Intramolecular Crosslinking of Polyvinylidene Fluoride by Homogeneous Solution Irradiation

High Energy Chemistry - Intramolecular crosslinking of polyvinylidene fluoride (PVDF) was observed to have occurred when the PVDF homogeneous solution was subject to γ-ray irradiation, which...     

Quantum Watermark Algorithm Based on Maximum Pixel Difference and Tent Map

International Journal of Theoretical Physics - A new quantum watermark algorithm is presented by combining maximum pixel difference partitioning with the least significant bit substitution...     

利用ICP-AES中钙的主次灵敏线同时测定各种盐湖卤水中的钙

等离子发射光谱（ICP-AES）已广泛应用于医学,地质,水质,环境等领域的检测。本文利用钙的主、次灵敏线同时测定盐湖卤水及盐水中各种不同含量的钙,其加标回收率在94.0%—100.8%范围内,与经典的容量法对比,数据能满足要求,样品浓度小于100mg/L时用灵敏线Ca317.9nm测定,样品浓度大于100mg/L时用次灵敏线Ca210.3nm测定。此法快速、准确,结果令人满意。     

Ruthenium nanoclusters anchored on cobalt phosphide hollow microspheres by green phosphating process for full water splitting in acidic electrolyte

Transition metal phosphide(TMP) based electrocatalysts possessing special crystal and electronic structures attract broad attention in the field of electrocatalysis.Immense effort is made to optimize TMP catalysts aiming to satisfy the electrochemical catalysis performance.In this work,an environmentally friendly in situ green phosphating strategy and spatial limiting effect of the RuCo precursor is employed to fabricate the ruthenium nanoclusters anchored on cobalt phosphide hollow microspheres(Ru NCs/Co₂P HMs).The obtained Ru NCs/Co₂P HMs electrocatalysts exhibit high hydrogen evolution reaction(HER) activity at wide pH ranges,which require an overpotential of 77 mV to achieve the current density of 10 mA/cm² in 0.5 mol/L H₂SO₄ and 118 mV in 1.0 mol/L KOH.Besides,the multifunctional Ru NCs/Co₂P HMs exhibit good oxygen evolution reaction(OER) activity with an overpotential of 197 mV to reach the current density of 10 mA/cm² in 0.5 mol/L H₂SO₄,which is below that of the commercial RuO₂ electrocatalyst(248 mV).A two-electrode electrolyzer is assembled as well,in acid electrolyte,it achieves a current density of 10 mA/cm² at a voltage of 1.53 V,which is superior to that of the benchmark of precious metal-based electrolyzer(1.58 V).     

对数似然图像分割的快速主动轮廓跟踪算法

针对跟踪目标尺度变化问题,提出了基于灰度对数似然图像分割的快速主动轮廓跟踪算法。改进的主动轮廓跟踪算法将根据以目标与背景的颜色差异而建立的对数似然图对图像进行阈值分割和数学形态学处理,再将Kalman滤波器结合到主动轮廓跟踪算法进行目标跟踪。改进的主动轮廓跟踪算法对目标分割准确,轮廓特征显著,跟踪效果稳定,算法能很好地适应跟踪目标尺度变化。通过Kalman滤波器对目标位置点的预测减少了主动轮廓跟踪算法收敛的迭代次数,使算法的运算效率提高了33%左右。     

基于内置电光晶体F P标准具的扫描滤波方法

基于内置电光晶体的F-P标准具,利用F-P多光束干涉原理和晶体的线性电光效应,提出了一种能有效提高啁啾脉冲信噪比的扫描滤波方法。给出了电光晶体加载电压的时变函数表达式,分析了影响信噪比提升效果的主要因素,并重点讨论了电光晶体的电压控制参数对信噪比提升效果和滤波器透过率的影响。研究结果表明,利用该扫描滤波方法可将啁啾脉冲激光信噪比提升约2个量级。     

±100 kV三电极场畸变气体火花开关

设计了一种用于直线变压器驱动源的三电极场畸变气体火花开关。开关采用SF6气体绝缘,开关尺寸和电感较小,实测开关电感约为67 nH。在工作电压80 kV、工作系数为70%时,开关触发时延为40.0 ns,抖动约2.8 ns。对比研究了钨铜合金和黄铜两种电极材料对开关静态和触发击穿特性的影响,研究结果表明：铜钨合金电极开关的自击穿电压分散性、触发时延及抖动、自放电概率和电极表面烧蚀均小于黄铜电极,更适宜作为三电极场畸变开关的电极材料。     

强光一号POS等离子体源性能参数测量

以强光一号等离子体源（电缆枪）为研究对象,采用电荷收集器（法拉第杯）对强光一号等离子体源性能参数进行测量。实验结果表明：等离子体发射密度与电缆等离子体枪枪芯到枪口的距离正相关,而发射速度与电缆等离子体枪枪芯到枪口的距离负相关;增大电缆枪驱动电压时,等离子体发射密度增速远小于驱动电流增速。重复性研究表明,对由数十支电缆枪组成的等离子体源而言,单支电缆枪放电分散性对其输出等离子体整体分布均匀性影响不大。不确定度分析表明,通过多次重复实验求平均值,可以有效减小实验结果的不确定度,发射密度测量结果的合成标准不确定度在10%以内。     

多间隙气体开关电感

介绍了一种用于快脉冲直线变压器的低电感多间隙气体开关。专门构造了多种形式的单通道放电实验,测量了在不同形态单通道放电时的开关电感,研究发现:单通道放电时开关电感除了受到角向电流的影响,还与电弧通道引起的放电回路面积变化有关,开关电感理论计算值与单通道放电时的实测结果最接近;开关在自放电和触发时,均形成了多通道放电,电感明显降低,触发时开关电感最小约为49 nH,电极角向电流的影响可以忽略。