1.5次微分吸附阴极溶出伏安法测定毛地黄毒苷及其电极过程的探讨

毛地黄毒苷是治疗心脏病的有效药物,它在汞电极上能吸附还原.以1.5次微分吸附阴极溶出伏安法测定检出限达3.2×10~(-10)mol/L.吸附溶出响应依赖于试液浓度、富集电位、富集时间、介质、溶液pH、温度及扫速等因素.不同富集时间,不同浓度范围内.浓度与峰高有良好的线性关系.毒苷的常规循环伏安图上出现两对氧化还原峰,电极反应相似于α,β不饱和羰基的1,2和1,4加成,电极反应可逆.毒苷在汞电极上的饱和吸附量为3.54×10~(-11)mol/cm~2.     

金属柱平板慢波系统高频特性研究

对于离散的金属柱结构构建的周期性平板慢波系统,本文利用3维FDTD方法结合HFSS仿真软件深入分析了该慢波系统的高频特性.研究了金属柱高度、周期长度对色散特性的影响,计算了耦合阻抗,并与传统光栅慢波系统特性进行了对比分析.分析表明金属柱慢波系统既有与传统光栅慢波系统相似的高频特性,又具有独自的特点,位于离散的金属柱周期间隙中的电子注互作用耦合阻抗具有对称性;金属柱结构用作真空电子器件的高频系统可增加发生有效互作用的电子注厚度,降低起振电流密度,提高器件效率.本文的分析结果为设计低电流密度工作的多电子注短毫 关键词： 金属柱平板慢波系统 3维FDTD算法 色散特性 耦合阻抗     

基于神经网络的三维宽场显微图像复原研究

提出一种利用BP神经网络进行三维宽场显微图像复原的非线性映射方法,将三维图像转化为二维图像进行处理,利用神经网络的学习能力,通过训练,建立含有散焦信息的二维模糊图像与二维清晰图像之间的映射关系,然后对切片堆叠进行逐幅复原,从而实现显微图像的三维复原.得到的复原图像在视觉上和定量分析上都获得了很好的效果.由于采用小规模神经网络,训练时间短,计算量小,使实时复原成为可能.     

高功率半导体激光端面泵浦方形掺Nd3+离子激光晶体热形变研究

为了解决高功率半导体激光器端面泵浦激光晶体引起的热效应问题,激光晶体泵浦端面的热形变必须进行准确的计算.通过对于全固态激光器中激光晶体的工作特点分析,建立了矩形截面激光晶体热分析模型.基于热传导方程,提出了泊松方程的一种新解,并获得了矩形截面激光晶体端面热形变分布的一般解析表达式.同时讨论了半导体激光器偏心泵浦激光晶体给端面热形变带来的影响.与有限元分析方法以及其他数值分析方法相比,解析分析方法不会给计算引入任何的误差.热形变的解析分析为解决激光晶体的热效应问题以及提高激光器的性能提供了理论的依据.     

一种用于电光开关的高速、高压电脉冲的产生

介绍了一种用于电光开关驱动源的高压超快电脉冲产生技术;电路采用级联的雪崩晶体管串和微波传输线结构,输出阻抗50Ω;在50Ω负载情况下,获得脉冲下降时间为1ns、幅度达到5kV、峰值电压为6.4 kV、幅度和半宽度稳定性优于2％、触发晃动为±15ps、触发延时为30 ns,脉冲峰值电流为128 A的高压高速大电流脉冲.     

光刻机硅片表面不平度原位检测技术

随着光刻特征尺寸的不断减小,硅片表面不平度对光刻性能的影响越来越显著.该文提出了一种新的硅片表面不平度的原位检测技术本文在分析特殊测试标记成像规律的基础上,讨论了测试标记的对准位置偏移量与硅片表面起伏高度的变化规律,提出了一种新的硅片表面不平度原位检测技术.实验表明,该技术可实现硅片表面不平度及硅片表面形貌的高准确度原位测量.该技术考虑了光刻机承片台吸附力的非均匀性对硅片表面不平度的影响,更真实反映曝光工作状态下的硅片表面不平度大小.与现有的原位检测方法相比,硅片表面不平度的测量空间分辨率提高了1.67%倍,可实现硅片表面形貌的原位检测.     

