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21.
Nilsson CL Cooper HJ Håkansson K Marshall AG Ostberg Y Lavrinovicha M Bergström S 《Journal of the American Society for Mass Spectrometry》2002,13(4):295-299
Borrelia burgdorferi sensu lato is a tick-borne pathogen that causes Lyme disease. The characterization of membrane proteins from this and other pathogens may yield a better understanding of the mechanisms of infection and information useful for vaccine design. Characterization of the highly hydrophobic Borrelia outer membrane component P13 from a mutant (OspA- OspB- OspC- and OspD-) strain was undertaken by use of a combination of mass spectrometric methods. In a previous investigation, an electrospray ionization (ESI) mass spectrum of the intact protein provided an average molecular weight that was 20 Da lower than the predicted molecular weight. The mass deviation could be explained by a modification of the N-terminus of the protein such as pyroglutamylation (-17 Da) in combination with the experimental error of measurement, however more information was required. New structural information for this membrane protein was provided by peptide mapping with matrix-assisted laser desorption/ionization time-of-flight mass spectrometry (MALDI TOF MS) and sequencing with ESI-quadrupole-TOF tandem MS. 相似文献
22.
A super-operator formulation for decoupling symmetry blocks of the full 2p-h TDA electron propagator matrix is presented, accuracy is explored using the full 2p-h TDA overlap amplitudes to calculate relative ionization intensities for N2 and H2O. The effect of excluding orbitais on IPs and relative ionization cross sections is reported. 相似文献
23.
Yngve Stenstr⊘m 《合成通讯》2013,43(19):2801-2810
Zinc powder activated by heating in an inert atmosphere gave good yields when used for the title reactions. The very easy work up procedure for the cyclobutanones further increases the potential of the method. 相似文献
24.
A short and concise synthesis of volicitin is presented. The synthesis is based on repeated chemoselective copper salt cross coupling reactions of alkynes and propargylic halides. 相似文献
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26.
Larring Yngve Pishahang Mehdi Tolchard Julian Lind Anna M. Sunding Martin F. Stensrød Ruth E. Jacobs Marijke Snijkers Frans van der Kolk Tjalling Albertsen Knuth 《Journal of Thermal Analysis and Calorimetry》2020,140(2):577-589
Journal of Thermal Analysis and Calorimetry - The CLOU performance of the CaTixMn0.9?xMg0.1O3 (CMTM) perovskite-type system was investigated, comparing materials produced at laboratory scale... 相似文献
27.
An improved route to 5,8,8-trimethylbicyclo[4.3.0]-4-nonen-3-one, a key intermediate for the synthesis of the protoilludane skeleton and in particular Δ7-protoilludene, is reported. Attempts on an alternative synthesis of Δ6-protoilludene based on a phenylsulfonyl allene cycloaddition reaction is also presented. 相似文献
28.
The theoretical concept of a potential energy surface, so important for the accepted pictures of molecular structure and bonding, plays a key role in most current methods of molecular reaction dynamics. However, the lack of quality potential energy surfaces for anything but the smallest of systems and the great expense and difficulty in producing several surfaces and their nonadiabatic coupling terms with sufficient accuracy is becoming a hindrance to accurate reaction dynamics. The electron nuclear dynamics (END) theory provides a new way to address this problem by circumventing the use of potential energy surfaces while accounting fully for nonadiabatic couplings. Preliminary results for the prototypical low-energy reactive collision between the hydrogen molecular ion and the hydrogen molecule are given for both electron transfer and chemical exchange. © 1996 John Wiley & Sons, Inc. 相似文献
29.
Th. W. Richards V. Yngve Ch. O. Steinmetz und W. Buell Meldrum 《Fresenius' Journal of Analytical Chemistry》1919,58(1):26-28
Ohne Zusammenfassung 相似文献
30.