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31.
Synthesis and Properties of the Layered Perovskite Phase Sr3Mo1.5Zn0.5O7‐δ The new layered perovskite phase Sr3Mo1.5Zn0.5O7‐δ was synthesized by solid state reaction using a Zn/ZnO oxygen buffer. The crystal structure was refined from X‐ray powder pattern by the Rietveld method. The compound crystallizes tetragonal in the space group I4/mmm (no. 139) with the lattice parameters a = 3.9631(3) Å, c = 20.583(1) Å. An oxygen deficiency corresponding to δ ≈ 0.25 was determinated, indicating the presence of molybdenum in mixed valence (Mo4+ and Mo6+). 相似文献
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Werner WinterGünther W.H Höhne 《Thermochimica Acta》2003,403(1):43-53
A method for measuring heat capacities of small samples using a chip-calorimeter and a heat pulse technique is described. The theoretical background to calculate the heat transport properties and the heat capacity of the sample from the pulse response function is given. Problems and potentials of the method are discussed. An example is given. 相似文献
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Klaus Anderle Richard Birenheide Martin J. A. Werner Joachim H. Wendorff 《Liquid crystals》1991,9(5):691-699
Polarized light leads to an effective reorientation of the optic axis in the glassy state of liquid-crystalline side chain polymers containing azobenzene mesogenic groups, via a trans-cis and cis-trans isomerization. Using a combination of U V and IR dichroitic studies it is shown for copolymers consisting of chromophores (azobenzene) and non-chromophores (phenylbenzoate) that only the chromophores are reoriented by light as far as the glassy state is concerned. Individual chromophores are thus addressed by photoselection. Photoselection in the fluid nematic state, on the other hand, leads also to a reorientation of the non-chromophores. 相似文献
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O. Dumbrajs M. Thumm J. Pretterebner D. Wagner 《International Journal of Infrared and Millimeter Waves》1992,13(6):825-840
Mode conversion at discontinuities of an ordinary gyrotron cavity is examined. It is shown how the production of unwanted spurious modes can be reduced substantially by introducing smooth transition regions between the individual parts of the cavity. The cavity of the 140 GHz KfK gyrotron operating in the TE10,4 mode is used as an example. Cavity and adjacent tapered output waveguide are optimized as a single unit. 相似文献
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An improved method including extraction procedures is presented for the analysis of nucleotides in suspension-cultivated animal cells. Quantification was performed by ion-pair high-performance liquid chromatography after perchloric acid extraction. It was found that the amount of perchloric acid taken for extraction influenced the yield and that cell washing procedures caused deterioration of the analysis results for triphosphates. More than thirty nucleotides and sugar-nucleotides were separated within 25 min using a Supelcosil reversed-phase column (3 microns) with tetrabutylammonium hydrogensulphate as pairing agent and methanol-pH gradient elution. Cultivated hybridoma cells showed variations in intracellular nucleotide concentrations as well as relative amounts during different growth phases, which could reflect the physiological state of a cell culture. 相似文献
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