IMPROVED GENERALIZED ADMITTANCE MATRIX TECHNIQUE AND ITS APPLICATIONS TO RIGOROUS ANALYSIS OF MILLIMETER-WAVE DEVICES IN RECTANGULAR WAVEGUIDE

An improved generalized admittance (GAM) matrix technique is presented in this paper. Matrix transformation eliminates the singularity factor of GAM, denominator (1+Γ), because of new presentations of GAM. The relationship equations between II-port current and I-port incidence wave is computed by mode matching method. The generalized scattering matrix (GSM) of waveguide structure and its discontinuity problems is obtained with relationship equations and reflection coefficients. The GSM’s of millimeter-wave multistepped bend and T-junction in rectangular waveguide are computed by the improved GAM technique. The results comparisons between the proposed method and commercial software HFSS10.0 show the validity of the proposed method, which improves the validity of the GAM technique and reduces mathematical efforts. It is general, very efficient and can be used to solve other complicated and multiport network problems.     

D→Klv～l衰变过程的研究

用光锥QCD求和规则研究D→Klv～_l衰变过程，首先计算D→K跃迁形状因子，通过构造新的关联函数，消除了twist-3波函数的不确定性给计算结果所带来的影响，从而使计算结果更加精确. 计算得到的分支比与最近的实验数据相一致. 关键词： QCD光锥求和规则 D介子半轻衰变 分支比 形状因子     

Synthesis and enhanced acetone gas-sensing performance of ZnSnO<Subscript>3</Subscript>/SnO<Subscript>2</Subscript> hollow urchin nanostructures

A kind of novel ZnSnO₃/SnO₂ hollow urchin nanostructure was synthesized by a facile, eco-friendly two-step liquid-phase process. The structure, morphology, and composition of samples were characterized using X-ray diffraction (XRD), scanning electron microscopy (SEM), transmission electron microscopy (TEM), X-ray photoelectron spectroscopy (XPS), and nitrogen adsorption–desorption techniques. The results revealed that many tiny needle-like SnO₂ nanowires with the average diameter of 5 nm uniformly grew on the surface of the ZnSnO₃ hollow microspheres and the ZnSnO₃/SnO₂ hollow urchin nanostructures with different SnO₂ content also were successfully prepared. In order to comprehend the evolution process of the ZnSnO₃/SnO₂ hollow urchin nanostructures, the possible growth mechanism of samples was illustrated via several experiments in different reaction conditions. Moreover, the gas-sensing performance of as-prepared samples was investigated. The results showed that ZnSnO₃/SnO₂ hollow urchin nanostructures with high response to various concentration levels of acetone enhanced selectivity, satisfying repeatability, and good long-term stability for acetone detection. Specially, the 10 wt% ZnSnO₃/SnO₂ hollow urchin nanostructure exhibited the best gas sensitivity (17.03 for 50 ppm acetone) may be a reliable biomarker for the diabetes patients, which could be ascribed to its large specific surface area, complete pore permeability, and increase of chemisorbed oxygen due to the doping of SnO₂.     

基于增益光纤长度优化的双波长运转掺铒光纤锁模激光器

构建了可自启动的双波长运转掺铒光纤锁模激光器.通过优化增益光纤长度,利用掺铒光纤在1530nm附近的再吸收效应调节激光器的增益谱,使激光器在1530nm和1560nm附近具有相同的增益强度.实验中采用31cm掺铒光纤作为增益光纤,以透射式半导体可饱和吸收体作为锁模器件,实现了自启动双波长锁模运转.激光器锁模输出重复频率为58.01MHz,信噪比为58.2dB,最高输出功率为4.8mW.锁模输出的光谱在1532.4nm和1552.3nm处具有两个强度接近的谱峰,谱峰间距约为20nm.该激光器无需手动调节即可实现双波长运转,更便于实际使用.