通用组合型层析摄影反演

本文采用Ｂｅｓｓｅｌ函数与Ｚｅｒｎｉｃｋｅ函数组合的方式，编制了一通用的Ｔｏｍｏｇｒａｐｈｙ程序。它既可用于撕裂模磁岛结构的研究，又可用于杂质剖面的反演。结果说明，这种组合方式既有Ｂｅｓｓｅｌ函数的优点－在边界无毛齿，又有Ｚｅｒｎｉｃｋｅ函数的优点－在中心反演精度较高。     

[Na_4(H_2O)_7][Fe(OH)_6Mo_6O_(18)]: a new [12] metallacrown-6 structure with an octahedrally coordinated iron at the center

The reaction of an aqueous solution of sodium molybdate with iron powder at low pH (-0.184) gives rise to the formation of a six-member Mo ring-shape cluster with an Fe (II) encapsulated at the center, [Na4(H2O)7][Fe(OH)6Mo6O18](1), which is further linked to a remarkable three-dimensional network via sodium ions.     

环流器等离子体撕裂模稳定电流剖面

用分区拼接和局部平台化方法,得到m≠1撕裂模稳定的等离子体电流剖面,拟合了HL-1装置低q实验的电流剖面。     

无机阴离子对镍-4-〔(5-氯-2-吡啶)偶氮〕-1,3-二氨基苯显色反应的作用机理及应用研究

被试的六种无机钠盐对Ni~(2-)-5-Cl-PADAB显色体系有不同程度的增敏作用,并能提高显色反应的选择性。初步探讨了无机阴离子对显色反应作用的机理。已成功地将Ni~(2-)-5-Cl-PADAB-NaBr体系用于废水中镍的测定。     

同位素稀释高分辨气相色谱-高分辨质谱法检测烟道气中的低氯代二恶英

建立了同位素稀释高分辨气相色谱-高分辨质谱检测烟道气中痕量低氯代二恶英的分析方法。采用索氏提取富集烟道气样品中的目标物,提取液经过复合硅胶柱和碱性氧化铝柱净化后,进行高分辨气相色谱-高分辨质谱检测。采用DB-5MS毛细管色谱柱（30 m×0.25 mm×0.25 μm）分离,以保留时间和同位素特征离子丰度比定性,以与同位素的峰面积比值定量。实验结果表明,方法的回收率为66.6%~112.5%,相对标准偏差（RSD）的范围为19.9%~40.5%（n=5）,方法的检出限（LOD）为0.027~0.485 μg/L。应用该方法检测了3个焚烧炉烟道气样品,回收率在85.7%~137.0%范围内,样品中目标物含量分布在11.4~9183 pg/Nm³之间。结果表明该方法适合用于烟道气中痕量低氯代二恶英的检测。     

ON F-z-SUPPLEMENTED SUBGROUPS OF FINITE GROUPS

A subgroup H of a group G is called F-z-supplemented in G if there exists a subgroup K of G, such that G = HK and H∩K≤ Z∞F(G), where Z∞F(G) is the F-hypercenter of G. We obtain some results about the F-z-supplemented subgroups and use them to determine the structure of some groups.     

发动机被动液阻悬置动态特性比较研究

采用集总参数法和键合图法建立了惯性通道式、解耦盘惯性通道式以及节流盘解耦盘惯性通道式三种液阻悬置的动力学模型,建立了状态空间方程,获得了液阻悬置低频和高频的动态特性,对比分析认为惯性通道解耦盘式液阻悬置和节流盘解耦盘惯性通道式液阻悬置具有良好的频变幅变特性,而节流盘惯性通道解耦盘式液阻悬置拓宽了被动液阻悬置高频的使用频率,改善了惯性通道式和惯性通道解耦盘式被动液阻悬置高频的动态特性.     

Transformation from a low-dimensional framework to a high-dimensional architecture based on different metal ions: syntheses, structures, and photoluminescences

Five novel metal pamidronates (3-ammonium-1-hydroxypropylidene-1,1-bisphosphonate, APD) formulated as Ni2(C3NH10P2O7)4.4H2O (1), M(C3NH9P2O7).H2O (M = Co (2), Mn (3), Zn (4)) and Cu3(C3NH8P2O7)2.2H2O (5) have been hydrothermally synthesized under similar conditions. Compound 1 is a molecular binuclear nickel cluster. Compounds 2 and 3 exhibit similar one-dimensional ladderlike structures. Compound 4 possesses a novel two-dimensional gridlike framework. Compound 5 shows an unusual three-dimensional architecture, in which two-dimensional layers with a parquet motif are pillared by {CuO4} planar squares. Different dinuclear secondary building units (SBUs) are observed in compounds 1-5, depending on the different coordination modes of APD. They also exhibit different photoluminescence properties.