用喷涂晶种法ZSM-5合成沸石膜及其影响因素考察

在多孔α－Ａｌ２Ｏ３载体上,采用喷涂方法引入一层晶种,再用水热法合成出渗透量大、气体选择分离系数高的ＺＳＭ－５沸石膜;对影响ＺＳＭ－５沸石膜合成的主要因素进行卫考察,并用ＸＲＤ,ＳＥＭ及单组分气体渗透性能测定对所合成的沸石膜进行了表征。结果表明,所合成的沸石膜是典型的ＺＳＭ－５沸石膜,膜表面晶粒排列有序,整齐地连成一致密层,绝大部分晶粒的取向一致,无较大裂缺存在,经一次合成的沸石膜的Ｈ２渗透率可达     

固体材料激光冷却的实验研究及其最新进展

近年来，基于反斯托克斯荧光制冷(Anti—Stokes Fluorescent Cooling)的固体材料激光冷却技术得到了快速发展。本文首先简单介绍了固体材料激光冷却的基本原理及其技术；其次，详细介绍了各种固体激光冷却的新材料、新方案和新结果及其最新实验进展；最后，就固体激光冷却技术的应用前景及其未来发展方向等问题进行了简单讨论与展望。     

Three-dimensional GaN-Ga2O3 core shell structure revealed by x-ray diffraction microscopy

In combination of direct phase retrieval of coherent x-ray diffraction patterns with a novel tomographic reconstruction algorithm, we, for the first time, carried out quantitative 3D imaging of a heat-treated GaN particle with each voxel corresponding to 17 x 17 x 17 nm3. We observed the platelet structure of GaN and the formation of small islands on the surface of the platelets, and successfully captured the internal GaN-Ga2O3 core shell structure in three dimensions. This work opens the door for nondestructive and quantitative imaging of 3D morphology and 3D internal structure of a wide range of materials at the nanometer scale resolution that are amorphous or possess only short-range atomic organization.     

长白山地区几种红景天品种的傅里叶变换红外光谱法鉴别研究

分别用石油醚,氯仿,甲醇对长白山地区的野生和栽培高山红景天和长白红景天进行了提取,并首次对提取物进行了傅里叶变换红外光谱法测定,还用红景天块做了相应的验证研究。结果表明,长白山地区的野生和栽培高山红景天和长白红景天的红外光谱图谱有明显不同,故可用作鉴别其品种或评价其质量的一种手段。     

Numerical Simulation on the Production Mechanism of Surface-Wave Plasmas Sustained along a Metal Rod

For interpreting the production mechanism of surface-wave plasmas sustained along a metal rod, electromagnetic simulation on the electromagnetic field distributions and particle-in-cell/Monte Carlo collision （PIC/MCC） simulation of the ionization process are present. The results show that the enhanced electric field of surface plasmon polaritons （SPPs） can be excited in the ion sheath layer between the negative-voltage metal rod and the surface-wave plasmas, which is responsible for maintaining the plasma discharge. Moreover, the spatio-temporal evolutions of plasma density and electric fields are simulated by the PIC/MCC model. It is further suggested that the expanded ion sheath layer can extend the length of plasma domain by increasing the plasma absorbed energy from SPPs.     

用"删除法则"求3个同科电子的光谱项

提出了3个同科电子体系在L-S耦合中确定光谱项的“删除法则”,并加以证明．利用“删除法则”可以很方便地求出3个同科电子所形成的光谱项．     

阴极荧光光谱有效收集效率的计算与测量（I）

从点光源均匀发光模型出发,重点导出了回转半椭球面镜的阴极荧光(Cathodoluminescence,简称CL)光谱有效收集效率η_λ~(eff)的计算公式,分析讨论了收集效率η_λ~(eff)与椭球参数e、收集角、Δφ出射角Δ(?)以及出射光束方位角θ_N的关系,给出了相应的理论计算和模拟实验结果.研究表明,理论计算与实验结果一致.     

Wu-King 加载偶极天线的FDTD分析

 用时域有限差分法分析了高斯脉冲激励的Wu-King加载偶极天线的特性。给出了天线周围空间瞬态场的变化情况及天线上的电流波形,这种形象化的结果为加载脉冲辐射天线的设计和改进提供了直观的物理依据。通过时域远近场变换,得到了天线脉冲辐射远场。计算并给出了描述脉冲辐射器性能的时域参数：保真度和能量方向图。     

光子晶体Vlasov天线辐射特性研究

 通过在Vlasov天线口径上加装金属面,再在金属面上环绕天线口径排布金属圆柱构成光子晶体,设计出一种新型的光子晶体Vlasov天线。数值仿真及实验结果均表明,光子晶体的带隙特性改善了天线的辐射特性,使得E面上的最大增益在工作频段内平均提高了2.43 dB。