聚双(6-咔唑基己氧基)磷腈的合成

以PCl5和NH4Cl为原料采用"一步法"合成了线型聚二氯磷腈(4);4与6-咔唑基己醇发生亲核取代反应合成了聚双(6-咔唑基己氧基)磷腈(5),其结构经1H NMR,31P NMR,IR和GPC表征。热分析结果表明,5具有良好的热稳定性和较高的玻璃化温度。     

TFT—LCDs的缺陷检测和修补技术

概述了 TFT-LCDs 的缺陷分类、成因以及各种 TFT-LCDs 无缺陷技术,着重阐述了 TFT 矩阵板的一种电气缺陷检测原理和确定缺陷类型及位置的方法;介绍了各种缺陷的激光修补技术。     

荧光寿命成像显微的频域外差法测量及数据处理方法研究

介绍了一种实现荧光寿命成像显微的方法──频域外差法，研究并改进了相位调制度数据的逐点分析法，设计了相应的数据处理软件。通过对模拟数据的处理表明，该分析法具有很高的处理精度。     

Parallel optical coherence tomography using a CCD camera

Parallel optical coherence tomography is demonstrated using a 12-bit scientific-grade charge-coupled device array. A superluminescent diode in combination with a free-space Michelson interferometer was employed to achieve 10-μm axial resolution and 1.1-μm transverse resolution on a 902×575 /μm2 field of view. We imaged a test mirror and bovine retinal tissue using a four-step phase shift method.     

取样成像扫描式分幅技术

 介绍了用于惯性约束聚变（ICF）等离子体诊断的取样成像扫描分幅技术的原理,分析了该分幅技术的有关特性参数,如曝光时间、画幅数目、空间分辨率等。借助于特别设计的扫描变像管进行了该技术的原理性实验,并利用计算机数字图像处理技术进行图像的重构。实验获得了持续时间约100ps的发光过程的16幅图像,曝光时间优于6.3ps,阴极上空间分辨率为3.5 lp/mm。     

Trichromatic phase manipulation of the response of a two-level medium to an arbitrarily intense probe field

The phase dependence and independence of the response of a trichromatically driven two-level medium to an arbitrarily intense probe field have been studied. The sum of the relative phases of the sideband components of the trichromatic field compared to the central component plays a crucial role in the response of the medium. For a weak probe field, as the sum of the relative phases changes from The phase dependence and independence of the response of a trichromatieally driven two-level medium to an arbitrarily intense probe field have been studied. The sum of the relative phases of the sideband components of the trichromatic field compared to the central component plays a crucial role in the response of the medium. For a weak probe field, as the sum of the relative phases changes from 0 to π, multiple switching can be achieved, in which switching from normal to anomalous dispersion occurs in multiple separate frequency regimes. The remarkable dependence on the sum phase is also shown for a strong probe field. On the other hand, when the sum of the two relative phases is fixed, the changes in the respective phases have no influence on the response of the medium.     

葛根素-7-磷酸二乙酯的NMR研究

葛根素是从常用中药野葛根中分离提取出来的一种具有很强生物活性的异黄酮碳苷类化合物,设计并合成了一种新的化合物葛根素-7-磷酸二乙酯. 在常温下,这种新的化合物在NMR谱上有两组相关的信号峰,即在溶液中以两种不同的构象存在. 本文利用HSQC和HMBC等多种二维核磁共振技术对这种化合物的NMR谱进行了全归属.     

Comparative Investigation of QHS and DQHS with Density Functional Theory

1 INTRODUCTION QHS (C15H22O5) is a novel antimalarial drug isolated from Chinese herb Artemisia annua L in 1972. Structural studies by chemical analysis, X-ray single-crystal diffraction and other spectroscopic me- thods showed that QHS is a sesquiterpene lactone with a peroxide group (Fig. 1)[1]. In the past few decades, great achievements have been acquired in search for the mechanism of action of QHS[2～5]. Its unique endoperoxy bridge has attracted worldwide attention. Due to …     

GSUF-10-Ⅰ型UHF电视发射机的维护

1 发射机工作原理及维护 1.1 中频调制器 1.1.1 工作原理 中频调制是将来自电视中心的视频、音频信号分别调制在中频图像载频38 MHz和伴音载频31.50 MHz上,输出额定电平的已调图像中频信号和已调伴音中频信号,它们输出的标准电平为图像中频0 dBm,图像与伴音中频输出电平差为10 dB.调制器由6块印制板组成,分别叙述如下.