1-偶氮苯-3-(3-硝基-5-氯-2-吡啶)-三氮烯的合成及其与汞的显色反应

合成了显色剂1-偶氮苯-3-(3-硝基-5-氯-2-吡啶)-三氮烯(ABNCPyT),并用元素分析法和红外光谱法对其分子结构作了鉴定.研究了ABNCPyT与汞的显色反应,在pH 10.5的Na2B4O7-NaOH缓冲溶液中和聚氧乙烯烷基酚(Triton X-100)表面活性剂存在下,试剂与汞(Ⅱ)生成4:1型红色配合物.配合物的最大吸收峰位于525 nm,表现摩尔吸光率为1.92×105L·mol-1·cm-1.汞(Ⅱ)质量浓度在600 靏稬-1以内符合比耳定律.用拟定方法测定废水中微量汞,所得结果与原子吸收光谱法的结果一致,测得其相对标准偏差(n=5)≤2.5%,方法的回收率在97.5%～103.0%.     

基于双面质点振速测量的声场分离技术

现有的声场分离技术或是基于双面声压测量或是基于单面声压和质点振速测量。本文以二维空间傅里叶变换法作为声场分离算法,提出一种基于双面质点振速测量的声场分离技术。论文首先推导出了该方法的理论模型,随后通过仿真研究验证了该方法的有效性,并通过与基于双面声压测量的声场分离方法的比较说明了其优越性。结果表明:采用基于双面质点振速测量的声场分离方法可以有效实现声场分离;基于双面质点振速测量的声场分离方法可以获得更高的质点振速分离精度,而基于双面声压测量的声场分离方法可以获得更高的声压分离精度。     

硅锆复合包覆BiVO4晶体的表征及其机理研究

利用正硅酸乙酯(TEOS)和氧氯化锆(ZrOCl2·8H2O)的水解反应并经高温煅烧后,在BiVO4晶体表面形成SiO2·ZrSiO4膜,以提高BiVO4的耐高温性.采用红外光谱仪、X射线衍射仪、差热分析仪对产品进行了表征,并得出结论:包覆SiO2·ZrSiO4膜后的BiVO4晶体,其耐热温度由680℃提高到1000℃,并对包覆机理进行了探讨.     

有关力学工作的一些反思

近年来,我国的一部分力学工作者产生了一些困惑,他们感觉力学学科受到的重视程度在下降,远不如上世纪五六十年代.     

Cauchy Problems for KdV-type Equations and Higher-Order Conditional Symmetries

We develop the generalized conditional symmetry （GCS） approach to solve the problem of dimensional reduction of Cauchy problems for the KdV-type equations. We characterize these equations that admit certain higherorder GCSs and show the main reduction procedure by some examples. The obtained reductions cannot be derived within the framework of the standard Lie approach.     

Scheme to Implement Optimal Asymmetric Economical Phase-Covariant Quantum Cloning in Cavity QED

We propose an experimentally feasible scheme to implement the optimal asymmetric economical 1→2 phase-covariant quantum cloning in two dimensions based on the cavity QED technique. The protocol is very simple and only two atoms are required. Our scheme is insensitive to the cavity field states and cavity decay. During the processes, the cavity is only virtually excited and it thus greatly prolongs the efficient decoherent time. Therefore, it may be realized in experiment.     

Solitary Solution of Discrete mKdV Equation by Homotopy Analysis Method

In this paper, we apply homotopy analysis method to solve discrete mKdV equation and successfully obtain the bell-shaped solitary solution to mKdV equation. Comparison between our solution and the exact solution shows that homotopy analysis method is effective and validity in solving hybrid nonlinear problems, including solitary solution of difference-differential equation.     

Conservation Laws of a Discrete Soliton System

In this paper, we obtain an infinite number of conservation laws for a discrete soliton system by using a solvable generalized Riccati equation.     

公共诠释的社会功能与带有批判维度的主体际交往方式

公共诠释是一种社会共同体成员之间的话语交往方式,具有社会功能。诠释学起源于对文化经典的诠释,这在中国传统文化中已有丰富的实践。对文化经典和社会主流价值观念的诠释能够起到凝聚社会共识和维系社会团结的作用。公共诠释与生活形式、伦常规范乃至政治权力相关联。这里存在共同体与个体、客观与主观、传承与革新之间的辩证关系。马克思在《德意志意识形态》和《黑格尔法哲学批判》等著作中阐明,与压迫阶级的统治权力结合在一起的意识形态具有虚假性和欺骗作用。这意味着公共诠释能起到正反两方面的作用。只有把握好这里的辩证关系才能充分发挥公共诠释的积极意义。