三乙胺功能化聚乙二醇双子离子液体催化合成吡喃并[2,3-c]吡唑

合成了一种三乙胺功能化聚乙二醇双子离子液体,研究了其作为催化剂,在水相中以芳香醛、丙二腈、乙酰乙酸乙酯、水合肼或苯肼为原料的四组分一锅法反应,制备了16种不同取代基的吡喃并[2,3-c]吡唑化合物,产率为86%~94%.该离子液体稳定性高,可以方便的回收,重复使用5次,活性没有明显的下降.该方法具有反应条件温和,操作简单,产物易分离,对环境友好等优点.     

Isolation and identification of nondestructive desulfurization bacterium

A nondestructive desulfurization microorganism has been isolated. The metabolism product analyses show that the strain can be a kind of biocatalyst to oxidize dibenzothiophene (DBT) into 2-hydroxydiphenyl (HBP), therefore the sulfur in DBT is removed selectively. The 16SrRNA information, cell wall analysis, physical, biochemical properties and morphological properties suggest that the isolated strain is Rhodococcus erythropolis. The strain can grow in the basal salts medium (BSM) that DBT concentration is no more than 10 mmol/L, and the optimal DBT concentration for growth is 1 mmol/L, however, the optimal DBT concentration for desulfurization is 0.5 mmol/L. The further research shows that the strain can also desulfur some other or-ganosulfur-containing compounds such as thianaphthene, phenyl sulfide and 4,6-dimethyldiben-zothiophene (4,6-DMDBT).     

新型低温复合相变蓄冷材料的研制

根据凝固点降低理论自行研制出一种-10℃以下的低温相变材料.首先将筛选得到的有机醇、无机盐和水按照一定比例配制出低温相变材料,利用步冷曲线法找到合适的共晶点,利用DSC测试法得到其相变潜热,瞬态平面热源法得到热导率.最终得到相变温度为-14.8℃、相变潜热225.9 kJ/kg、导热率为0.57 W/(m·K)的低温相...     

2009上海国际音响格兰披治大奖获奖器材、品牌点评

最具性价比书架式扬声器;最具性价比落地式扬声器;最佳家庭影院扬声器;最经典扬声器;最佳扬声器;最受欢迎扬声器;最佳影音放大器;最受欢迎影音放大器     

An improved deep multiscale crowd counting network with perspective awareness

Crowd counting is a challenging task, which is partly due to the multiscale variation and perspective distortion of crowd images. To solve these problems, an improved deep multiscale crowd counting network with perspective awareness was proposed. This network contains two branches. One branch uses the improved ResNet50 network to extract multiscale features, and the other extracts perspective information using a perspective-aware network formed by fully convolutional networks. The proposed network structure improves the counting accuracy when the crowd scale changes, and reduce the influence of perspective distortion. To accommodate various crowd scenarios, data-driven approaches are used to fine-tune the trained convolutional neural networks (CNN) model of the target scenes. The extensive experiments on three public datasets demonstrate the validity and reliability of the proposed method.     

中小企业第三方数据存储与灾备服务需求研究

以我国中小型企业数据存储服务与灾备状况的调查为研究背景,结合国内外数据存储服务与灾备发展趋势和应用现状,从企业宕机成本、灾备投入、数据服务外包的促进与制约因素等多方面探讨了我国企业第三方数据存储与容灾备份服务的现实状况,通过分析灾备市场,提出第三方数据存储与灾备服务的未来发展建议。     

晶圆级芯片尺寸封装柔性焊点热循环可靠性

建立了晶圆级芯片尺寸封装(WLCSP)柔性无铅焊点三维有限元分析模型,基于该模型对柔性无铅焊点热循环等效应力应变进行了分析,并预测了焊点可靠性寿命。选取第一柔性层厚度、第二柔性层厚度、上焊盘直径和下焊盘直径作为关键因素,采用L16(45)正交设计了16种不同水平组合的柔性无铅焊点,获取了这些焊点的热循环等效应力数据,对等效应力数据进行了极差分析和方差分析。结果表明:在热循环加载条件下,采用柔性层结构方式能有效降低焊点内的等效应力应变;在置信度为90%的情况下,下焊盘直径和第一柔性层厚度对柔性焊点等效应力有显著影响。各因素对焊点等效应力的影响排序为下焊盘直径影响最大,其次是第一柔性层厚度,再次是第二柔性层厚度,最后是上焊盘直径。     

《网管员世界》“故障诊断”栏目征稿启事

为了能够给网管员朋友提供更加丰富的内容，现征集以下稿件：1．企业网络基础建设与维护中的遇到挫折及解决方法。     

对军工科研院所强化创新发展营造文化建设氛围的策略分析

本文分析了军工科研院所科技发展面临的状况，特别是如何激发军工科研所创新能力，梳理了提高全体员工工作积极性的基本思路，对如何调动全体员工做出创新性工作的基本内涵进行了系统性分析，提出了加强自身科技创新发展的几个重要解决方法。