Certification of the sulphur content of three rapeseed reference materials

Summary The sulphur content of three rapeseed reference materials has been certified on the basis of measurements made by inductively coupled plasma-optical emission spectroscopy, isotope-dilution mass spectrometry and ion chromatography. Their suitability for the calibration of x-ray fluorescence spectrometers used for measuring sulphur in rapeseed samples was established.     

Line Narrowing of a Tunable High Pressure CO2 Laser by Means of an Improved Non-Littrow Cavity

A model is reported to foresee ,for different mirror choices, the spectral properties of a high pressure, frequency tunable, CO₂ laser, operating with a non-Littrow grating mounting. The calculations show a larger frequency selectivity for not collimated plane cavities. The model is experimentally verified in a suitable high pressure laser. In particular narrowed linewidths less than 300MHz ( FWHM) are obtained.     

死髓变色前牙的激光漂白治疗临床评价

本文的研究目的是探讨激光冠内漂白治疗死髓牙变色的治疗作用。材料与方法 :漂白基本操作同激光活髓牙变色的漂白操作程序。先将牙龈及口唇有效防护 ,将漂白药物放在唇舌两面并同时封入根冠内。结果 :所有牙齿的灰暗变色均有 3- 5级的色度提高。平均治疗次数为 3.4± 0 .75 ,脱色 85 %以上的占 89%。结论 :牙齿创伤和牙髓分解是冠内变色的常见原因 ,激光冠内漂白是治疗这种变色的有效手段 ,可以完全恢复患者的自信。     

分离流动的脉冲热线测量方法研究与应用

1引言分离流动经常出现在许多实际流动中，对流体机械和飞行器产生重大影响。但由于这种流动具有方向性，变化快，给测量带来了困难。到目前为止，主要有以下三种测量方法：山激光多普勒测速治（＊D川；（2）飞行热线（F坊In含＊。卜w让e）；O）脉冲热线技术（PulsedAVire。‘脉冲热线”比“激光多普勒测速仪”价格低一个数量级，操作简单，是一种比较理想的测量技术。其原理最初由Baner山提出，随后经过BradburyP］，Eaton问，Castro＊和Fernholz问等人不断发展与完善，目前国外正推广应用在分离流动的研究中。但在国内，尚不多见其…     

具有非局部边界条件的奇摄动反应扩散问题

本文研究了一类具有非局部边界条件的奇摄动反应扩散初始边值问题．在适当的条件下，利用比较定理讨论了问题解的渐近性态．     

用激光散斑场检测药液内杂质含量分布

本文分析了利用散斑斑纹检测大输液药品杂质含量的机理，报道了检测大输液药品杂质的实例．     

Determination of mepiquatchloride in animal and plant matrices by ion chromatography with conductivity detection

Summary A new residue method, based on ion chromatography, for the determination of trace amounts of the ionic plant growth regulator mepiquatchloride is described. The method is adapted to plant and animal matrices and does not require any derivatization steps. This new technique provides higher recoveries of the analyte, better reproducibility and increased speed than the previous method. The limit of determination is 0.05 mg/kg.     

Millimeter wave beams diffracted from reflecting gratings

According to the angular-spectrum method, a radiation beam of an antenna horn in the Fresnal region is decomposed into the plane waves with the fast Fourier transform algorithm and the waves diffracted from a reflection grating are superposed as a diffracted beam. Compared with the reflected beam from the same size mirror, the radiation half width of the diffracted beam from a grating is narrower and its lateral shape is shift. These performances have been experimentally verified at Ka-band by: (1). The relative diffraction efficiencies in the first order with two triangular gratings which is put along propagating direction of a beam produced by a conical lens-horn. (2). H-plane lateral width with power—3dB lapsed of the focus beam from a grating and a mirror in a grating spectrometer for millimeter waves (25–100 GHz).     

苯对N,N-二甲基甲酰胺化合物~1H NMR的影响研究

本文研究了N,N-二甲基甲酰胺(DMF)在四氯化碳和苯混合溶剂中的~1H NMR。观察到N,N-二甲基甲酰胺(DMF)分子中两个甲基和混合溶剂中苯的共振吸收峰的化学位移随苯的摩尔分数增加而逐渐移向高场,而且两个甲基共振吸收峰向高场移动的程度不同,α甲基较β甲基为甚。DMF分子中两个甲基和混合溶剂中苯的化学位移可以用线性方程表示(δ=A+Bx),这里x是混合溶剂中苯的摩尔分数。相关系数R接近于-1。     

用于留数算术中的数值／留数／数值的转换

介绍用光学方法完成留数算术中的数值/留数/数值的转换,并附有实验结果。