Nonlinear dynamic behaviors of a bolted joint rotor system supported by ball bearings

Archive of Applied Mechanics - A dynamic model of the rotor-bearing system with bolted joint structure is set up based on the Lagrange’s equations, which considers the bearing clearance, the...     

阳离子交换皂石黏土在基质辅助激光解吸电离飞行时间质谱分析中的应用

将一种人工合成的无机聚合物——蒙脱石皂石黏土（smectite,Sm）应用于基质辅助激光解吸电离飞行时间质谱分析（matrix-assisted laser desorption/ionization time of flight mass spectrometry, MALDI-TOF-MS）,以检测糖类化合物。 将传统的有机基质2,4,6-三羟基苯乙酮（trihydroxyacetophenone, THAP）与阳离子交换后的皂石黏土混合制备成新型复合基质,应用于糖类化合物的检测。通过比较不同的制样方法,测定不同分子直径的糖类化合物,发现由于受复合基质晶面间距的限制,只有小分子糖类化合物能进入晶面间隙充分接触有机基质并被离子化,从而实现对小分子糖类化合物的选择性检测。     

基于红外和可见光图像逐级自适应融合的场景深度估计

从图像中恢复场景的深度是计算机视觉领域中的一个关键问题。考虑到单一类型图像在深度估计中受场景不同光照的限制,提出了基于红外和可见光图像逐级自适应融合的场景深度估计方法（PF-CNN）。该方法包括双流滤波器部分耦合网络、自适应多模态特征融合网络以及自适应逐级特征融合网络。在双流卷积中红外和可见光图像的滤波器部分耦合使两者特征得到增强;自适应多模态特征融合网络学习红外和可见光图像的残差特征并将两者自适应加权融合,充分利用两者的互补信息;逐级特征融合网络学习多层融合特征的结合,充分利用不同卷积层的不同特征。实验结果表明:PF-CNN在测试集上获得了较好的效果,将阈值指标提高了5%,明显优于其他方法。     

铌酸锂晶体的光折变效应

铌酸锂(LiNbO₃, LN)是一种多功能多用途的人工晶体,被称为“光学硅”。近期以铌酸锂薄膜(LNOI)为平台的集成光子学发展迅速,有将“光学硅”变为现实的趋势。高集成意味着高局域高光强密度,使铌酸锂晶体的光折变效应变得不容忽视。光折变效应是光致折射率变化的简称,是非线性光学的重要组成部分。本文回顾了铌酸锂晶体光折变效应的发现和机理、不同掺杂及掺杂组合对光折变效应的调控,重点介绍了铋镁双掺铌酸锂晶体的光折变性能及相关理论和实验结果,概述了铌酸锂光折变波导和孤子,及基于LNOI的集成光子学器件中的光折变效应,并对未来的研究趋势进行了展望。期待我国发挥铌酸锂光折变研究及LNOI产业化的优势,在光子学芯片的竞争中占据主导地位。     

Transition Metal Catalyzed Enantioselective Borylative Cyclization Reactions

Due to the significance of corresponding products,enantioselective borylative cyclization reactions have been studied intensively in recent years.Many groups have developed efficient methods to transform unsaturated system into asymmetric cyclic organoboron compounds with the ring-size range from three-membered to six-membered in general.Notably,in some cases,fused rings which contain more than two contiguous chiral centers could be obtained by this kind of strategies.This review summarized and reviewed the recent advances in this field and classified these work according to the species of metal catalysts.     

