玻璃料对铜基金属结合剂性能及结构的影响

采用粉末冶金法向铜基金属结合剂中引入玻璃料,结合材料电子万能试验机、洛氏硬度仪、SEM等检测方法,研究了玻璃料加入对铜基金属结合剂及金刚石磨具的影响.结果表明,随着玻璃料含量的增加,铜基结合剂的抗折强度和抗冲击强度呈下降的趋势,其硬度呈逐渐上升趋势,硬脆相的引入提高了铜基金属结合剂的自锐性;玻璃相和金属相之间结合紧密,两相之间化学元素在界面处发生相互扩散;玻璃料的加入使结合剂对磨料的包裹更加紧密,大大提高了结合剂对金刚石的把持力,有利于增加金刚石磨具寿命及加工效率.     

超分子构筑调控合成结构规整的梯形聚合物及其应用研究

综述了"超分子构筑调控的逐步偶联/聚合法",该方法将高分子化学与超分子化学相结合,利用多种类型的超分子弱键协同作用首先构筑预期的梯形超分子结构,再经聚合得到共价键梯形高分子.利用该方法合成了一系列结构规整的氧桥基和有机桥基梯形聚硅氧烷以及碳基梯形聚酯,并利用侧基间π-π叠加作用实现了对聚合物立体构型控制.扼要介绍了梯形聚合物在先进材料方面的应用,例如梯形聚硅氧烷液晶光致取向膜;由梯形聚硅氧烷合成的管状聚硅氧烷在高室温储存期微电子环氧塑封料方面的应用;以及基于梯形聚硅氧烷的拟筛板聚合物在二阶非线性光学材料方面的应用等.     

新的光散射体系测定蛋白质的研究

以1,6-己二胺二吖啶为荧光探针,建立了一种新的蛋白质共振散射检测体系。实验考察了该吖啶荧光探针的共振散射特征光谱、散射反应稳定性,研究了缓冲介质pH、探针浓度等参数对测定蛋白质的影响。结果表明,当pH 8.9时,1,6-己二胺二吖啶染料的散射波长为470 nm;加入BSA,反应约9 min后,体系光散射强度达到最大并维持稳定,2 h内无明显变化。当1,6-己二胺二吖啶探针(浓度1.00×10-4mol·L-1)用量为3.00 mL时,蛋白质与1,6-己二胺二吖啶的光散射增强作用显著,共振散射强度随着BSA的增加而明显增强,光散射强度与蛋白质浓度成良好线性关系,线性浓度范围为1.00～5.00 μg·mL-1,检测限(3σ/K)为0.085 μg·mL-1。测定了血清样品,浓度为2.00～4.00 μg·mL-1,回收率为98.0%～101.7%,测定偏差小于1.7％。     

Research on Flood Loss Distribution and Catastrophe Bond Pricing Based on Bayesian Inference

Taking flood catastrophe risk in China as the research background, aiming at the characteristics of flood loss ``low frequency and high loss', Bayesian inference method is used to fit the loss distribution, and Bayesian inference is used to obtain the loss frequency distribution and loss quota distribution of flood in China. On this basis, Monte Carlo simulation method is used to calculate the probability distribution of annual flood loss in China under different trigger conditions, and then CAPM is used to study the pricing of flood catastrophe bonds in China. It is concluded that under different trigger conditions, as the trigger value increases gradually, the corresponding trigger is triggered. Comparing the three types of bonds, it can be found that the price of bonds decreases with the decrease of principal guarantee ratio and the increase of principal loss ratio, that is, the investment risk is directly proportional to the return, which provides reference for issuing flood catastrophe bonds in China.     

Charged-Exciton Complexes in Quantum Dots

It is known experimentally that stable charged-exciton complexes can exist in low-dimensional semiconductor nanostructures. Much less is known about the properties of such charged-exciton complexes since three-body problems are very difficult to be solved, even numerically. Here we introduce the correlated hyperspherical harmonics as basis functions to solve the hyperangular equation for negatively and positively charged excitons (trions) in a harmonic quantum dot. By using this method, we have calculated the energy spectra of the low-lying states of a charged exciton as a function of the radius of quantum dot. Based on symmetry analysis, the level crossover as the dot radius increases can be fully explained as the results of symmetry constraint.``     

用多极理论分析圆桩对称微波谐振腔

用多极理论计算具有复杂几何形状、圆柱对称微波腔的谐振频率,推导出用多极理论计算圆柱对称微波腔谐振频率的本征值方程。三个工程实例的计算结果表明,用多极理论计算圆柱对称微波腔谐振频率,不仅具有较高的计算精度,而且可以很方便地应用于复杂几何形状圆柱对称微波腔工程问题的设计与计算,多极理论是计算圆柱对称微波腔谐振频率的一种有效方法。     

三人热力学偏导数│эU／эn│S.V,│эH／эn│S,p和│эF／эn│T.V等于系

对三个热力学偏导数（эＵ／эｎ）Ｓ．Ｖ（эＨ／эｎ）Ｓ．ｐ和（эＦ／эｎ）Ｔ．Ｖ等于系统化学势给出了又一种证明方法。     

声子注入下超导锡膜的非均匀态

用Sn-I-Sn-I-Sn-I-Sn三重结进行实验,在强声子注入下,超导锡膜中出现了不同形式的空间非均匀态。 关键词：     

基于边缘软判决的小波域自适应图像去噪

提出了一个新的图像去噪方法。该方法基于非抽样小波变换的多分辨分解,在各尺度下对小波系数进行了边缘和非边缘分类,并根据它们的不同统计特性运用了不同的估计技术。鉴于边缘分类的不确定性,提出了依概率的软分类技术,通过计算边缘发生的概率,判决当前系数应该采用哪一种估计。仿真结果表明:该方法在滤除图像噪声的同时,边缘得到了保持,较目前存在的一些方法更具有优越性。     

激光点火系统温度效应及其控制技术的研究

激光点火系统应用于武器系统必须符合高低温性能的要求。研究了激光点火系统的高低温特性,得到了激光二极管阈值电流和输出光功率随温度变化的规律。基于对规律的分析,研制了带温控技术的激光点火系统。该系统以单片机为控制部件,以TEC为温控部件,以负温度系数热敏电阻为测温元件。