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51.
M. Aneesuddin P. N. Char M. Raza Hussain E. R. Saxena 《Journal of Thermal Analysis and Calorimetry》1983,26(2):205-215
When chalcopyrite is heated in air, up to 350? there is no marked change. Between 350 and 440?, surface material is oxidised to iron sulphate, CuSO4 and Fe2O3, while in regions not accessible to oxygen the formation of Cu5FeS4, FeS and S takes place. From 440 to 500? oxidation and sulphation phenomena occur. Stable compounds between 500 and 650? are iron sulphate, CuSO4 and Fe4O3, with a minor amount of 6CuO.Cu2O indicated at 650?. After the decomposition of iron sulphate, CuSO4 decomposes, first to CuO.CuSO4 and then to CuO. By 750? the sulphur has been totally lost from all compounds, while the oxides of copper and iron partly react to form CuFe2O4. Final products of oxidation between 800 and 850? are CuO, CuFe2O4 and Fe3O4. 相似文献
52.
The reaction of 1H‐indol‐2,3‐diones with 1,6‐dibromohexane has resulted in the formation of new 1H‐indol‐2,3‐diones‐1,1′‐(1,6‐hexanediyl)bis in quantitative yields. These compounds have been used for the synthesis of novel [3′‐(2,3‐dimethyl‐5‐oxo‐1‐phenyl‐3‐pyrazolin‐4‐yl)spiro[3H‐indol‐3,2′‐thiazolidine]‐2,4′‐dione]‐1,1′‐(1,6‐hexanediyl)bis via bis Schiff's bases, [3‐(2,3‐dimethyl‐5‐oxo‐1‐phenyl‐3‐pyrazolin‐4‐yl) imino‐1H‐indol‐2‐one]‐1,1′‐(1,6‐hexanediyl)bis. 相似文献
53.
The electrical conductivity of polyvinylidenefluoride (PVDF) – polysulfone (PSF) blend films have been measured by studying the I–V characteristics in the temperature range of 298–398 K. The results are shown by measuring the dependence of current on field, temperature, and blending compositions in the form of I–V characteristics and analysis has been made by interpretation of Poole–Frenkel, Schottky ln (J) vs. T plots, Richardson and Arrhenius plots. For individual polymers, the conduction mechanism observed to be a Poole–Frenkel type. On blending, the charge conduction appears to be the Schottky emission at lower temperature while Poole–Frenkel mechanism at higher temperature. The analysis of these results suggests that Pool–Frenkel mechanism is mainly responsible for the observed conduction. The conductivity was found to increase with an increase in the polysulfone concentration in the blend; it could be justified in terms of mobility of charge carriers. It is found that mobility of charge carriers increases with the increase in polysulfone concentration in the blend. 相似文献
54.
R. Khare P.K. Shukla G.K. Mishra C. Mukherjee S. Talwar V.K. Dubey P. Saxena J.K. Mittal 《Optics Communications》2009,282(19):3850-3853
We present an analytical and experimental study of a novel confocal optical pulse stretcher (COPS). The simple and passive pulse stretcher consists of two concave mirrors and a scraper beam-splitter and its optical configuration ensures a perfect spatial overlapping of laser pulses at the beam-splitter. The pulse stretcher is compact and suitable for laser pulses of large divergences. The confocal optical pulse stretcher is demonstrated on a pulsed copper vapour laser to convert a 40 ns (1/e2 % points) pulse into a 55 ns with reduction of peak power by a factor of 1.375 without loss of pulse energy. 相似文献
55.
Time-dependent photoexcitation and optical spectroscopy of pi-conjugated molecules is described using a new method for the simulation of excited state molecular dynamics in extended molecular systems with sizes up to hundreds of atoms. Applications are made to poly(p-phenylene vinylene) oligomers. Our analysis shows self-trapping of excitations on about six repeat units in the course of photoexcitation relaxation, identifies specific slow (torsion) and fast (bond-stretch) nuclear motions strongly coupled to the electronic degrees of freedom, and predicts spectroscopic signatures of molecular conformations. 相似文献
56.
Latent damage tracks of energetic40Ar ions (18·56 MeV/u) have been recorded in Lexan polycarbonate detector. Bulk and track-etch parameters are evaluated under successive chemical
etching. Our results show a linear correlation between the measured track-etch rate along the track and the corresponding
total energy-loss rate and predict a threshold value of 5·0 MeV mg−1 cm2 for track registration. Maximum etchable track lengths of40Ar ions as a function of energies have also been measured and compared with three different sets of theoretical ranges. 相似文献
57.
Saxena Poonam T. K. Bandopadhyaya 《International Journal of Infrared and Millimeter Waves》1998,19(3):503-509
For any communication service operating in the Microwave/ Millimeter wave region, statistical information characterising the attenuation due to rain along satellite slant path would be required for the design of satellite communication links and for the broadcasting network above 20 Ghz. It is necessary to have a prior knowledge of the probability of exceeding different levels of rain attenuation in order to design appropriate fade margins into systems and establishing estimates of the year to year variability of rain fade margin for particular geographic regions of India so that the communication system reflects the extremes of these variabilities. Direct measurement of beacon signals from geostationary satellites have been a mean to determine the above information and experiments can be pursued with satellite such as INSAT. [1]Attenuatiuon of Millimeter Waves by rainfall restricts the path length of a communication system. A knowledge of the rain attenuation at such frequencies is therefore desirable in designing a reliable communication system. Signal level fading over line-of-sight links strongly depends on the hop length, frequency and climate. For short hops, the probability of occurance of deep fades becomes diminishingly small. However, since an extended hop length is possible for regions with little rain activity, clear weather fading can affect the link reliability in a similar way ti a rain.[2] 相似文献
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