非晶钛酸铋的晶化过程

利用差热分析、X射线衍射和透射电子显微镜等技术对溶胶-凝胶法合成的凝胶的晶化过程进行了分析，实验结果表明，Bi₄Ti₃O₁₂非晶凝胶晶化过程经历了四个过程：首先在433℃先形成了Bi₂O₃和TiO₂亚稳相，然后在488℃时TiO₂亚稳相与Bi₂O₃反应形成Bi，Ti复合氧化物亚稳相Bi₂T 关键词： 钛酸铋 铁电材料 溶胶凝胶 非晶 晶化过程     

Pressure dependence of the thermal stability in LiMn2O4

Structural stability in terms of the decomposition temperature in LiMn₂O₄ was systematically investigated by a series of high-temperature and high-pressure experiments.LiMn₂O₄ was found to have structural stability up to 5 GPa at room temperature.Under ambient pressure,the compound decomposed at 1300℃.The decomposition temperature decreased with increasing pressure,yielding more complex decomposed products.Below the decomposition temperature,the crystal structure of LiMn₂O₄ varied with pressure.The presented results in this study offer new insights into the thermal and pressure stability of LiMn₂O₄ materials as a cathode for lithium-ion batteries that can operate under extreme conditions.Therefore,these findings may serve as a useful guide for future work for improving lithium-ion batteries.     

一种高分辨率的光纤光栅传感解调技术

报道了一种基于光纤激光器波长扫描寻址的高分辨率的光纤光栅传感解调方案。光纤激光器的扫描寻址过程由微机来控制。微机控制光纤激光器波长扫描的同时,同步采集、处理传感信号,并通过曲线拟合给出传感光栅的中心反射波长值。本解调方案的波长移动分辨率为０．１ｐｍ,可以实现高分辨率的温度及应变测量。     

实现20Gbit/s的OTDM孤子信号56km色散位移光纤的传输

在国内最先采用孤子的方式将8×2.5Gb/s的OTDM信号在色散位移光纤中传输了56.1km,对8×2.5Gb/s的OTDM进行解复用后进行了误码测量,系统功率代价为2.9dB.系统采用增益开关半导体激光器作光孤子源,高Q电滤波方式提取时钟,非线性光学环路镜解复用。孤子脉冲最大半宽度为20ps,传输光纤平均色散1.2ps/nm/km。     

牛顿环实验测量结果的不确定度评定及其表示

讨论了不等精度测量牛顿环曲率半径及牛顿环直径不确定度的评定及表示     

Notable shift of ultraviolet intensity on Sn-doped ZnO nanostructure fabricated by sol–gel method

Sn-doped ZnO (SZO) thin films are deposited by sol–gel dip-coating method with Sn content at 0 at.% and 1–15 at.% with an increment of 2 at.%. The structure and luminescence of the films are investigated. X-ray diffraction results indicate that all the SZO samples show preferential orientation along the (002) direction, and the scanning electron microscope exhibits that the surface morphology of the films change from nanoparticles to nanorods with increasing Sn concentration. X-ray photoelectron spectroscopy reveals that Sn exists as valence of +4 in the matrix. The photoluminescence peaks at 381 and 398 nm are observed in all the samples. The ratio of intensity of peak at 381 nm to that of peak at 398 nm differed markedly. The intensity of peak at 398 nm might be due to the response for the Sn atoms, while the intensity of peak at 381 nm is probably related to the quantum size effect.     

The intersection marker method for 3D interface tracking of deformable surfaces in finite volumes

Currently, the majority of computational fluid dynamics (CFD) codes use the finite volume method to spatially discretise the computational domain, sometimes as an array of cubic control volumes. The Finite volume method works well with single‐phase flow simulations, but two‐phase flow simulations are more challenging because of the need to track the surface interface traversing and deforming within the 3D grid. Surface area and volume fraction details of each interface cell must be accurately accounted for, in order to calculate for the momentum exchange and rates of heat and mass transfer across the interface. To attain a higher accuracy in two‐phase flow CFD calculations, the intersection marker (ISM) method is developed. The ISM method is a hybrid Lagrangian–Eulerian front‐tracking algorithm that can model an arbitrary 3D surface within an array of cubic control volumes. The ISM method has a cell‐by‐cell remeshing capability that is volume conservative and is suitable for the tracking of complex interface deformation in transient two‐phase CFD simulations. Copyright © 2015 John Wiley & Sons, Ltd.     

非低温法的稀有气体纯化技术概述

稀有气体广泛应用于工业生产中,如离子刻蚀、检漏等。但是它们在地球上的含量比较少,属于稀有资源,因此需要对它们进行纯化以循环再利用。首先介绍了不同气体纯化的原理,然后以实际生产中的不同稀有气体使用范围为例,说明纯化装置的设计方法和需要考虑的问题。为以后气体纯化装置的设计提供借鉴。