基于线性方程组数学分离模型建立光纤传感过程检测复方缬沙坦氢氯噻嗪片溶出度

基于线性方程组数学分离模型建立在线过程检测复方缬沙坦氢氯噻嗪片溶出度方法。分别扫描缬沙坦和氢氯噻嗪的紫外吸收光谱,两组分在最大吸收波长处完全重叠。根据朗伯比尔定律吸光度加和性原理,分别测定两组分在最大吸收波长处的吸光系数,建立线性方程组数学分离模型,采用光纤传感过程分析技术(FODT)检测缬沙坦氢氯噻嗪片的溶出度,并与HPLC法相比较。在规定的溶出介质中,两种成分同时实时测定,并且FODT累积溶出度与HPLC法相比较结果无显著性差异(p>0.05)。不同批次药物的溶出行为一致,说明制剂工艺稳定,均匀度好。溶出曲线显示缬沙坦溶出快于并高于氢氯噻嗪,且30 min时两组分的溶出度均大于80%符合美国药典规定。结果表明,应用线性方程组数学分离模型结合FODT法可实现复方缬沙坦氢氯噻嗪片中双组分溶出度的同时检测,并可提供双组分的溶出过程曲线和全部溶出数据,直观反映各组分在各溶出时段的快慢,为此药建立标准提供依据。与HPLC法单点数据相比优势明显,更有利于药品评价和抽验质量分析。     

Hadronic Scenarios for Gamma-Ray Emission from Three Supernova Remnants Interacting with Molecular Clouds

GeV γ-rays detected with the large area telescope on board the Fermi Gamma-ray space telescope in the direc- tion of HB21, MSH 17-39 and G337.0-0.1 have been recently reported. The three supernova remnants （SNRs） show interactions with molecular clouds, and they are effective gamma-ray emitters as the relativistic protons accelerated by the SNR shocks inelastically colliding with the dense gas in the clouds. The origin of the observed γ-rays for the three remnants is investigated in the scenario of the diffusive shock acceleration. In the model, a part of the SNR shock transmits into the nearby molecular clouds, and the shock velocity is greatly reduced. As a result, a shock with a relatively low Alfven Mach number is generated, and the spectra of the accelerated protons and thee＇γ-ray photons produced via proton-proton interaction can be obtained. The results show that the observed γ-ray spectra for the three SNRs interacting with the molecular clouds can be reproduced. It can be concluded that the hadronic origin of the γ-rays for the three SNRs is approved, and the ability of SNR shocks to accelerate protons is also supported.     

电子白板系统中参数标定方法的研究

为了避开复杂繁琐的摄像机标定过程,提出了一种基于CCD摄像机的电子白板系统参数标定新方法,实现了开机自动标定系统参数的功能。采用Harris角点检测算法成功提取了参考点的像素坐标,并直接运用射影变换交比不变性,推导出白板边框图像像素距离与实际物理距离的映射关系式,进而获得了摄像机的光心坐标。简要分析影响系统标定精度的因素,并设计出减小标定误差的方案,最后搭建实验平台标定系统参数。实验结果表明:该标定方法实现简单,应用方便,且对于单位长度为1 cm的标定块而言,标定误差小于0.04 cm。     

示波器电子运动规律与波形显示关系研究

本文详细地论述了示波管荧光屏上的显示波形与电子运动规律、波形周期与扫描电压周期间的关系,以便帮助学生理解和解决学习示波器原理过程中遇到的疑难、疑惑问题。     

Electronic Structure and Optical Properties of Antimony-Doped SnO_2 from First-Principle Study

A first-principles study has been performed to calculate the electronic and optical properties of the SbxSn1xO system.The simulations are based upon the method of generalized gradient approximations with the Perdew-Burke-Ernzerhof form in the framework of density functional theory.The supercell structure shows a trend from expanding to shrinking with the increasing Sb concentration.The increasing Sb concentration induces the band gap narrowing.Optical transition has shifted to the low energy range with increasing Sb concentration.Other important optical constants such as the dielectric function,reflectivity,refractive index,and electron energy loss function for Sb-doped SnO2 are discussed.The optical absorption edge of SnO2 doped with Sb also shows a redshift.     

弗兰克-赫兹实验中温度与电子平均自由程的关系

运用原子非弹性碰撞模型来测量F-H曲线峰谷间距随峰谷数的线性关系,研究温度对电子平均自由程的影响,并尝试探讨一种较为准确的测量原子第一激发能的实验方法.     

Result of search for low velocity exotic particles

The L3＋C experiment, taking advantage of the L3 muon magnetic spectrometer, measured the spatial tracks of charged cosmic ray particles to obtain rigidity as well as velocity. One possible low velocity exotic particle is observed. The existing uncertainties are discussed, and the flux upper limit of the low velocity exotic particles from this observation is deduced based on the assumption of a null observation. The result is 6.2×10^-10 cm^-2·s^-1·sr^-1 at 90% confidence level in the velocity range from 0.04c to 0.5c.     

新大线同沟敷设热力分析

针对新大线同沟敷设管道,采用非结构化有限容积法,分析了不同的物性条件下,常温输送原油对加热输送原油的热力影响.     

填埋垃圾渗滤液中水溶性有机物去除规律研究

采集垃圾渗滤液四个不同处理阶段水样,提取制备水溶性有机物(DOM),采用荧光光谱、紫外光谱及红外光谱,研究了不同阶段渗滤液DOM含量与结构特征。结果显示,整个处理过程渗滤液DOM浓度降低了377.6 mg·L-1,总去除率为78.34%,厌氧处理氧化沟和MBR过程分别去除了不同处理阶段出水中的水溶性有机物碳(DOC);厌氧处理增加了渗滤液DOM中不饱和化合物和多糖类物质含量,提高了渗滤液的可生化性;氧化沟处理有效降解了不饱和化合物和糖类。调节池和和厌氧处理过程DOM出现了类蛋白荧光峰和类腐殖质荧光峰,而氧化沟和MBR出水只有类腐殖质荧光峰,类蛋白物质和类富里酸物质主要在厌氧区和氧化沟中去除,而类胡敏酸物质主要在MBR过程中去除。     

适用于非常规工作环境中热释电型激光能量计的研制

现有的激光能量计传感器灵敏度系数都与其所处环境温度有关,在-50℃～70℃的温度范围内,灵敏度偏差较大,直接影响测量结果。为了达到消除环境温度的影响,采取在不同环境温度下对热释型能量计的灵敏度进行校准的研究方法。该校准方法与普通激光能量计的校准方法的不同之处在于对热释电型能量计进行校准时,温度由室温扩展到-50℃～70℃的温度范围。利用环境试验箱,每隔10℃固定一个温度点,进行激光能量的测量实验,得到各个温度点所对应的灵敏度修正系数,再借助最小二乘法建立起各个温度点上能量计灵敏度系数同环境温度的函数关系,从而实现了-50℃～70℃的温度范围内激光能量的准确计量。研制能直接工作于非常规工作环境下的热释电型激光能量计,对解决激光能量测量的外场需求有一定现实意义。