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The ternary hybrid films consisting of chitosan(CS),polyethylene glycol(PEG)and nano-sized silica which was surface-modified by amino groups(RNSA)were prepared.The structures of the blend membranes were characterized by attenuation total reflection-infrared spectroscopy(ATR-IR),X-ray diffraction(XRD),optical microscopy(OM)and differential scanning calorimetry(DSC).The results showed that the addition of silica affected not only the distribution and crystallinity of PEG on the sample surface,but also the ... 相似文献
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Effect of initial chirp on near-infrared supercontinuum generation by a nanosecond pulse in a nonlinear fiber amplifier
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Theoretical and experimental research on the effect of initial chirp on near-infrared supercontinuum generation by a nanosecond pulse in a nonlinear fiber amplifier is carded out. The complex Ginzburg-Landau equation is used to simulate the propagation of the pulse in the fiber amplifier and the results show that pulses with negative initial chirp produce the widest supercontinuum and pulses with positive initial chirp produce the narrowest supercontinuum when the central wavelength of the pump lies in the normal dispersion region of the gain fiber. A self-made line width narrowing system is utilized to control the initial chirp of the nanosecond pump pulse and a four-stage master oscillator power amplifier configuration is adopted to produce a high power near-infrared suppercontinuum. The experimental results are in good agreement with simulations which can provide some guidance on further optimization of the system in future work. 相似文献
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Thin films of incompatible polymer blends can form a variety of structures during preparation and subsequent annealing process. For the polymer blend system consisting of polystyrene and poIy(styrene-co-p-bromo-styrene), i.e., PS/PBrxS, its compatibility could be adjusted by varying the degree of bromination and the molecular weight of both components comprised, in this paper, surface chemical compositions of the cast and the annealing films were investigated by X-ray photoelectron spectroscopy (XPS) and contact angle measurement; meanwhile, surface topographical changes are followed by atomic force microscopy (AFM). In addition, substantial attention was paid to the effect of annealing on the morphologic variations induced by phase separation and/or dewetting of the thin film. Moreover, the influences of the molecular weight, Aw, as well as the brominated degree, x%, on the sample surface are explored systematically, and the corresponding observations are explained in virtue of the Flory-Huggins theory, along with the dewetting of the polymer thin film. 相似文献
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结合某雷达信号处理系统硬件平台,介绍了雷达信号处理硬件平台的结构和组成, 以及算法实现方案,给出了参差 MTI 中的 AMTI 滤波器在单杂波和多杂波情况下,实现对杂波抑制的方法,并重点介绍了系统中通讯控制器的软件设计及功能实现,最后通过硬件的平台搭建和硬件程序的调试,实现了参差 MTI 中的 AMTI 滤波器对单杂波和多杂波的抑制功能。 相似文献
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原子力显微镜与透射电镜对比研究嵌段共聚物微相分离形态 总被引:3,自引:0,他引:3
嵌段共聚物微观相分离形态结构由于其理论与应用中的重要性一直是人们研究的热点 [1] .本文研究的聚苯乙烯 -聚乙烯 /聚丁烯 -聚苯乙烯三嵌段共聚物 (SEBS)为聚苯乙烯 -聚丁二烯 -聚苯乙烯 (SBS)饱和加氢后的产物 .由于中间嵌段中的双键大多已加氢饱和 ,过去一直没有合适的染色剂进行染色 ,所以在 2 0世纪 80年代中期以前 ,SEBS形态结构未见文献报道 [1] .近年来 ,由于新型染色剂 Ru O4 的应用 ,使得用透射电镜 (TEM)观察其微相分离形态成为可能 . 随着对嵌段共聚物形态结构认识程度深入 ,人们迫切希望能有新的手段提供更加丰富的… 相似文献
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基于半导体可饱和吸收镜和光纤光栅实现了稳定的2 m波段被动调Q光纤脉冲激光器,输出激光的中心波长为1958.2 nm。随着泵浦功率的增加,输出脉冲的重复频率不断增加,而对应脉冲的宽度不断减小。输出脉冲重复频率的变化范围为20~80 kHz,脉冲宽度的变化范围为490 ns~1 s。当泵浦功率为1.3 W时,调Q光纤激光器的最大平均输出功率为91 mW,脉冲重复频率为80 kHz,脉冲宽度为490 ns,对应的最大单脉冲能量约为1.14 J。 相似文献
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