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141.
Min‐Chieh Chuang Joshua Ray Windmiller Padmanabhan Santhosh Gabriela Valdés Ramírez Michal Galik Tzu‐Yang Chou Joseph Wang 《Electroanalysis》2010,22(21):2511-2518
This study examines the influence of textile substrates upon the behavior of wearable screen‐printed electrodes and demonstrates the attractive sensing properties of these sensors towards the detection of nitroaromatic explosives. Compared to electrodes printed on common cotton or polyester substrates, GORE‐TEX‐based electrochemical sensors display reproducible background cyclic voltammograms, reflecting the excellent water‐repellant properties of the GORE‐TEX fabric. The wetting properties of different printed textile electrodes are elucidated using contact angle measurements. The influence of laundry washing and mechanical stress is explored. The GORE‐TEX‐based printed electrodes exhibit favorable detection of 2,4‐dinitrotoluene (DNT) and 2,4,6‐trinitrotoluene (TNT) explosives, including rapid detection of DNT vapor. 相似文献
142.
Mass spectrometry (MS) is a powerful technique for protein identification in proteomic research. Two-dimensional gel electrophoresis (2-DE) combined with MS is a significant method for protein separation and identification. For protein identification, peptide sequencing is usually carried out by an effective but expensive nano-flow liquid chromatographic system combined to tandem mass spectrometry (MS/MS). However, protein identification based on such method is time-consuming, and contamination may occur as a result of column overloading. In this study, we establish an alternative nanoscale system for protein identification using MS/MS. The system consists of several devices that can be purchased from commercial sources and can be connected to an electrospray ionization quadrupole-time of flight (ESI-Q-TOF) MS in order to analyze proteins from 2D gels. This inexpensive strategy provides an attractive alternative method for rapid identification of proteins using a nanospray source. In addition, the device is disposable so that contamination is avoided. It is shown that peptide sequencing based on this device using ESI-Q-TOF MS is accomplished within 10 min. 相似文献
143.
144.
Tsai WH Chuang HY Chen HH Wu YW Cheng SH Huang TC 《Journal of chromatography. A》2010,1217(49):7812-7815
A simple sugaring-out assisted liquid-liquid extraction method combined with high-performance liquid-chromatography with fluorescence detection (HPLC-FL) was developed for the extraction and determination of sulfonamides in honey. Sample preparation consisted of acid hydrolysis to release sugar-bound sulfonamides. After derivatization with fluorescamine, the derivatives were partitioned into the organic layer under the honey (sugar)/water/acetonitrile system. The clear organic extract obtained by centrifugation could be injected into the HPLC system either directly or after dilution. Linearity was obtained with the coefficient of determination (R(2)) higher than 0.998 from 2 to 200 ng/mL. Under the optimal conditions, recoveries were determined for honey fortified at three levels (5, 20, and 100 ng/g) were 80.9-99.6% with coefficients of variation of 0.3-4.4%. Limits of detection for the sulfonamides studied were found to range from 0.6 to 0.9 ng/g. 相似文献
145.
Existing atomistic simulation techniques to study grain boundary motion are usually limited to either high velocities or temperatures and are difficult to compare to realistic experimental conditions. Here we introduce an adapted simulation method that can access boundary velocities in the experimental range and extract mobilities in the zero driving force limit at temperatures as low as ~0.2T(m) (T(m) is the melting point). The method reveals three mechanistic regimes of boundary mobility at zero net velocity depending on the system temperature. 相似文献
146.
147.
Volume polarization holographic recording in phenanthrenequinone-doped poly (methyl methacrylate) photopolymer is obtained. Photoinduced birefringence in a 2 mm thick sample is measured by a phase-modulated ellipsometry. The birefringence induced in this material by linearly polarized beam at 514 nm reaches 1.2×10(-5). In addition, ability for recording volume polarization grating using two different polarization configurations is demonstrated and compared. The experimental results show that the diffraction efficiency of the hologram reaches to ~40% by using two orthogonal circularly polarized beams. 相似文献
148.
In this paper, we consider a generalized model of the two friction models, both of which have two different types of control forces with time-delayed feedback proposed by Ashesh Sara et al. By taking the time delay as the bifurcation parameter, we discuss the local stability of the Hopf bifurcations. Under some condition, the generalized model harbors a phenomenon that the equilibrium may undergo finite switches from stability to instability to stability and finally become unstable. By applying the method introduced by Faria and Magalhaes, we compute the normal form on the center manifold to determine the direction and stability of the Hopf bifurcations. Numerical simulations are carried out and more than one periodic solutions may exist according to the bifurcation diagram given by BIFTOOL. Finally a brief conclusion is presented. 相似文献
149.
Trade credit financing plays a vital role in current business operations. Vendors extend payment dates to encourage sales, and buyers are not required to pay immediately after receiving products. This is equivalent to receiving a price reduction. Besides, buyers reduce their need for capital from bank loans. In addition, a number of defective products are produced during the production process. The number of defective items influences the on-hand inventory levels of buyers, service levels, and frequency of orders. To ensure that the analysis incorporates a realistic production environment, we developed an integrated inventory model with a two-part trade credit and considered an imperfect production process that can be improved by capital investment. The objective was to determine the optimal ordering, shipping, and quality improvement policies to maximize joint total profit. An iterative algorithm was established to determine the optimal strategy. Furthermore, a sensitivity analysis was conducted to examine the effects of changing parameter values on the optimal solution. 相似文献
150.
A novel variable-sized block encoding with threshold control for colour image quantization (CIQ) is presented in this paper.
In CIQ, the colour palette used has a great influence on the reconstructed image quality. Typically, a higher image quality
and a larger storage cost are obtained when a larger-sized palette is used in CIQ. To cut down the storage cost while preserving
quality of the reconstructed images, the threshold control policy for quadtree segmentation is used in this paper. Experimental
results show that the proposed method adaptively provides desired bit rates while having better image qualities comparing
to CIQ with the usage of multiple palettes of different sizes. 相似文献