第二代北斗客户端用射频声表面波滤波器的研制

介绍了一种可满足第二代北斗客户端用B3波段载频滤波的声表面波(SAW)射频滤波器。该滤波器采用“5换能器纵向耦合结构+谐振器”的混合型设计方案,在充分考虑了SMD3030A封装及键合引线寄生影响后,成功研制出-1 dB带宽35 MHz、插入损耗2.2 dB、矩形系数1.9的滤波器产品。结果表明,仿真与实测吻合性较好,证明了该设计方案的可行性。     

A rare-earth spectral traceability anti-counterfeiting detection technology

In this paper, a rare-earth spectral traceability anti-counterfeiting detection technology is proposed. Configure rare-earth samples No.1, No.2 and No.3 with different doping ratios. The spectral signals of these three samples are collected and integrated into a sample library. The traceability anti-counterfeiting detection is to compare the spectral information of the samples to be tested with the established sample library by selecting specific wavelength points for light intensity values. If the sample to be measured meets the light intensity range of the established sample library at a specific wavelength point, the sample model will be output. If it does not meet the light intensity range, the sample to be tested is fake. After testing, the anti-counterfeit rate of samples No.1, No.2 and No.3 can reach 100%. This testing process does not destroy the sample, and the anti-counterfeit effect is unique and reliable.     

一种高动态低信噪比环境下基于多样本点串行快速傅里叶变换的信号捕获方法

高超音速技术是未来空间飞行器的发展趋势,同时对通信平台在超高动态、低信噪比环境下的快速捕获能力也提出了新的挑战.针对经典捕获算法受频偏影响的局限性,该文提出一种基于信号多样本点串行快速傅里叶变换的信号捕获算法(MS-FFT),所提算法通过串行执行多个样本点的FFT,采用非相干合并后的峰值搜索得到捕获结果,在不增加复杂度的条件下,避免了频偏对捕获性能的影响.通过对峰值信噪比(PSNR)理论公式的推导,证明了MS-FFT的频偏适应范围取决于采样率,随着数模转换器件采样能力的不断提升,具有比经典算法更大的频偏适应范围.最后,通过仿真验证了上述理论推导的正确性,证明了所提算法更加适合超高动态环境的应用场景.     

掺杂对CeO2结构及性能的影响研究进展

纳米CeO2具有比表面积大,储氧性能好,负载金属分散度高等许多优良特性,掺杂对CeO2的结构及性能又有进一步改善,因而是目前研究的热点。本文综述了掺杂对CeO2结构的影响,掺杂对CeO2在催化剂方面的应用研究,以及作为阳极材料的研究进展。展望了掺杂对改进CeO2性能的研究方向。     

Surface chemistry of nanoscale Fe_3O_4 dispersed in magnetic fluids

The interaction between stabilizers and nanoparticles is one of the important factors to prepare stable magnetic fluids. The magnetic nano-size Fe3O4 core with single domain and the average grain size around 8-12 nm were prepared by chemical precipitation method. The O/Fe molar ratio of the particle surface was measured by X-ray photoelectron spectroscopy (XPS). The heat effects of stabilizers ad- sorption on nanoparticles were measured by solution calorimetry. The excess amount of oxygen was possibly the result of the hydroxygen formed on the surface of the nanoparticles. The heat effects showed that compounds containing carboxyl groups can be adsorbed chemically on magnetite by forming chemical bonds. The other stabilizers involving NH-groups, such as polyethylene-imine, can be adsorbed physically. The exothermic value is about half of the former case.     

Correlation Analysis of the Runoff of the Rivers and the Seisms in China

In recent hundred years the annual discharge variations of the Changjiang River (represented by the Yichang station) and the Huanghe River (represented by Shanxian and Tangnaihe, respectively) have closely related to the geographical distribution of the earthquakes coming about in China in the same year, Both the occurrence of the destructive seism or seismic swarm in the river basins and the disappearance of the shocks in the east and south of the basins are the conditions that the Changjiang and Huanghe Rivers are the high flow while that the strong earthquake of magnitude 7 or more occurred in North China is the condition for the Changjiang low flow year and that of 6 or more in the Qilian Mountains area is for the Huanghe River. In the latter part of this paper, a 2-year sample is given to explain that the conditions of the 2 rivers being high flow years are that the north-south seismic belt is active and in the meanwhile no seism occurred in South China, and those of the low flow year are that the     

A New β-Carboline Alkaloid and a New Derivate of Isoferulic Acid from Anemone altaica

A new β-carboline alkaloid, 4-（9H-β-carbolin-1-yl）-4-oxobutyric acid and a new derivate of isoferulic acid, （E）-3-（3-hydroxy-4-methoxyphenyl）acrylic acid carboxymethyl ester, were isolated from the roots of Anemone altaica. Their structures were determined on the basis of spectral data.     

Study of Tea Digitized Chromatographic Fingerprint Spectra Using Micellar Electrokinetic Chromatography

IntroductionTeaisthemostwidelyconsumedbeverageinpeople’slife .Theheightenedpopularityofthisbeveragethroughouttheworldinrecentyearsmaybedueinparttotheevidenceofarelationshipbetweenteaconsumptionandpreventionofcertainformsofhumandisease .Themaincomponentsofteaarepolyphenoliccompounds ,commonlyknownascatechins ,whichrepresentagroupofcom poundsbelongingtotheflavonoidfamily .Thesecom poundsarewidelydistributedinthetealeavesandconsti tuteupto 30 %ofthedryleafweight.1Muchinteresthasbeenfocusedoncat…     

PHOTOSENSITIVITY OF Ce (Ⅳ) INITIATED METHYL ACRYLATE POLYMERIZATION

The influences of UV light irradiation (313 nm) and diffused daylight on the polymerization of methyl acrylate initiated by the ceric ammonium nitrate without any reducing agent have been studied both in aqueous nitric acid and in pure water. The rate of polymerization was found to be accelerated and the overall activation energy and the induction time were found to be decreased sharply by the UV light irradiation. Under UV light, the rate of polymerization is 8 times as high as the rate in dark. The rate of polymerization was found to attain a maximum with the increase of nitric acid concentration and the rate of polymerization became less sensitive to UV light in the presence of nitric acid whereas the induction period reduced outstandingly. Based on the experimental results, the mechanism is proposed.