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41.
Dutra JC da C Terzi S Bevilaqua JV Damaso MC Couri S Langone MA Senna LF 《Applied biochemistry and biotechnology》2008,147(1-3):63-75
The aim of this study was to monitor the biomass growth of Aspergillus niger in solid-state fermentation (SSF) for lipase production using digital image processing technique. The strain A. niger 11T53A14 was cultivated in SSF using wheat bran as support, which was enriched with 0.91% (m/v) of ammonium sulfate. The addition of several vegetable oils (castor, soybean, olive, corn, and palm oils) was investigated
to enhance lipase production. The maximum lipase activity was obtained using 2% (m/m) castor oil. In these conditions, the growth was evaluated each 24 h for 5 days by the glycosamine content analysis and digital
image processing. Lipase activity was also determined. The results indicated that the digital image process technique can
be used to monitor biomass growth in a SSF process and to correlate biomass growth and enzyme activity. In addition, the immobilized
esterification lipase activity was determined for the butyl oleate synthesis, with and without 50% v/v hexane, resulting in 650 and 120 U/g, respectively. The enzyme was also used for transesterification of soybean oil and ethanol
with maximum yield of 2.4%, after 30 min of reaction. 相似文献
42.
Analysis of underivatized cellodextrin oligosaccharides by capillary electrophoresis with direct photochemically induced UV‐detection
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Elodie Alinat Selma Jemmali Nathalie Delaunay Xavier Archer Pierre Gareil 《Electrophoresis》2015,36(14):1555-1563
This work focuses on the development of a CE method allowing, for the first time, the simultaneous separation of the underivatized first seven cellodextrin oligomers (glucose, cellobiose, cellotriose, cellotetraose, cellopentaose, cellohexaose, and celloheptaose), with a view to analyze the hydrolysates obtained after partial acid depolymerization of nitrocellulose, and eight carbohydrates (ribose, xylose, fructose, mannose, galactose, maltose, lactose, and sucrose), which might be potential interfering compounds in explosives samples. Separation was achieved with a highly alkaline BGE containing sodium chloride and direct mid‐UV‐absorbance detection was performed after photo‐oxidation in the detection window. EOF was reversed to speed up the analysis using a dynamic capillary coating by hexadimethrine bromide. A central composite design was carried out to determine the effects of BGE conductivity and sodium hydroxide concentration on resolutions between neighboring peaks, and analysis time. A desirability analysis on modeled responses was applied to maximize resolutions and to minimize analysis time. The simultaneous analysis in 20 min total runtime of the 15 carbohydrates plus internal reference (naphthalene sulfonate) was carried out at 25°C with a BGE composed of 77.4 mM NaOH and 183 mM NaCl to adjust the conductivity at the optimum value. Finally, the resolution robustness was checked. This new method should also be of interest to monitor food and nonfood crop products. 相似文献
43.
This paper presents new definitions which are a natural combination of the definition for asymptotically equivalence and Δ m -lacunary strongly summable with respect to a modulus f. Using this definitions we have proved the (f, Δ m )-asymptotically equivalence and Δ m -lacunary statistical asymptotically equivalence analogues of theorems of Tripathy and Et (Stud Univ Babe?-Bolyai Math (1):119–130, 2005) and Çolak’s theorems (Filomat 17:9–14, 2003). 相似文献
44.
Working within a plain texture (S,S), the authors construct a completion of a dicovering uniformity υ on (S,S) in terms of prime S-filters. In case υ is separated, a separated completion is then obtained using the T0-quotient, and it is shown that this construction produces a reflector. For a totally bounded di-uniformity it is verified that these constructions lead to dicompactifications of the uniform ditopology. A condition is given under which complementation is preserved on passing to these completions, and an example on the real texture (R,R,ρ) is presented. 相似文献
45.
Analysis and Review of Chemical Reactions and Transport Processes in Pulsed Electrical Discharge Plasma Formed Directly in Liquid Water 总被引:1,自引:0,他引:1
Electrical discharges formed directly in liquid water include three general cases where (a) streamer-like plasma channels form in, but do not span, the electrode gap, (b) spark discharges produce transient plasma channels that span the electrode gap, and (c) arc discharges form plasma channels with relatively longer life times. Other factors including the input energy (from <1?J/pulse to >1?kJ/pulse) as well as solution properties and the rates of energy delivery affect the nature of the discharge channels. An understanding of the formation of chemical species, including the highly reactive hydroxyl radical and more stable molecular species such as hydrogen and hydrogen peroxide, in such plasma requires determination of temporal and spatial variations of temperature, pressure, plasma volume, and electrical characteristics including current, voltage (electric field), and plasma conductivity. In spark and arc discharges analysis of the physical processes has focused on hydrodynamic and thermal characterization, while only a limited amount of work has connected these physical processes to chemical reactions. On the other hand, the most successful model of the chemical reactions in streamer-like discharges relies on simple assumptions concerning the temperature and pressure in the plasma channels, while analysis of the physical processes is more limited. This paper reviews the literature on the mathematical modeling of electrical discharges in liquid water spanning the range from streamer-like to spark and arc discharges, and compares the properties and processes in these electrical discharges to those in electron beam radiolysis and ultrasound. 相似文献
46.
