A Concise and Stereoselective Synthesis of the Cathasterone''''s Side Chain

A concise and stereoselective synthesis of cathasterone's side chain using methyl isopropyl ketone 3 as the fragment is described.     

GM（1，1）模型的样条插值函数的残差拟合

本文用样条函数对GM(1，1)模型的残差序列进行插值拟合，然后作用于二阶线性微分方程，并以此修正原模型，得到一种新的预测模型的数值解．     

向量集值优化超有效解的对偶问题

借助于Contingent切锥和集值映射的上图而引入的有关集值映射的Contingent切导数，对约束集值优化问题的超有效解建立了最优性Kuhn Tucker必要及充分性条件,借此建立了向量集值优化超有效解的Wolfe型和Mond Weir型对偶定理.     

Digital phase shift holographic interferometry and its application in the experimental flow study

The application of digital phase shift holographic interferometry to flow-visualization and flow temperature measurement of a 2D thermal flow field was experimentally investigated. An improved recording system for two reference beam phase shift holographic interferometry is set up for this experiment, and details of this experimental technique are described. The phase distribution obtained by this technique presents an excellent picture of flow visualization. From this phase image, temperature distribution of the 2D thermal flow field is also calculated and compared with some measured values obtained using thermocouple probes.     

Preparation of side‐on bisazobenzene‐containing homopolymers and block copolymers via ATRP and studies on their photoisomerization and photoalignment behaviors

The preparation of a series of novel homopolymers and copolymers containing bisazobenzene chromophores with side‐on structure in the side chains via atom transfer radical polymerization (ATRP) were presented. UV–vis spectra of the thin films of these polymers under irradiation of 488 nm Ar⁺ laser suggested that the photoisomerization of the bisazobenzene chromophores happened mainly on one of the two azo groups in the bisazobenzene chromophores with similar probability due to their side‐on structure. Good photoalignment behaviors of these polymers were proved by photoinduced birefringence measurements because side‐on structure permitted the two azo groups in the bisazobenzene chromophores both participated in the trans–cis–trans photoisomerization cycles equally to induce the whole chromophore reorientation. Furthermore, the reorientation axis located at the middle of chromophore decreased the sweep volume during photoalignment. The impetus for this study was to evaluate the photoisomerization and photoalignment process of side‐on bisazobenzene‐containing polymers and to find possible applications in the photosensitive devices. © 2007 Wiley Periodicals, Inc. J Polym Sci Part A: Polym Chem 45: 3460–3472, 2007     

Reactions of [60]Fullerene with Di(azidomethyl) benzenes

Alargenumberofadditionsto[6O]fullerenehavebeeninvestigated.However,mostoftheworkhaveconcentratedontheformationofthemono-additionproductS0f[60]fullerene'-Thedevelopment0fselechveroutestomultipleadductShascurrentlybecomethefrontierinthechendstryof[60]fuIlerene'~'.FollowingtheaPplicahonoftether-directedremotefunctionalizati0ntotheregi0specificformati0nofthedi-andtriadductSof[60]fullerene,F.Diederichetal6alsodescribed'awayforthedirectdifunctionalizationof[60]fullerenebasedonacyclizationreachono…     

城市环境铅污染状况研究

介绍了邢台近１０年来环境灰尘，土壤，地面水，地下水，大气及部分作物的铅污染和累积状况，并分析了产生原因及影响。     

解非线性约束拟凸规划的一个梯度投影法

目前国内外所流行的梯度投影法(包括Rosen的原有算法和一些修正算法)还存在以下几个问题:一、要增加Polak程序以保证算法的收僉性。二、在计算投影梯度时,每步一般要作两次投影。三、对于非线性约束问题,负梯度投影方向是不可行的,因此必须在此方向的基础上构造出能保证算法收歛的新可行下降方向。而目前为构造出这个新方向所作的计算都比较复杂。 1981年[5]提出了一个处理线性约束条件的梯度投影法,基本上解决了线     

Singular Integrals in Several Complex Variables (I)—Henkin Integrals of Strictly Pseudoconvex Domain

对于多复变数强拟凸域的Henkin-Ramirez核或Stein-Kerzman核所定义的Cauchy型积分，本文指出：可以有多种形式的Plemelj公式，甚至Cauchy型积分的极限值可以等于某种Cauchy主值，这些都显示了多复变数函数与单复变数函数本质上的不同。