一种快速抽提微量成分的热逆流提取装置

液固萃取在化学实验及研究中常常遇到,索氏提取器是液团萃取普遍采用的装置,它具有简单、提取率高等特点,但采用索氏提取器从较大体积的固体样品中提取微量成分是很困难的。对于要求在较高温度下进行液固萃取也难于实现。为此我们设计了一种热逆流提取器,它不仅可满足上述要求,而且使萃取过程连续化。该装置主要由单口烧瓶、三颈烧瓶和热逆流提取器组成(图1)。     

X射线荧光光谱铝环-双层压片法测定土壤中常量和微量元素

本文提出用铝环-双层压片法制片,经验系数法校正吸收-增强效应,对少量土壤样品中的常量和微量元素进行了定量测定。取样量为500 mg,制样与测量精确度好于5%,用本法对标样的分析表明,分析值与推荐值基本一致,本法具有简单、快速、成本低的特点,适用于少量样品的分析。     

光梯度力与激光捕获

从电偶极子在非均匀电磁场中所受梯度力出发,用光的电磁理论和电解质小球的电偶极子模型,论述了介质小球在光场中所受光梯度力与光强梯度成正比,并以此来定量说明激光对介质小球的捕获原理.     

基于UPE-SVM模型的脊髓损伤康复方案决策算法

脊髓损伤患者康复治疗方案一般是由医生根据患者功能评估结果人工制定的,康复治疗方案决策存在效率低下、标准不一以及病例数据集样本类别不平衡等问题。本文提出了一种用于脊髓损伤智能康复治疗方案决策的UPE-SVM推理模型,并基于124例脊髓损伤病例建立了用于模型训练与验证的病例数据集。应用训练好的UPE-SVM模型,推理出对应患者病症特征的初始治疗方案,供治疗师参考修正出最终治疗方案,并更新到病例数据集。使用更新后的新病例数据集,继续在线训练UPE-SVM模型,提高UPE-SVM模型的学习能力和泛化能力。经测试集验证,此决策算法的AUC指标为0.85,F₁-score为0.80,精确率为80%,召回率为85%,有效克服了数据集的样本类别不平衡问题,提高了智能康复治疗处方的决策准确率。     

ZnO缓冲层对Mg0.3Zn0.7O紫外探测器的影响

利用溶胶-凝胶法制备了Mg0.3Zn0.7O薄膜,并制作了金属-半导体-金属结构的深紫外探测器.研究了高质量ZnO缓冲层的引入对Mg0.3Zn0.7O薄膜的吸收谱和结晶特性以及Mg0.3Zn0.7O紫外探测器响应参数的影响.实验结果表明:ZnO缓冲层的引入使Mg0.3Zn0.7O薄膜的紫外-可见光吸收谱有轻微的红移,但可以明显提高薄膜的结晶质量,同时ZnO/Mg0.3Zn0.7O探测器的I-V特性表明,ZnO缓冲层的引入可以显著提高器件的光电流,改善其响应特性,在20V偏压下将Mg0.3Zn0.7O探测器的响应度由0.035 A/W提高至0.63 A/W.     

具有负反馈的分段曲率校正CMOS带隙基准源

提出了一种新型带有负反馈的分段曲率校正带隙电压基准源,该基准源的主要特色是利用温度相关的电阻比技术获得一个分段曲率校正电流,校正了一阶带隙基准源的非线性温度特性. 该分段线性电流产生电路还形成了一个负反馈,以改善带隙基准源的电源抑制和线性调整率. 测试结果表明：在2.6V电源电压下,该基准源在没有采用校正的条件下,在-50~125℃温度范围内实现了最大21.2ppm/℃温度系数,电源抑制比为-60dB. 在2.6~5.6V电源电压下的线性调整率为0.8mV/V. 采用中芯国际（SMIC) 0.35μm 5V n阱数字CMOS工艺成功实现,有效芯片面积0.04mm2,其总功耗为0.18mW. 该基准源应用于3, 5V兼容的光纤接收跨阻放大器.     

集成电路设计方法及IP设计技术的研究

文章就主要针对集成电路的设计方法和IP设计技术进行研究,希望对相关领域研究提供帮助.     

Water-based processed and alkoxide-based processed indium oxide thin-film transistors at different annealing temperatures

In this study,indium oxide(In_2O_3) thin-film transistors(TFTs) are fabricated by two kinds of low temperature solution-processed technologies(Ta ≤ 300?C),i.e.,water-based(DIW-based) process and alkoxide-based(2-ME-based)process.The thickness values,crystallization properties,chemical structures,surface roughness values,and optical properties of In_2O_3 thin-films and the electrical characteristics of In_2O_3 TFTs are studied at different annealing temperatures.Thermal annealing at higher temperature leads to an increase in the saturation mobility(μsat) and a negative shift in the threshold voltage(VTH).The DIW-based processed In_2O_3-TFT annealed at 300?C exhibits excellent device performance,and one annealed at 200?C exhibits an acceptable μsat of 0.86 cm~2/V·s comparable to that of a-Si:H TFTs,whereas the 2-ME-based TFT annealed at 300?C exhibits an abundant μsat of 1.65 cm~2/Vs and one annealed at 200?C is inactive.The results are attributed to the fact that the DIW-based process induces a higher degree of oxidation and less defect states than the 2-ME-based process at the same temperature.The DIW-based process for fabricating the In_2O_3 TFT opens the way for the development of nontoxic,low-cost,and low-temperature oxide electronics.     

Microwave Assistant Synthesis and Dimeric Crystal Structure of 2-(((6-Chloropyridin-3-yl)-methyl)thio)-5-(pyridin-4-yl)-1,3,4-thiadiazole

The title compound 2-(((6-chloropyridin-3-yl)methyl)thio)-5-(pyridin-4-yl)-1,3,4-thiadiazole 5(C26H18Cl2N8S4) was synthesized, and its structure was confirmed by 1H NMR, MS and elemental analyses and X-ray diffraction. It crystallizes in the triclinic system, space group P1 with a = 9.452(4), b = 12.335(4), c = 13.017(5) A, α = 90.624(5), β = 110.541(5), γ =104.879(4)°, Dc = 1.561 g/cm3, Z = 2, V = 1364.9(9) A3, F(000) = 656, the final R = 0.0300 and w R = 0.0635 for 4206 observed reflections with I 2σ(I). The preliminary biological test showed that the title compound has activities against Stemphylium lycopersici(Enjoji) Yamamoto, Fusarium oxysporum. sp. cucumebrium, and Botrytis cinerea with inhibitory activities to be 9.82%, 44.44% and 20.00%, respectively.     

过模弯曲圆波导模式耦合设计

基于耦合波理论,波导轴线采用常规圆弧弯曲和改进的正弦弯曲结构,对TE01—TM11模式变换器进行全面优化分析,计算中考虑了多模、反向波、金属壁所带来的欧姆损耗以及相位重匹配等因素.以正弦弯曲设计的Ka波段TE01—TM11模式变换器的转换效率达到99%,带宽超过32%,并得出常弯曲结构中波导半径、波导曲率、变换器长度和转换效率之间的关系.