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行波管在工作一段时间以后其电子枪各极间绝缘电阻可能发生变化,因此针对行波管的特点,设计出可靠的工作电源及行波管关断电路是保证武器装备可靠性的重要因素之一。在行波管电子枪极间绝缘电阻变小时,某应用系统行波管关断电路因不能使行波管完全关断,造成管体温度上升,保护电路动作,从而导致出现了雷达发射机无法及时开启的故障。文中通过对2种行波管关断方式等效电路的讨论,提出了避免应用系统故障的有效关断电路模式。 相似文献
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Thermo-responsive polymeric micelles of poly (ethylene glycol)-b-poly(2-hydroxyethyl methacrylate-g-lactide)-b-poly(N-isopropylacrylamide) (PEG-P(HEMA-PLA)-PNIPAM) with core–shell–corona structure were fabricated for applications in controlled drug release. The graft copolymer of PEG-P(HEMA-PLA)-PNIPAM was self-assembled into core–shell micelles with a densely PLA core and mixed PEG/PNIPAM shells at 25 °C in aqueous media. By increasing the temperature above the lower critical solution temperature of PNIPAM, these core–shell micelles could be converted into core–shell–corona micelles because of the collapse of PNIPAM block on the PLA core as the inner shell and the soluble PEG block stretching outside as the outer corona. Anticancer drug doxorubicin (DOX) was loaded in the polymeric micelles as a model drug. Compared with polymeric micelles formed by liner PEG-b-PLA-b-PNIPAM triblock copolymer, these polymeric micelles exhibited higher loading capacity, and release of DOX from the polymeric micelles with core–shell–corona structure was well-controlled. 相似文献
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制备了一种以三乙烯二胺(DABCO)为基础的离子液体;在水溶剂中,以该离子液体为催化剂催化三组分一锅法制备四氢苯并吡喃的反应,得到2-氨基-3-氰基-4-芳基-7,7-二甲基-5-氧代-4H-5,6,7,8-四氢苯并[b]吡喃;考察了反应时间、催化剂用量、催化剂加入时间、反应温度对反应收率的影响,确定了最优反应条件;由不同的芳香醛和活性亚甲基化合物制备了一系列四氢苯并吡喃衍生物,并讨论了可能的反应机理.结果表明,所选用的合成反应条件温和、时间短、收率高、后处理简单,且催化剂重复使用4次催化效果变化不大;就反应机理而言,所用催化剂具有双重催化活性. 相似文献
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Anguo Wu Tingting Duan Dan Tang Youhua Xu Liang Feng Zhaoguang Zheng Jiaxiao Zhu Rushang Wang Quan Zhu 《Chromatographia》2013,76(23-24):1649-1655
Nitrite and nitrate are main stable products of nitric oxide, a pivotal cellular signaling molecule, in biological fluids. Therefore, accurate measurement of the two ions is profoundly important. Nitrite is difficult to be determined for a larger number of interferences and unstable in the presence of oxygen. In this paper, a simple, cost-effective and accurate HPLC method for the determination of nitrite and nitrate was developed. On the basis of the reaction that nitrite is oxidized rapidly to nitrate with the addition of acidic potassium permanganate, the determination of nitrite and nitrate was achieved by the following strategy: each sample was injected twice for HPLC analysis, i.e. the first injection was to measure nitrate, and the second injection was to measure total nitrate including initial nitrate and the nitrate from the conversion of nitrite with the addition of acid potassium permanganate in the sample. The amount of nitrite can be calculated as difference between injections 2 and 1. The HPLC separation was performed on a reversed phase C18 column for 15 min. The mobile phase consisted of methanol–water (2:98 by volume); the water in the mobile phase contained 0.60 mM phosphate salt (potassium dihydrogen and disodium hydrogen phosphate) and 2.5 mM tetrabutylammonium perchlorate (TBAP). The UV wavelength was set at 210 nm. Additionally, we systemically investigated the effects of the concentration of phosphate salt and TBAP in the mobile phase, the pH of the mobile phase, and the amount of acidic potassium permanganate added to the sample on the separation efficacy. The results showed that the limits of detection (LOD) and the limit of quantitation (LOQ) were 0.075 and 0.25 μM for nitrate (containing the oxidized nitrite), respectively. The linear range was 1–800 μM. This developed approach was successfully applied to assay nitrite/nitrate levels in cell culture medium, cell lysate, rat plasma and urine. 相似文献
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普通彩电与I2C总线控制彩电的差异分析 总被引:3,自引:0,他引:3
从普通彩电与I^2C总线控制彩电在控制技术方面的差异角度,提出了检修I^2C总线控制彩电应具有的数字逻辑思维观念。 相似文献
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Tan Q Wang L Ma L Yu H Ding J Liu Q Xiao A Ren G 《The journal of physical chemistry. B》2008,112(35):11171-11176
A novel ferrocenyl anion receptor N, N, N, N-(dimethyl, ethyl, ferrocenecarboxylic amidodimethylene) ammonium fluoborate 2 with multiple binding sites was synthesized. Its anion recognition behaviors were investigated by CV, 1H NMR and UV-vis spectrum. It was found that the combination of two interactions enforced the anion binding ability and the binding selectivity of 2 to phosphate anion. The effects of scan rate on the CV curves of 2 with phosphate were also investigated. In different scan rate, the CV curves kept stable which indicated the strong binding between 2 and phosphate. According to relationships of peak potential, peak currents and scan rate of 2 binding with phosphate, the kinetic parameters of electrode process such as diffusion coefficient Dapp, surface transfer coefficient alphan alpha, and standard rate constant k0 were calculated. 相似文献
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Generalized Space Shift Keying (GSSK) modulation is a low-complexity spatial multiplexing technique for multiple-antenna wireless systems. However, effective transmit antenna combinations have to be preselected, and there exist redundant antenna combinations which are not used in GSSK. In this paper, a novel adaptive mapping scheme for GSSK modulation, named as Adaptive Mapping Generalized Space Shift Keying (AMGSSK), is presented. Compared with GSSK, the antenna combinations are updated adaptively according to the Channel State Information (CSI) in the proposed AMGSSK system, and the performance of average Symbol Error Rate (SER) is reduced considerably. In the proposed scheme, two algorithms for selecting the optimum antenna combinations are described. The SER performance of AMGSSK is analyzed theoretically, and validated by Monte Carlo simulation. It is shown that the proposed AMGSSK scheme has good performance in SER and spectral efficiency. 相似文献
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Qingquan Liu Li Wang Anguo Xiao Haojie Yu Qiaohua Tan Jianhua Ding Conglin Yu 《Macromolecular Symposia》2008,261(1):113-120
Summary: Monodisperse polystyrene (PS) microspheres with different sizes were prepared by dispersion polymerization in dispersion media of ethanol/water and isopropayl alcohol/water, respectively. The effect of polarity of the dispersion medium, stabilizer and initiator concentration on the average sizes and size range were evaluated. The results show that monodisperse PS microspheres with different sizes could be prepared in dispersion media of ethanol and isopropyl alcohol/water when appropriate initiator and stabilizer concentrations were employed, and the latter is a more appropriate medium to prepare uniform PS microspheres. It was found that the microsphere sizes reduced with increasing water content in the dispersion medium. Furthermore, in isopropyl alcohol/water dispersions, the average sizes decreased with increasing stabilizer concentration. 相似文献