Synthesis and some chemical transformations of 1-N-(β-hydroxyethyl)-3,6-dimethyluracil

Conclusions A study was made of the synthesis and some of the chemical transformations of 1-N-(-hydroxyethyl)-3,6-dimethyluracil.Translated from Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, No. 2, pp. 422–428, February, 1972.     

A study of the anthocyanins of hibiscus hybrids

Chemistry of Natural Compounds -     

Synthesis and properties of silacyclobutylsilazanes

Ammonolysis of silacyclobutanes {ie305-01} (R=Cl, CH₃) gives silacyelobutane di- and polysilazanes. Reaction of the disilazane {ie305-02} with 1-chloro-1-methyl-1-silacyelobutane at 20–80° gives a trisilyl-substituted amine {ie305-03}. Trisilyl-substituted amines with one silacyclobutyl group, are obtained by reacting silacyclobutanes {ie305-04} (R=CH₃, C₆H₅). with sodium or potassium silylamides prepared from hexamethyldisilazane. It is shown that it is possible to obtain silylamides by reacting disilazanes directly with potassium metal at 90–100°.     

Aggregation des menschlichen Serumalbumins unter den Bedingungen der W ärmedenaturierung

Ohne Zusammenfassung     

Gravimetric determination of zirconium with a new azopyrazolone derivative

3-Methyl-5-oxo-1-phenyl-2-pyrazolin-4-ylazo-2'-(6',8'-naphthalenedisulfonic acid) (disodium salt) is proposed as a new reagent for the gravimetric determination of zirconium. The precipitate formed at pH 1–1.5 can be weighed directly and there are few interferences.