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Due to the difficulty in synthesizing perhalogenated metallophthalocyanine, the method of ammonium molybdate solid phase catalysis was introduced, and by using tetrachlorophthalic anhydride and urea as the raw materials, hexadecachloro zinc phthalocyanine (ZnPcCl16) was synthesized. Components of the composite were analyzed by energy spectrum, and its functional group structures and absorption peaks were characterized by IR and UV-vis spectroscopy. The thin films of gas sensors were prepared in a vacuum evaporation system and evaporated onto SiO2 substrates, where sensing electrodes were made by MEMS micromachining. The optimal conditions for the films are: substrate temperature of 150 ℃ evaporation current of 95 A and film thickness of 50 nm. The result showed that the sensors were ideally sensitive to Cl2 gas and could detect the minimum concentration of 0.3 ppm. 相似文献
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在实用的认知无线电系统中,频谱感知技术必须具备在噪声电平高动态变化和无线信道严重衰落电磁背景下,进行实时盲频谱感知的能力,这为经典的频谱感知算法带来巨大的挑战。该文提出的功率谱分段对消频谱感知算法,依据傅里叶变换的渐进正态性和相互独立性,计算出功率谱的统计特性,利用监测频带内部分谱线强度和与全部谱线强度和的比值作为检验统计量进行信号存在性的判断。该文推导了算法的虚警概率和不同信道模型下正确检测概率的数学表达式,并依据Neyman-Pearson准则得到判决门限的闭式表达式。理论分析和仿真结果均表明:功率谱分段对消频谱感知算法对噪声不确定度具有鲁棒性;固定信噪比,算法的频谱感知性能不受噪声电平改变的影响;应用于高斯白噪声和平坦慢衰落信道中,可在较宽的信噪比范围内获得较优越的频谱感知性能;算法计算复杂度低,可在微秒级时长内完成频谱感知。 相似文献
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该文主要研究一种面向到达时间差(TDOA)被动定位的定位节点选择方法。首先,通过经典的闭式解析算法将TDOA非线性方程转化为伪线性方程,并使用位置误差的协方差矩阵来度量定位精度。其次,在可用节点数量给定的条件下,在数学上将定位节点选择问题转化为最小化位置误差协方差矩阵的迹这一非凸优化问题。然后,将非凸优化问题凸松弛并化为半正定规划问题,从而快速有效地求解出最优的定位节点组合。仿真结果表明,所提节点优选方法的性能非常接近穷尽搜索方法,而且克服了穷尽搜索方法运算复杂度高、时效性差的不足,从而验证了所提方法的有效性。
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