The effect of micro-morphology of Bi2O3 on catalytic properties of Co/Bi catalyst for wet air oxidation of acetic acid

The novel phase transfer catalysts S-8 [4-(dimethyloctylammonium) propansultan] and DB-X [1,4-bis(triethylmethylammonium)benzene dibromide] were synthesized and employed for high conversion synthesis of dichlorocyclopropane from various olefins.This revised version was published online in December 2005 with corrections to the Cover Date.     

塔顶放大器在工程设计中的应用探讨

塔顶放大器在移动通信领域有较为广泛的应用，它通过降低(改善)等效接收噪声系数，从而提高上行接收灵敏度。本文将简要介绍塔顶放大器的应用和提高接收机灵敏度的计算。     

一种基于TV模型的自适应图像修复方法

图像修复是数字图像处理的重要内容，可用于被损坏的图像和视频修复、视频文字去除以及视频错误隐藏等。基于TV模型的修复方法有较好的恢复效果，但对参数的选取比较敏感，且运算量较大。本文提出了一种基于TV模型的自适应图像修复方法，与原方法相比可以有效提高该算法的稳健性，并能显著的减少运算时间。     

Synthesis of optically active 6-substituted 2-(aminomethyl)chromans

Three novel, optically active, 6-substituted 2-(aminomethyl)chromans were synthesized from readily available chroman 2-carboxylic acid precursors. These chroman-containing primary amines are useful building blocks for the synthesis of chroman-derived pharmaceutical agents.     

Determination of polymeric aluminum in soil extracted with a modified anion-exchange resin as a solid-phase adsorbent by ICP-AES.

In the present work, a new method was established by applying solid-phase extraction (SPE) to preconcentrate and separate polymeric aluminum (Al) and using ICP-AES to determine the polymeric Al, the total monomeric Al, and the total Al in soil extracts, respectively. A modified resin was prepared with impregnated 8-hydroxyquinoline-5-sulfoxinate (HQS) on the anion-exchange resin. It has good recognition ability for Al fractions, compared to the commonly used cation ion-exchange resin, which has a better ability to adsorb cations and a weak ability to recognize detailed Al species. The optimum conditions for Al fractionation sorption, elution and separation and the interference of foreign ions were studied with the prepared resin by continuous column and batch procedures. Monomeric Al was bound to Pyrocathecol Violet (PCV) at pH 6.2, whereas the polymeric Al species did not react with PCV for at least 15 min. Because a stable complex of Al-PCV was not absorbed on the HQS modified resin, the polymeric Al could be preconcentrated on-line by the HQS-modified resin. The adsorbed polymeric Al was eluted with 3 mL of 3 mol L(-1) of HCl, and then detected by ICP-AES. The method has been applied to directly determine polymeric Al in soil extracts with high selectivity as well as a high preconcentration factor. It gives a limit of detection of 0.6 ng mL(-1) with a relative standard deviation of less than 5.7% (n = 5, 0.24 microg mL(-1) Al).     

半自由声场的全息重建和预测实验研究

半自由声场环境下的声源重建和声场预测研究对声全息技术走向实际应用具有非常重要的意义.在提出基于分布源边界点法的半自由声场全息重建和预测方法的基础上，对此展开了实验研究.并将重建和预测的结果与常规方法重建和预测的结果进行了比较和讨论，说明了重建预测过程中反射声压的影响和考虑反射声压的必要性，证明了所提出方法在解决半自由声场环境下存在地面反射时的声源重建和声场预测时的有效性和准确性.还提出了采用奇异值截断滤波和Tikhonov正则化方法来削弱测量误差的影响，从而进一步优化了重建结果，提高了全息成像的可信度. 关键词： 声全息 半自由场 边界点 声辐射 反射声     

脂肪乳剂Intralipid代谢产物的高效液相色谱测定

本文介绍了利用ＨＰＬＣ色谱柱前衍生化技术简便，正确和灵敏地测定血清中游离脂肪酸的方法。在最佳条件下，一些脂肪酸的最低检知量为０．０４μｇ。方法已用于脂肪乳剂Ｉｎｔｒａｌｉｐｉｄ在诱发急性坏死性胰腺炎动物体内代谢产物测定。     

OSI参考模型与B—ISDN协议参考模型的比较

分析了ＯＳＩ参考模型和Ｂ－ＩＳＤＮ协议参考模型之间的关系，为Ｂ－ＩＳＤＮ与以ＯＳＩ为标准的数据网的互联打下了基础。     

非线性网络的混合域分析法

本文研究了对非线性网络进行混合域分析的谐波平衡法,它既可以改善计算精度,又可以提高速度,计算速度比全时域分析提高十倍以上,并且比全频域法要简单得多.它可以用来分析混频器、功率上变频器、振荡器等非线性电路.