Summary: Hyperbranched poly(urea‐urethane)‐functionalized multiwalled carbon nanotubes (MWNT‐HPUs) have been synthesized by a one‐pot polycondensation of tolylene 2,4‐diisocyanate and diethanolamine in the presence of MWNTs terminated with multiple hydroxy groups. FT‐IR, Raman, 1H NMR, and 13C NMR spectra reveal that the HPU trees are covalently grafted onto the MWNT surfaces. After a high density of HPU trees (83.5 wt.‐%) is attached to the MWNTs, core‐shell nanostructures with MWNTs as the core and the HPU trees as the shell are formed. A loose and uniform nanotube network can be observed by TEM, SEM, and AFM. The resulting MWNT‐HPUs are soluble in polar solvents such as dimethylformamide, dimethylacetamine, 1‐methyl‐2‐pyrrolidinone, and dimethyl sulfoxide.
Eighteen interfering nuclear reactions that likely occur in neutron activation analysis of platinum group elements are studied.
Their degrees are calculated by the basic principle of activation analysis. The calculation results indicate that most of
the nuclear interferences become significant only if the interfering elements exist in major amount and the elements of interest
in trace amount. However, the second-order interference to platinum analysis from gold and the fission interference to analysis
of ruthenium and palladium from uranium cannot be neglected even if the gold and uranium exist as trace constituents in samples.
Project supported by the National Natural Science Foundation of China (Grant No. 19392100) and the China Postdoctoral Science
Foundation. 相似文献
Neutron activation analysis (NAA) was used to determine the concentrations of 6 elements Cr, Co, Rb, Cl, Br and I in 12 kinds of Chinese diets. The daily dietary intakes of these elements in 4 areas groups of China were investigated and the analytical results were compared with other countries and WHO recommended dietary intakes. 相似文献
A Q- value of 4.046 ±0.102 MeV has been determined for the two protons transfer reaction 160Gd(18O, 20Ne) 158Sm at 98.95 MeV. This result yields a first experimental measured value of ? 65.738 ± 0.102 MeV for the mass excess of 158Sm, the nucleus far from stability. The result is compared with current theoretical predictions. 相似文献
When an Automatic Speech Recognition (ASR) system is applied in noisy environments, Voice Activity Detection (VAD) is crucial
to the performance of the overall system. The employment of the VAD for ASR on embedded mobile systems will minimize physical
distractions and make the system convenient to use. Conventional VAD algorithm is of high complexity, which makes it unsuitable
for embedded mobile devices; or of low robustness, which holds back its application in mobile noisy environments. In this
paper, we propose a robust VAD algorithm specifically designed for ASR on embedded mobile devices. The architecture of the
proposed algorithm is based on a two-level decision making strategy, where there is an interaction between a lower features-based
level and subsequent decision logic based on a finite-state machine. Many discriminating features are employed in the lower
level to improve the robustness of the VAD. The two-level decision strategy allows different features to be used in different
states and reduces the cost of the algorithm, which makes the proposed algorithm suitable for embedded mobile devices. The
evaluation experiments show the proposed VAD algorithm is robust and contribute to the overall performance gain of the ASR
system in various acoustic environments. 相似文献
Some formulae on correlative match of both optical aperture and wave aberration to determine image quality are derived in this paper. The optimizing match zone on optical aperture and wave aberration were found both theoretically and experimentally. The results are importantly different from traditional criteria for image quality. 相似文献