幂零群的若干充分条件

本文利用Ｃ－正规子群的性质，得到了若干有限群为幂零群的充分条件，推广了一些著名定理，如Ｔｈｏｍｐｓｏｎ定理及Ｉｔ＾ｏ定理。     

ADVANCES IN MICROEMULSION PHASE ON SELF-ASSEMBLY AND MICELLE EXTRACTION WITH BLOCK COPOLYMERS

In this paper we review our work on self-assembly of the system, poly（ethylene oxide）-poly（propylene oxide）-poly（elhylene oxide） （PEO-PPO-PEO） block copolymers, which is a kind of macromolecular complex fluids. The control of self-assembly could be obtained by adding inorganic salts or aliphatic alcohols. By self-assembly of amphiphilic block copelymers a microemulsion phase is formed which could be applied in micelle extraction, such as hollow-fiber membrane micelle extraction, magnetic micelle extraction and immobilized micelle extraction.     

开设"用光电法测量人体心率"实验的体会

介绍了开设“用光电法测量人体心率”设计选作实验的体会,指出注重培养学生的综合实验素质能力,不仅要求验证物理规律,更注重学以致用,引导学生运用所学知识解决实验问题,关注应用.     

Two New Constituents from the Soft Coral Nephthea hainansis

Two new compounds, namely 7α, 10α-dimethyl-3β-isopropene-1, 2-ene-octahydro-naphthalene (1) and ethyl 5Z,8Z, 11Z, 14Z-nonadecatetraenoate (2) were isolated from the soft coralNephthea hainansis. Compound 1 was a pseutosesquiterpene and 2 was a polyunsaturated fattyacid ethylate. Their structures were established on the basis of spectroscopic methods.     

On regression model selection for the data with correlated errors

A class of regression model selection criteria for the data with correlated errors is proposed. The proposed class of selection criteria is an estimator of weighted prediction risk. In addition, the proposed selection criteria are the generalizations of several commonly used criteria in statistical analysis. The theoretical and asymptotic properties for the class of criteria are established. Further, in the medium-sample case, the results based on a simulation study are quite consistent with the theoretical ones. The proposed criteria perform well in the simulations. Several applications are also given for a variety of statistical models.     

Discovery of New Natural Products by Intact‐Cell Mass Spectrometry and LC‐SPE‐NMR: Malbranpyrroles,Novel Polyketides from Thermophilic Fungus Malbranchea sulfurea

Six photosensitive polyketides, malbranpyrroles A–F, were discovered from the thermophilic fungus Malbranchea sulfurea by using intact‐cell desorption/ionization on silicon mass (ICD‐MS) and LC‐SPE‐NMR. These two strategies facilitate the searching and structural determination of unstable natural products. The ICD‐MS indicated that only brown hyphae of M. sulfurea can produce malbranpyrroles. The biosynthetic pathway of malbranpyrroles was evidenced by ¹³C isotope precursors and amino acid feeding experiments. The cytotoxicity data revealed that the conformation of the conjugated system in malbranpyrroles does not affect cytotoxic potency against cancer cell lines. In addition, the chlorine atom was shown to be the pharmacophore for cytotoxicity.     

基于传导变换的传导知识研究

基于传导变换的传导知识是一类重要的可拓知识.本文以传导变换和传导效应为基础,规定了传导度和传导知识的定义与类型,为研究传导知识的挖掘奠定理论基础.     

A novel tetranuclear copper(I) sulfanide complex with bis(diphenylphosphino)amine

The title novel mixed μ₂‐SH‐ and μ₃‐SH‐bridged tetranuclear copper(I) complex, cyclo‐bis[μ₂‐bis(diphenylphosphino)amine]di‐μ₃‐sulfanido‐di‐μ₂‐sulfanido‐tetracopper(I) methanol disolvate, [Cu₄(SH)₄(C₂₄H₂₁NP₂)₂]·2CH₃OH, has crystallographically imposed centrosymmetry and affords a neutral Cu₄S₄ core with a distorted step‐like structure. The distances of 2.8458 (16) and 2.8179 (16) Å between copper(I) centres indicate the presence of ligand‐supported Cu...Cu interactions. Strong N—H...O and O—H...S hydrogen bonds between the tetranuclear cluster and methanol solvent molecules result in a two‐dimensional hydrogen‐bonded supramolecular network. This complex is the first example of a coinage tetranuclear metal complex with mixed μ₂‐SH‐ and μ₃‐SH‐bridged chromophores.     

The effect of a single atom in the terminal position of a fluorocarbon chain on liquid crystalline properties

Eight series of chiral compounds with semi-fluorocarbon chains have been synthesized. The compounds were characterized by IR, ¹H NMR, ¹⁹F NMR and mass spectroscopies and elemental analysis. Their phase transition behaviour was investigated by differential scanning calorimetry and polarizing optical microscopy. Their clearing points increase with an increase of the length of fluorocarbon chain. For a certain compound, when the terminal hydrogen atom in the semi-fluoroalkyl chain was substituted by a chlorine atom, both the clearing point and melting point were increased, and the thermal stability of the chiral smectic C (SmC*) phase was enhanced. However, the clearing point decreased and the melting point increased with the introduction of a triple bond into the core.     

General Kloosterman Sums and the Difference Between an Integer and Its Inverse Modulo Q

The main purpose of this paper is to use the generalized Bernoulli numbers, Gauss sums and the mean value theorems of Dirichlet L-functions to study the asymptotic property of one class of number-theoretic functions, and to give four interesting hybrid mean value formulae.