MEMS微梁粘着动力分析

针对严重影响MEMS性能和可靠性的微梁粘着问题,根据W-S微观连续介质理论,建立了粘着力数学模型;针对粘着力对微梁刚度的强非线性影响,利用单元离散法,通过对粘着力时空变量相分离,对500μm×1μm×0.1μm表面镀金的微悬臂梁粘着进行了动力仿真,发现了“跳跃粘着”现象,从而为微梁的系统研究提供理论基础。     

REMARK ON STABILITY OF ISHIKAWA ITERATIVE PROCEDURES

1　ＩｎｔｒｏｄｕｃｔｉｏｎａｎｄＰｒｅｌｉｍｉｎａｒｉｅｓＳｕｐｐｏｓｅＥｉｓａｒｅａｌＢａｎａｃｈｓｐａｃｅａｎｄＴｉｓａｓｅｌｆｍａｐｏｆＥ .Ｓｕｐｐｏｓｅｘ0 ∈Ｅａｎｄｘｎ+1=ｆ(Ｔ ,ｘｎ)ｄｅｆｉｎｅｓａｎｉｔｅｒａｔｉｏｎｐｒｏｃｅｄｕｒｅｗｈｉｃｈｙｉｅｌｄｓａｓｅｑｕｅｎｃｅｏｆｐｏｉｎｔｓ ｘｎ ∞ｎ=0 ｉｎＥ .Ｆｏｒａｎｅｘａｍｐｌｅ ,ｔｈｅｆｕｎｃｔｉｏｎｉｔｅｒａｔｉｏｎｘｎ+1=ｆ(Ｔ ,ｘｎ) =Ｔｘ0 .ＳｕｐｐｏｓｅＦ(Ｔ) =ｘ∈Ｅ :Ｔｘ=ｘ ≠ ａｎｄｔｈａｔ ｘｎ ｃｏｎｖｅｒｇｅｓｓ…     

粘性减阻技术及其应用

本文综述了几种粘性减阻方法及其减阻的机理，联系了其在水相、油相中节约能源、材料，提高速度和效率等方面的应用     

Density Functional Theory Study of the Interaction between Guanine and Catechin

The interacting patterns and mechanism of the catechin and guanine have been investigated with the density functional theory B3LYP method by 6‐31G* basis set. Fourteen stable structures for the catechin‐guanine complexes have been found which form two hydrogen bonds at least. The results indicate that the complexes are mainly stabilized by the hydrogen bonding interactions. At the same time, the number and strength of hydrogen bond play a co‐determinant parts in the stability of the complexes which can form two or more hydrogen bonds. Theories of atoms in molecules (AIM) and natural bond orbital (NBO) have been adopted to investigate the hydrogen bonds involved in all systems. The interaction energies of all complexes have been corrected for basis set superposition error (BSSE), ranging from ?38.86 to ?14.56 kJ/mol. The results showed that the hydrogen bonding contributes to the interaction energies dominantly. The corresponding bonds stretching motions in all complexes are red‐shifted relative to that of the monomer, which is in agreement with experimental results.     

Three antibacterial naphthoquinone analogues from cultured mycobiont of lichen Astrothelium sp.

<正>A new naphthoquinone compound named 7-hydroxyl-8-methoxyltrypethelone 3 together with two known compounds trypethelone 1 and trypethelone methyl ether 2 was isolated from cultured mycobiont of Astrothelium sp.The structures were elucidated by 1D and 2D NMR spectroscopic analysis as well as comparison with those reported in literatures.Compound 1 displayed significant antibacterial activity against Bacillus subtilis(ATCC 6633),and showed modest antibacterial activity against Staphylococcus aureus col(MRSA)(CGMCC 1.2465),while compounds 2 and 3 showed modest antibacterial activity against Enterococcus faecalis 850E(CGMCC 1.2135) and S.aureus col(MRSA)(CGMCC 1.2465).     

