FAR-INFRARED AND INFRARED REFLECTIONS OF Tl2Ba2Ca2Cu3O10 FILM

The far-infrared and infrared reflection spectra of Tl₂Ba₂Ca₂Cu₃O₁₀ superconducting film are reported in this paper. It is found there are three sharp reflection edges in both the superconducting and normal states, their positions being near ≈ 150, ≈ 350 and ≈600 cm^-1. We attribute these reflection spectra to the Drude free carriers and a wide mid-infrared absorption band. When the incident angle increases from 7° to 30°, some additional stractures appear in the refiection spectra, which are the A_2u phonon modes vibrating along c-axis.     

剑桥中学证书国际物理实验考试介绍

介绍了剑桥大学地方考试联合会制定的普通水平学校证书国际考虑大纲对高中学生物理实验技能的要求。分析了剑桥国际物理实验考试和实验试题的特点。     

等离子体噻吩聚合膜的研究及I+注入的掺杂效应

以噻吩为单体,在等离子体环境中聚合成致密的有机膜。利用Rutherford背散射(RB2S)和质子弹性反冲(ERD)、傅里叶红外谱(FTIR)测定了膜的成分和结构;从近红外-可见-紫外光的反射和透射谱,运用传递矩阵方法研究了膜的光学性质;此外,还探讨了24keV的I⁺离子束的注入对等离子体噻吩聚合膜的掺杂效应。结果表明,注入层内电荷载流子的输运机理可用Mott的可变自由程跳跃(VRH)理论给以解释。 关键词：     

Kinetic Studies of Electrochemical Oxidation of 1,3-Benzenedithiol

The electrochemical oxidation of 1, 3-benzenedithiol was investigated in a 0. 100 mol/L tetrabutylammonium perchlorate/acetonitrile electrolyte. The electrochemical techniques used were potential sweep, bulk electrolysis, rotating disc and the potential step method. The combination of the techniques yielded the number of electrons transferred per molecule, the reaction order, the transfer coefficient, the diffusion coefficient and concentration of dithiol anions, the standard heterogeneous rate constant as well as the formal potential and equilibrium constant of the preceeding dissociation reaction. This paper also illustrates the methods for studying the electrode kinetics of reactions which (a) involve a chemical reaction preceeding the electron-transfer process, (b) have insoluble polymer products, and (c) are totally irreversible.     

重复试验随机效应模型误差方差的齐性检验$(k=2)$

本文对重复试验次数为2的随机效应方差分析模型, 给出了误差方差齐性, 即$H_0:\sigma_1^2 =\sigma_2^2\leftrightarrow H_1:\sigma_1^2\ne\sigma_2^2$的一种具有相合性的检验方法\bd 并对三个常见模型给出了检验统计量和拒绝域的具体表达式, 最后是两个应用实例\bd     

连续调查的整群抽样

本文讨论了连续调查中应用普查方法时的整群抽样和分层整群抽样。     

Theoretical Design of High-spin Organic Molecules with —^＊N—S— as a Spin-containing Fragment and Heterocycle as End Groups

IntroductionDesigns and syntheses of organic molecules withvery high-spin ground states have been a topic of greatinterest[1—8].One of the rational approaches to desig-ning high-spin molecules,which has been proposedand studied by several groups[9,10],in…     

Differential Proteomic Analysis of Neonatal Cardiomyocytes in Response to β-Adrenergic Receptor Stimulation

Introduction Adrenoceptors(ARs),membersofthesuperfami lyofG proteincoupledreceptors,arethemostimpor tantreceptorsinvolvedincardiacregulation[1].ARsin cardiacmuscleincludebothαARsandβARssub types,whileinmostmammalianheart,βARsarethe predominantsubtypes.…     

Halin-图的点强全染色

图G(V,E)的一个k-正常全染色f叫做一个k-点强全染色当且仅当对任意v∈V(G), N[v]中的元素被染不同色,其中N[v]={u|uv∈V(G)}∪{v}．χTvs(G)=min{k|存在图G的k- 点强全染色}叫做图G的点强全色数．对3-连通平面图G(V,E),如果删去面fo边界上的所有点后的图为一个树图,则G(V,E)叫做一个Halin-图．本文确定了最大度不小于6的Halin- 图和一些特殊图的的点强全色数XTvs(G),并提出了如下猜想:设G(V,E)为每一连通分支的阶不小于6的图,则χTvs(G)≤△(G) 2,其中△(G)为图G(V,E)的最大度．     

Mass Spectral Fragmentation of (S,S)-N,N′-Bis [1-(hydroxymethyl)alkyl]anthracene/Naphthalene-1,8-dicarboxamides under Electron Impact Ionization Conditions

IntroductionN,N′-Bis [1-( hydroxymethyl) alkyl] dicarboxa-mides are important intermediates for the syntheses ofbis-oxazolines, which are a class of the most importantand widely used ligands in catalytic asymmetric reac-tions[1,2]. On determining the str…