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251.
Comparison of three sequential extraction procedures to describe metal fractionation in anaerobic granular sludges 总被引:2,自引:0,他引:2
In the last few decades, several sequential extraction procedures have been developed to quantify the chemical status of metals in the solid phase. In this study, three extraction techniques (modified [A. Tessier, P.G.C. Campbell, M. Bisson, Anal. Chem. 51 (1979) 844]; [R.C. Stover, L.E. Sommers, D.J. Silvera, J. Water Pollut. Con. F. 48 (1976) 2165]; and the Bureau Communautaire de Reference (BCR) [K.F. Mossop, C.M. Davidson, Anal. Chim. Acta 478 (2003) 111]) were applied to study the distribution of trace (Co, Ni, Zn and Cu) and major (Mn and Fe) elements in two different anaerobic granular sludges from full-scale methanogenic wastewater treatment plants. The Stover scheme displayed a higher number of fractions that induces a poor recovery compared to the other schemes. The sequential extraction scheme recommended by BCR and the modified Tessier scheme gave similar trends and are sufficiently repeatable and reproducible for application in fractionation studies. However, the BCR scheme seems to be of limited utilisation to study anaerobic matrixes because the extraction stage for its reducible fraction may release substantial amounts of trace elements bound to the organic/sulfides fraction, and consequently, the recovery of trace elements in the oxide fraction may be overestimated at the expense of the oxidisable fraction. As a final conclusion, the modified Tessier scheme seems to be the most suitable scheme to study the metal partitioning in anaerobic granular sludges. 相似文献
252.
253.
Marcel Coz 《Journal of Mathematical Analysis and Applications》1983,92(1):66-95
Using Marchenko's own method, it is shown that three elements are required for the existence of a Marchenko fundamental equation. These are a convergent sum over the discrete spectrum, a bounded translation operator, and sometimes when there are “spectral singularities,” a domain in the complex plane of the momentum k where the representation of the regular solution as a linear combination of the two Jost solutions is meaningful. Meanwhile, we prove that for a class of complex potentials that will be called regular, a variant of Marchenko's equation exists. Clarification of the relationship between the completeness of the two sets of solutions for the unperturbed and the perturbed equation on one hand and the existence of a fundamental equation on the other hand is also achieved. 相似文献
254.
255.
Marcel Evrard 《Mathematische Zeitschrift》1979,166(3):277-288
Sans résumé 相似文献
256.
In the course of electrophilic cyclisation attempts, o-phenyltellurobenzoyl-chloride did not cyclise to telluroxanthone. but isomerised to 2-chloro tellurobenzophenone through intramolecular carbodetelluration. A breaking of the same Caromatic-Te bond is also realized by protonolysis. This last reaction leads to a preparative method of synthesis of ditellurosalicylic acid, a starting material for synthesis of benzocondensed tellurium heterocycles. 相似文献
257.
Even companies with large advertising budgets are sceptical of OR models in advertising—such models often appear overly complex, unrealistic and costly to use. Here a simple econometric model is proposed which utilises existing company data. The parameters are estimated for the five leading brands in a sector of the German alcoholic drinks market. Estimates of the short and long run advertising elasticities are made and optimum advertising appropriations are calculated. 相似文献
258.
Leopold Laitem Leon Christiaens Marcel Renson 《Magnetic resonance in chemistry : MRC》1980,13(5):319-322
An important 13C NMR shielding effect on carbons bearing a heavy chalcogen is demonstrated. This effect is parallel to that induced by iodine, but to a lesser extent. For acyclic compounds and for partially saturated heterocycles, there is an excellent linear correlation between the 13C chemical shifts of carbons bearing a chalcogen and carbons bearing a halogen atom in the corresponding compound. The linearity of the relationship is less satisfactory with heteroaromatic compounds. 相似文献
259.
Horminone, taxoquinone and other royleanones, obtained from two Abyssinian Plectranthus species (Labiatae). From the coloured glands on the leaves of two botanically unclassified Plectranthus sp. from Abyssinia, a series of royleanones has been isolated, namely royleanone ( 1 ) and 6,7-dehydroroyleanone ( 2 ) from one species, and 6,7-dehydroroyleanone, horminone ( 3 ), taxoquinone ( 4 ), 6β, 7α-dihydroxyroyleanone ( 5 ), 7α-acetoxy-6β-hydroxyroyleanone ( 6 ) and 7-oxoroyleanone ( 7 ) respectively, from the other. 相似文献
260.