99mTc-AMD3100: A novel potential receptor-targeting radiopharmaceutical for tumor imaging

<正>The chemokine CXCR4 receptor is over-expressed in a wide variety of tumors.In this study,AMD3100,which was a prototype non-peptide antagonist of CXCR4 receptor,was labeled with ~(99m)Tc.~(99m)Tc-AMD3100 was verified by thin layer radio chromatography(TLRC).The tumor-localizing properties of ~(99m)Tc-AMD3100 were evaluated and proved in mice bearing Hep-G2 tumor xenograft.~(99m)Tc-AMD3100 was a promising,novel receptor-specific radiopharmaceutical with potential application in the imaging of human tumors.     

A selective voltammetric detection for dopamine using poly (gallic acid) film modified electrode

<正>The electrochemistry behavior of dopamine was investigated by cyclic voltammetry and differential pulse voltammetry at a poly (gallic acid) film modified glassy carbon electrode.Two electrons and two protons participated in the diffusion-controlled electrocatalytic oxidation of dopamine with a diffusion coefficient of 2.186×10~(-5) cm~2/s.The interference of ascorbic acid with the determination of dopamine could be efficiently eliminated.This work provided a simple approach to selectively and sensitively detect dopamine in the presence of high concentration of ascorbic acid.     

Reactive adsorption of thiophene on Ni/ZnO adsorbent：Effect of ZnO textural structure on the desulfurization activity

To better understand the nature of reactive adsorption of thiophene on Ni/ZnO adsorbent, the effect of ZnO textural structure on the desulfurization activity was investigated. ZnO materials were synthesized by low-temperature solid-state reaction and the corresponding Ni/ZnO adsorbents were prepared by incipient impregnation method. The analysis results showed that the crystalline sizes of ZnO as-synthesized as well as the BET surface areas varied obviously with the calcination temperature. The activity evaluations indicated that the Ni/ZnO adsorbents prepared with ZnO possessed a favorable textural structure as active component exhibited good activity of removing thiophene. The evolutions of the main crystalline phases of Ni/ZnO adsorbents before and after reaction confirmed that ZnO played a crucial role in taking up S element and converting it into ZnS in the reactive adsorption process. It was concluded that ZnO with larger surface area and smaller crystal particles resulted in better desulfurization activity, which may be the main reason for the different activities of the Ni/ZnO adsorbents prepared with ZnO calcined at different temperatures.     

发展二氧化碳的绿色高新精细化工产业链建设低碳生态产业园

本文开发了从烯烃生产环氧烷烃,二氧化碳合成碳酸二甲酯联产二元醇,以绿色化学原料碳酸二甲酯代替剧毒的光气,开发了碳酸甲乙(丙、丁、戊、己、辛酯)、二乙(丙、丁、戊、己、辛)酯、二苯酯、呋喃唑酮、碳酰肼、苯胺基甲酸甲酯、苄胺基甲酸甲酯、对苯二胺二甲酸甲酯、间羟苯胺基甲酸甲酯、间甲苯胺基甲酸甲酯、二胺基甲酸甲酯二苯甲烷、己二胺二甲酸甲酯、烷基胺甲酸甲酯、肼基甲酸甲酯、嘧黄隆、甲黄隆、氯黄隆、异氰酸酯、聚氨酯、聚碳酸酯等一系列绿色清洁生产新工艺,间接实现了二氧化碳替代剧毒的光气,形成了具有中国特色的二氧化碳的绿色高新精细化工产业链,可建设成为低碳生态产业园。     

胶粘剂拉伸剪切强度测量结果的不确定度评定

依据GB/T 7124-2008《胶粘剂拉伸剪切强度的测定》,以环氧树脂结构胶为例,对胶粘剂拉伸剪切强度测量结果的不确定度分量进行了分析和量化,计算了合成标准不确定度和扩展不确定度。当环氧树脂结构胶的拉伸剪切强度为28.8 MPa时,扩展不确定度为1.0 MPa(k=2)。