Toward phenanthridin-2-ylidene: electrophilicity versus acidity in planar-constrained C-aryl iminium salts

A phenanthridinium salt was prepared in four steps, including an intramolecular CH-arylation and a hydride abstraction reaction. Treatment with sterically demanding bases does not lead to the corresponding carbene, but rather to addition products: the planar-constrained geometry significantly enhances the electrophilicity over the acidity of C-aryl iminium salts.     

A Novel Contactless Method for Characterization of Semiconductors：Surface Electron Bean Induced Voltage in Scanning Electron Microscopy

We present a novel contactless and nondestructive method called the surface electron beam induced voltage (SEBIV) method for characterizing semiconductor materials and devices.The SEBIV method is based on the detection of the surface potential induced by electron beams of scanning electron microscopy (SEM).The core part of the SEBIV detection set-up is a circular metal detector placed above the sample surface.The capacitance between the circular detector and whole surface of the sample is estimated to be about 0.64pf.It is large enough for the detection of the induced surface potential.The irradiation mode of electron beam (e-beam) influences the signal generation When the e-beam irradiates on the surface of semiconductors continuously,a differential signal is obtained.The real distribution of surface potentials can be obtained when a pulsed e-beam with a fixed frequency is used for irradiation and a lock-in amplifier is employed for detection.The polarity of induced potential depends on the structure of potential barriers and surface states of samples.The contrast of SEBIV images in SEM changes with irradiation time and e-beam intensity.     

适于12位和16位A／D转换器LSI的片上校准技术

晶体半导体公司研制了分辨率为16位、最大转换速度50k次/秒的A/D转换器和分辨率为12位、最大转换速度1M次/秒的A/D转换器LSI。这两种A/D转换器LSI都具有自校准非线性误差的功能,这种功能可调整与各位相对应的2~N(N是位数)个加权电容器的电容比。各位的电容器由偶数个小容量电容器构成,改变电容器数量的同时即可进行校准。用集成在芯片上的微计算机控制校准操作,可以使LSI制造过程中的试验变得简单。即使在用户正在使用着的系统上也能够自动进行校准,因而对温度变化和时效变化也能够进行补偿。     

Some hydrodynamic aspects of 3-phase inverse fluidized bed

Hydrodynamics of 3-phase inverse fluidized bed is studied experimentally using low density particles for different liquid and gas velocities. The hydrodynamic characteristics studied include pressure drop, minimum liquid and gas fluidization velocities and phase holdups. The minimum liquid fluidization velocity determined using the bed pressure gradient, decreases with increase in gas velocity. The axial profiles of phase holdups shows that the liquid holdup increases along the bed height, whereas the solid holdup decreases down the bed. However, the gas holdup is almost uniform in the bed.     

学了统计学可以有什么样的作为?(续)──介绍统计学的特点和用处

Ⅲ、统计学家是做什么的? 为了描述统计学家工作的各个领域,最好的方法是给出大量的事例.限于篇幅,这里叙述六个事例.第一个事例描述统计学家的一个新的且很有希望的出路,就是在私人单位里当顾问.许多统计学家例如大学里的那些统计学家,在个人的部分时间从事于这种顾问工作. 经历1 A.B.先生与几个公司和研究所一起工作.几乎每周一次,每次花两到四小时与他的委托人中的每一个人联系,虽然他极少看见他们中的一些人.他与他们中的许多人每天都要通过电话谈话.他经常研究他们的问题,并且为了进行工作他或者重复写他的指示或者根据研究的结果所进…     

用单片机产生有限带宽伪随机信号

由线性反馈移位寄存器产生出周期为ｐ＝２＾１１－１的伪随机白噪声，利用快速傅里叶变换及其逆变换去除了其中低于３５０Ｈｚ和高于５５０Ｈｚ的分量，获得带宽在３５０－５５０Ｈｚ之间的伪随机信号。     

《PTC技术交流会暨通信设备过电流保护用PTC热敏电阻行业标准预审会》报导

《ＰＴＣ技术交流会暨通信设备过电流保护用ＰＴＣ热敏电阻行业标准预审会》报导广东省邮电科学研究所于１９９４年１０月１０～１５日在深圳市主持召开了《ＰＴＣ技术交流会暨通信设备过电流保护用ＰＴＣ热敏电阻行业标准预审会》，会议收到论文９篇，国内外专家及相关人...     

126Cs的高自旋态能级结构

利用融合蒸发反应¹¹⁶Cd(¹⁴N,4n)¹²⁶Cs布居了¹²⁶Cs的高自旋态.观测到了100多条新的γ跃迁和相应的能级,建立了双奇核¹²⁶Cs由9个转动带构成的能级纲图.尝试性地指定了大部分能级的自旋和宇称以及各转动带的Nilsson单粒子组态.极大地丰富了已有的实验结果.     

数据通信传送业务和协议

CCITT和ISO现在正在开发统一质量的的数据传送业务和支持这种业务的传送协议的国际标准,这些标准用于独立于网络的通用网络。本文对传送业务的用途、结构,以及它和通信网的关系进行了介绍。同时也对所开发的传送业务和协议标准作了叙述。     

日本菊花螺Siphonaria Japonia化学成分的研究(I)

近年来相继从菊花螺属(Siphonaria)海洋软体动物中分离出一系列聚丙酸酯(Polypropi-onate)类化合物.这类化合物在自然界罕见,被认为是菊花螺属软体动物的典型代谢产物.本文实验所用的菊花螺采自福建省湄洲湾莲城半岛.该动物味很苦,有清凉解毒之功.