尿素水解法制备球形磁性Al2O3复合材料

利用酸化法在磁性Fe3O4纳米粒子表面包覆SiO2膜,制备了Fe3O4/SiO2复合粒子。然后将该复合粒子超声分散在尿素和铝盐的混合溶液中,利用油中成型法制备出球形纳米磁性Al2O3复合材料,通过水热焙烧等工序处理得γ-Al2O3。实验中采用XRD、TEM、BET、AGM等方法对复合粒子的性能进行了表征,探讨了制备过程对产物晶型的影响、产物的孔结构变化和磁学性能。另外添加的SiO2膜阻止了磁性Fe3O4纳米粒子的进一步团聚,使得Fe3O4纳米粒子保持较小尺寸并均匀分散在产物中,复合材料表现出超顺磁性;同时SiO2膜防止了磁核部分与Al2O3包覆层在高温焙烧时发生反应;还起到加强粘结的作用,使得Al2O3在使用过程中不容易脱落。     

牛血红蛋白催化荧光猝灭法测定痕量甲巯咪唑

在NH3·H2O-NH4Cl缓冲溶液中,牛血红蛋白催化H202氧化L-酪氨酸产生荧光,甲巯咪唑对该荧光体系具有较强的猝灭作用.据此建立了酶催化荧光猝灭法测定痕量甲巯咪唑的方法.结果表明,甲巯咪唑含量在0.986～14.8 μg/L范围内与荧光强度变化值呈线性关系,其线性回归方程为△F405nm=50.923p+191....     

A Polyoxometalate-Encapsulated Metal–Organic Framework Nanoplatform for Synergistic Photothermal–Chemotherapy and Anti-Inflammation of Ovarian Cancer

Photothermal therapy (PTT), as a noninvasive and local treatment, has emerged as a promising anti-tumor strategy with minimal damage to normal tissue under spatiotemporally controllable irradiation. However, the necrosis of cancer cells during PTT will induce an inflammatory reaction, which may motivate tumor regeneration and resistance to therapy. In this study, polyoxometalates and a chloroquine diphosphate (CQ) co-loaded metal–organic framework nanoplatform with hyaluronic acid coating was constructed for efficient ovarian cancer therapy and anti-inflammation. Our results demonstrated that this nanoplatform not only displayed considerable photothermal therapeutic capacity under 808 nm near-infrared laser, but also had an impressive anti-inflammatory capacity by scavenging reactive oxygen species in the tumor microenvironment. CQ with pH dependence was used for the deacidification of lysosomes and the inhibition of autophagy, cutting off a self-protection pathway induced by cell necrosis–autophagy, and achieving the synergistic treatment of tumors. Therefore, we combined the excellent properties of these materials to synthesize a nanoplatform and explored its therapeutic effects in various aspects. This work provides a promising novel prospect for PTT/anti-inflammation/anti-autophagy combinations for efficient ovarian cancer treatment through the fine tuning of material design.     

1.315μm光解碘激光的大气透过率测量实验

利用1.315μm光解碘激光器在实际大气中作了大气透过率的测量,在中等能见度,相对湿度为64％和温度为21℃的条件下,平均透过率为0.78,同时用现有的数据库和计算程序作了计算比较,发现实验结果与计算值基本一致。     

基于遗传模型改进蜂群算法的稀疏阵列优化

人工蜂群算法作为一种新兴的群体智能算法,在解决复杂连续问题时表现突出。但是由于算法本身内在运行机制的原因,算法在搜索上表现出优异的性能,却疏于开发。为了平衡搜索和开发二者之间的矛盾,提出了一种基于遗传模型改进的人工蜂群算法,并成功运用到了阵列综合领域。算法先将全局最优解引入邻域搜索过程,指导蜂群寻找最佳蜜源,加速算法收敛。为了避免人工蜂群算法陷入局部最优,需要提高其开发能力,通过借鉴遗传算法中的进化机制,建立了遗传模型,对采取最佳保留后的蜜源进行遗传操作,丰富蜜源的多样性。在一组广泛使用的数值函数上对改进人工蜂群算法进行了测试,实验数据表明,该算法相较于其他算法具有很强的竞争力。将该算法运用于线性阵列的稀疏优化,旨在降低阵列的峰值旁瓣电平,在同样的阵列约束下与其他算法进行了优化对比,仿真结果进一步证明了算法的有效性。