的分布计算的实现模型 并讨论了在该环境下实现 Ａｄａ９５ 分布计算所存在的问题和解决方法,以及如何实现非 Ａｄａ９５ 分布计算语义的 Ａｄａ 程序的分布并行计算的问题对于后者,着重讨论了远程会合的实现问题     

The Bergman kernel function: Explicit formulas and zeroes

We show how to compute the Bergman kernel functions of some special domains in a simple way. As an application of the explicit formulas, we show that the Bergman kernel functions of some convex domains, for instance the domain in defined by the inequality , have zeroes.

     

用动力学法测杨氏模量实验及其实验装置的研制

介绍了新研制的用动力学法杨氏模量的实验装置,它具有功耗低,灵敏度高的特点;教学中测量悬线不同位置时的共振频率,用作图法拟合出其精确值,以减少由于悬线不在节点引起的系统性误差,测量精密度比传统的静态拉伸法高一个量级以上。     

Solid-Phase Microextraction Followed by Gas Chromatography-Mass Spectrometry Analysis of the Volatile Components of Flos Chrysanthemi indici in Different Growing Areas

Headspace solid phase microextraction coupled with gas chromatography-mass spectrometry (HS-SPME-GC-MS) has been applied to the determination of the volatile compounds of a common traditional Chinese medicine , Flos Chrysanthemi indici. Twenty-six compounds were identified by the present method, which are similar to the results from steam distillation. Difference in analysis from ten growing areas was found to be in their relative content and total concentrations. Four active compounds (cineole, 3-thujanone, borneol and bornyl acetate) were applied to the evaluation of the quality of Flos Chrysanthemi indici from different areas. By comparing their peak areas, it was found that Flos Chrysanthemi indici with the best quality was from Hangzhou in China. These results show that HS-SPME-GC-MS is a simple, rapid and solvent-free method for the analysis of the volatile compounds in this material and a potential tool for its quality assurance.     

用DiffServ MPLS流量工程保证NGN承载网的QoS

在下一代网络（NGN）中，提供分等级、分业务、细粒度的Qos保证机制是一个关键性的问题。本文分析TNGN实现Qos保证的思路，认为最终解决NGN的QoS的方法，既不能单纯地采用IP过载的机制，也不能够照搬PSTN／ATM的QoS技术，而应该是两种技术的融合。并根据这个思路提出DiffServ MPLS流量工程解决NGN承载网的Qos问题的方案和实现原理。最后详细解释了如何应用DiffServ MPLS流量工程解决NGN中话音质量的问题。     

Multiwavelength Q-switched CO2 laser with continuous discharge

A low-pressure (20 mbar) CO₂ laser allows to extract pulses at several selected wavelengths simultaneously from the same active medium. We demonstrated this, using an industrial laser modified by a Q-switch and a resonator with two branches. In one branch the wavelengths are spatially separated, whereas in the other they oscillate in one common transverse mode. We designed a multi-wavelength resonator which requires a single additional reflector compared to usual laser cavities. It provided tunable oscillation at six wavelength simultaneously.     

电感耦合等离子体原子发射光谱法及离子选择电极法测定荧光级氧化钇中痕量铈的研究

文章描述了荧光级氧化钇中痕量稀土铈的测定方法,在溴酸钾存在下,5摩尔/升HNO_3介质中,以P507萃取微量铈,然后有机相用硝酸、过氧化氢反萃取、再将水相浓缩定容,然后以电感耦合等离子体原子发射光谱法分析。同时用铈的离子选择电极以二次标准加入法作第二种手段分析。样品溶液以乙醇预去溶方式引入等离子体,测定下限为2微克/克,方法简单、快速、准确。离子选择电极法测定铈离子下限1×10～(-5)摩尔/升,回收率为94-101%,方法简单,结果满意、价格便宜。