Crystal Structure of Methyl 3- (2-chlorophenyl )-3- (5, 5-dimethyl-3-hydroxy-2-cyclohexene- 1-one-2-yl) propionate

1INTRODUCTIONInorganicsolidsupportsascatalystshavebeenwellstudied,becauseoftheirap-plicationsinorganicsynthese('~".Recently,wehavereportedtheKnoevenagelcon-densationcatalysedbyKF-Al,O,['i.Inthispaper,wediscussedthecrystalstruc-tureofthetitlecomPoundsynthesizedbythereactionof2-chlorobenzaldehydey5,5-dimethyl-1,3-cyclohexanedioneandisopropylidenemalonateinmethanolcatalyzedbyKF-Alzo,'Inordertoconfirmthestructureofthetitlecompound,theX-raycrys-tallOgraphicstudywascarriedout.2EXPER1MEN…     

不允许卖空证券组合选择的有效子集

证券组合选择的有效子集是指它可取代原有的基本证券集来生成Markowits有效组合前沿.本文给出一个证券集的子集在不允许卖空的条件下是全集的有效子集的充要条件。     

逐步增加的Ⅱ型截尾下系统可靠性的Bayes分析及寿命预测

在逐步增加的型截尾模型下,研究部件寿命服从双参数指数分布的冷贮备串联系统可靠性指标的Bayes估计及单样本场合未来观测值的预测问题.在两个参数均未知的情形下,分别在平方损失(SE)、LINEX损失和熵(General Entropy,GE)损失函数下给出两个参数及可靠性指标的Bayes估计,对于超参数的确定,给出一种新的方法;并讨论了单样本场合未来观测值的预测问题,给出预测分布及预测区间;最后利用随机模拟方法进行比较,并对结果进行了讨论.     

Phase Dependence of Fluorescence Spectrum of a Two-Level Atom in a Trichromatic Field

We examine the phase-dependent effects in resonance fluorescence of a two-level atom driven by a trichromatic modulated field. It is shown that the fluorescence spectrum depends crucially on the sum of relative phases of the sideband components compared to the central component, not simply on the respective phases. The appearance or disappearance of the central peak and the selective elimination of the sideband peaks are achieved simply by varying the sum phase. Once the sum phase is fixed, the spectrum keeps its features unchanged regardless of the respective relative phases.     

A Novel Cholesterol Oxidase Biosensor Based on Pt-nanoparticle /Carbon Nanotube Modified Electrode

A variety of electrochemical biosensors for cholesterol detection have been proposed because of its importance in clinic and food analysis 1-2. Classical devices for the detection were based on monitoring either the consumption of oxygen or the production of H2O2. The amperometric determination of H2O2 oxidation is sensitive and stable, but it requires a high anodic potential (over 0.6 V vs Ag/AgCl) and is affected by co-oxidable substances such as ascorbic acid and uric acid usually presen…     

Timoshenko梁的耗散边界反馈控制

研究Timoshenko梁的非线性耗散边界反馈镇定.首先利用非线性半群理论证明闭环系统的适定性.然后利用LaSalle不变原理证明梁的振动在所建议的非线性控制作用下随时间渐近趋于0.进而对控制的非线性作进一步的限制,利用能量摄动方法得到梁的闭环振动指数稳定.     

服务台可修的GI／M（M／PH）／1排队系统

本文首次讨论一个到达间隔为一般分布的可修排队系统。假定服务时间、忙期服务台寿命都服从指疏分布，修复时间是ＰＨ变量。首先证明该系统可转化为一个经典的ＧＩ／￣ＰＨ／１排队模型，然后给出系统在稳态下的各种排队论指标和可靠性指标。     

锥有效拟凹集的有效点集的连通性

本文引进了锥有效拟凹集的概念，讨论了R ^m-严格拟凹与R ^m－有效拟凹的关系，证明了一个紧集为锥有效拟凹且其有效点集为闭集时，这个有效点集是连通的。     

Lagrange、Cauchy、积分中值定理与Taylor公式的统一证明

通过一个定理的结论,给出L agrange、C auchy、积分中值定理和T ay lor公式的统一证明,同时得出计算不定型极限的L′Hosp ita l法则的推广定理.     

反应挤出接枝共聚反应表观链增长常数的测量

以预辐照的LLDPE反应挤出接枝MAA作为研究对象，通过在双螺杆挤出机中的不同部位取样，用FFIR分析接枝物及均聚物的产量，并用ESR测试链增长自由基浓度，设计了测定接枝和均聚反应初始阶段的表观链增长常数的方法,结果表明，在本实验测试范围内表观接枝链增长常数不同于均聚链增长常数；所得的测量值符合理论预测值，证明测试方法适合高温熔融体系的研究。