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91.
Xiao‐Hui Liu Yan‐Guo Li Ying Lin Yue‐Sheng Li 《Journal of polymer science. Part A, Polymer chemistry》2007,45(7):1272-1281
The reversible addition–fragmentation chain transfer (RAFT) polymerization of acrylonitrile (AN) mediated by 2‐cyanoprop‐2‐yl dithiobenzoate was first applied to synthesize polyacrylonitrile (PAN) with a high molecular weight up to 32,800 and a polydispersity index as low as 1.29. The key to success was ascribed to the optimization of the experimental conditions to increase the fragmentation reaction efficiency of the intermediate radical. In accordance with the atom transfer radical polymerization of AN, ethylene carbonate was also a better solvent candidate for providing higher controlled/living RAFT polymerization behaviors than dimethylformamide and dimethyl sulfoxide. The various experimental parameters, including the temperature, the molar ratio of dithiobenzoate to the initiator, the molar ratio of the monomer to dithiobenzoate, the monomer concentration, and the addition of the comonomer, were varied to improve the control of the molecular weight and polydispersity index. The molecular weights of PANs were validated by gel permeation chromatography along with a universal calibration procedure and intrinsic viscosity measurements. 1H NMR analysis confirmed the high chain‐end functionality of the resultant polymers. © 2007 Wiley Periodicals, Inc. J Polym Sci Part A: Polym Chem 45: 1272–1281, 2007 相似文献
92.
基于爆轰波原理声源定位方法初探 总被引:5,自引:0,他引:5
基于弹丸发射时所发出的爆轰波,利用传感器接收时差信息,从而确定声源位置。本文建立了该声源定位反问题的物理和数学模型,并依据该模型寻求适当的数值解法,最后针对延拓-广义逆法声源定位问题进行了演算和简要分析。 相似文献
93.
物理实验课程考核、评估体系初探 总被引:4,自引:0,他引:4
对物理实验课程考核、评估方法进行了探讨,提出了物理实验课程考核、评估体系及实施细则.重点介绍了体系中的核心部分——正规的物理实验课程考试. 相似文献
94.
We investigate a spatial Prisoner's Dilemma game with nonlinear attractive effect on regular small-world networks. The players located on the sites of networks can either cooperate with their neighbours or defect. In every generation, each player updates its strategy by firstly choosing one of the neighbours with a probability proportional to .A^α denoting the attractiveness of the neighbour, where .4 is the collected payoff and ^α (-〉0) is a free parameter characterizing the extent of nonlinear effect. Then each player adopts its strategy with a probability dependent on their payoff difference. Using Monte Carlo simulations, we investigate the density pc of cooperators in the stationary state for various values of α and the rewiring probability q of the network. It is shown that the introduction of such attractive effect remarkably promotes the emergence and persistence of cooperation over a wide range of the temptation to defect for the same network structures. We also point out that long-range connections either enhance or inhibit the cooperation, which depends on the value of α and the payoff parameter b. 相似文献
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98.
The compound binomial risk model with time-correlated claims 总被引:1,自引:0,他引:1
Yuntao Xiao 《Insurance: Mathematics and Economics》2007,41(1):124-133
In this paper, we consider the compound binomial risk model with the time-correlated claims. It is assumed that every main claim will produce a by-claim but the occurrence of the by-claim may be delayed. We obtain the recursive formula of the joint distribution of the surplus immediately prior to ruin and deficit at ruin. Furthermore, the ruin probability is given by means of ruin probability and the deficit at ruin of the classical compound binomial risk model. Finally, we derive an upper bound for the ruin probability. 相似文献
99.
本篇文章首先定义了向量变分不等式的严格可行点概念,其次在假设了映射是强(D)-伪单调的情况下,证明了向量变分不等式解集非空有界与其严格可行点存在的等价性问题,推广了在数量变分不等式上得到的相应结果. 相似文献
100.
提出了一种基于模型驱动的元数据管理方案.方案采用了基于模型的形式化描述方法,统一了专业网管子系统间的元数据模式;通过引入模型驱动技术,从元模型的抽象层次消除了不同专业网管子系统之间存在的“信息孤岛”;方案还对综合网管环境下的元数据理论和交换机制进行了研究,并给出了元数据的管理框架以及元数据交换的Java接口映射. 相似文献