Luis Alberto Domingo Francia-Farje Camila Contin Diniz Almeida-Francia Selma Maria Michelin Matheus Marcia Miranda Torrejais Jair de Campos Soares 《Micron (Oxford, England : 1993)》2009,40(7):691-701
Although the myotendinous junction (MTJ) of skeletal striated muscle is well known, more detailed studies regarding the structure of the cardiac MTJ are scarce. The objective of the present study was to investigate the morphological characteristics of the MTJ in hearts of healthy and hypertensive (SHR) female rats using histological, ultrastructural and three-dimensional (SEM) methods, as well as to evaluate the expression of vinculin by immunofluorescence. In the two groups, light microscopy showed branching tendinous cords and collagen bundles penetrating the apex of the finger-like projections of the papillary muscle. SEM analysis revealed an enlarged apex of the papillary muscle in SHR which was not observed in healthy animals. The loss of force transmission appears to be compensated by the amplified connection between the papillary muscle and valvular collagen. A large number of intercalated disks close to the fiber apex, small amounts of an amorphous intercellular substance and numerous vesicles were observed in SHR. In these animals, the expression of vinculin was more marked showing a regular distribution and a pattern of transverse striations along the sarcolemma. The presence of this protein in transverse bands suggests that vinculin surrounds myofibrils in the region of the Z band. Vinculin staining was also more marked in the region of the tendinous cord–papillary muscle junctions of SHR compared to control animals. Vinculin was quantified by electrophoresis and higher amounts of this protein were observed in SHR compared to control animals. 相似文献
47.
Siéssere S Vitti M Semprini M Regalo SC Iyomasa MM Dias FJ Issa JP de Sousa LG 《Micron (Oxford, England : 1993)》2008,39(7):852-858
In order to obtain a precise diagnosis and treatment for temporomandibular dysfunctions, it is necessary to have morphological and functional knowledge of the temporomandibular joint. Anatomic components are important to the understanding of the complexity of temporomandibular joint. Nonetheless, just as important are the anatomic relationships that this joint has with the neighboring structures. Thus, the aim of this study was to present the anatomic relationships of the temporomandibular joint in its various surfaces: external or lateral, anterior, posterior, medial, superior, and posterosuperior, considering the morphological and histological aspects. Nine human heads, fixed in formalin (10%) underwent sagittal medial section and were subsequently dissected, evidencing the anatomic components of all surfaces to be analyzed. Components of the external surface were: skin, subcutaneous tissue, lymphatic ganglia, parotid gland, superficial temporal artery, transverse facial artery, zygomatic-orbital artery, superficial temporal vein, facial and auriculotemporal nerves, masseter muscle, and pre-auricular lymphonodus. The anterior surface comprised the masseter and lateral pterygoid muscles (upper and inferior heads), pterygoid venous plexus, mandibular notch, posterior deep temporal artery, masseteric nerve, and deep posterior temporal branches. Medial surface components were: internal maxillary artery, of which middle meningeal artery was one of the closest branches to the TMJ, anterior tympanic artery, inferior alveolar, lingual, auriculotemporal, and chorda tympani nerves, which belonged to the surface posterior to the anterior wall of the auditory duct; auricolotemporal nerve, parotid gland; and petrotympanic fissure. The cerebral fossa (meninges and encephalon) belonged to the superior surface and the ear belonged to the posterosuperior surface. Histologically, the temporomandibular joint is composed by different tissues that compound the mandibular head, mandibular fossa, and articular eminence of the temporomandibular joint. It was concluded that the temporomandibular joint is a complex structure and the clinician must have the ability to formulate the diagnosis based on the understanding of morphological aspects of the structures that compose the stomatognatic system. 相似文献
48.
AL-Jawad Selma M. H. Imran Natheer Jamal Aboud Kahlaa H. 《Journal of Sol-Gel Science and Technology》2021,100(3):423-439
Journal of Sol-Gel Science and Technology - Mn-CdS nanoflowers were successfully deposited using hydrothermal technique at 150 °C for 2 h. The effect of changing the dopant... 相似文献
49.
Shakir Zahraa S. AL-Jawad Selma M. H. Ahmed Duha S. 《Journal of Sol-Gel Science and Technology》2021,100(1):115-131
Journal of Sol-Gel Science and Technology - In recent years, cobalt attracted large interest in biological application, due to its biocompatibility and low toxicity. The synthesis of Co... 相似文献
50.
V. Heiman J. S. Carver Selma L. Bandemer Ph. J. Schaible G. Nadai und W. Schut 《Fresenius' Journal of Analytical Chemistry》1937,110(1-2):50-51
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