芳烃混合物的三维荧光光谱的降秩因子分析

本文介绍了降秩因子（ＲＡＦＡ）方法，它是从一个多组分混合物中直接定量计算其中某一组分，而不必知道其他组分的物种及含量的一种定量分析的数学方法。它适用于双线性的数据。本实验首先将荧光分光光度计与外接计算机相连，以获得样品的激发－发射矩阵（ＥＥＭ），再用ＲＡＦＡ方法对蒽，萘，菲，芘，芴，Ｑｕ六种标样的一至五组分的混合物进行定量分析，获得满意的结果。     

微细加工技术在微光开关制造中的应用

微光开关是新一代全光通信网络中的关键器件。利用微细加工技术制造微光开关具有很多突出的优点，受到了广泛的研究。总结了几种典型的微光开关制造中运用的微细加工技术，并介绍了它们的应用和相应的特点。     

A shifted gamma distribution model for long-range dependent Internet traffic

It is important to characterize the distributional property and the correlation structure of traffic arrival processes in modeling internet traffic. The conventional fractional Gaussian noise (fGn) model fails in characterizing the distributional property when the distribution of the input traffic rates is nongaussian. We propose a shifted gamma distribution model which can solve this problem. A linear-time generation algorithm is also given.     

线粒体改变在超微结构病理诊断中的作用

线粒体是细胞生理功能必需的细胞器。线粒体DNA的缺陷是许多临床疾病的基础，许多不同疾病都具有非特异性的线粒体的病变。本文主要综述了在不同病理情况下，线粒体主要的结构变化，以及其在超微结构病理诊断中的作用。     

一种短波跳频网的固定信道分配算法

本文基于顺序包和最大包分配算法，从需求向量为出发点，提出了一种将顺序包与最大包两种算法相结合的固定信道分配方案。研究结果表明，在分配所需要的信道数和对信道连续性的要求方面，该算法与其它算法相比具有优良的效果，并且还可用信道不连续的情形。     

含ZnS∶Mn~(2+)纳米晶玻璃中Mn~(2+)三种格位态的EPR研究

通过对ＺｎＳ∶Ｍｎ２＋ 不同含量的钠硼硅玻璃发光和激发光谱测量， 发现Ｍｎ 离子可能占据替位（Ｍｎ２＋ ）Ｓｕｂ 和间隙（Ｍｎ２＋ ）ｉｎｔ两种格位． 进一步的电子顺磁共振（Ｅｌｅｃｔｒｏｎ Ｐａｒａｍ ａｇｎｅｔｉｃＲｅｓｏｎａｎｃｅ， ＥＰＲ）实验证实了这一判断， 并从ＥＰＲ谱确认（Ｍｎ２＋ ）Ｓｕｂ， （Ｍｎ２＋ ）ｉｎｔ和Ｍｎ 团三种格位态的存在． 观测到ｇ 因子和超精细结构（ＨＦＳ）常数随纳米晶粒径的减小而增大． 这可能是由于量子限域效应下ＺｎＳ的ｓｐ３ 和Ｍｎ 的３ｄ５ 电子态杂化和表面态所引起的．     

Development of a novel HPLC‐MS/MS method for the determination of aconitine and its application to in vitro and rat microdialysis samples

A sensitive and selective LC‐MS/MS method was developed and validated for the determination of aconitine in microdialysate and rat plasma. Extraction of plasma sample was conducted by use of 1% trichloracetic acid and acetonitrile solution with 10 ng/mL internal standard (propafenone) spiked. Microdialysates were analyzed without sample purification. After sample preparation, 2 µL were injected and separated with an isocratic mobile phase consisting of acetonitrile:0.1% formic acid (60:40, v/v) at a flow rate of 0.3 mL/min. The Agilent G6410A triple quadrupole LC/MS system was operated under the multiple‐reaction monitoring mode (MRM) using the electrospray ionization technique in positive mode. Overall, the assay exhibited good precision and accuracy. The diffusion properties of aconitine investigated in in vitro microdialysis experiments revealed unfavourable concentration dependence avertable by keeping a constant pH 5.77 using isotonic phosphate buffer solution as perfusate. The mean relative recoveries were 48.23% [coefficient of variation (CV 4.47%)] and 55.38% (CV 2.89%) for retrodialysis and recovery experiments, respectively. The in vivo recovery of aconitine was 34.48% (CV 3.05%) and was stable over the 6 h study period. Following characterization of aconitine both in vitro and in vivo microdialysis, the developed setting is suitable for application in pharmacokinetics and pharmacodynamics studies. Copyright © 2009 John Wiley & Sons, Ltd.     

On cubic graphs which are irreducible for nonorientable surfaces

Let ∑?_n denote the nonorientable surface of nonorientable genus n. A graph G is irreducible for ∑?_n if G does not embed in ∑?_n but any proper subgraph does embed. Let I₃∑?_n) denote the set of cubic irreducible graphs for ∑?_n. This note provesTheorem. I₃(∑?_n) is finite for eachn.     

Non-free torsion-free profinite groups with open free subgroups

For every integere≧3 there exists a non-free torsion-free profinite group containing a as an open subgroup. Supported by Rothschild Fellowship.