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991.
Thomasser Christiane Danner Herbert Neureiter Markus Saidi Bamusi Braun Rudolf 《Applied biochemistry and biotechnology》2002,98(1-9):765-773
Lignocellulosic biomass has great potential as a cheap feedstock in biological processes to produce biofuels or chemicals;
however, dilute acid pretreatment at high temperatures produces undesirable compounds. Toxicity tests were done with inhibitors
in standard media, to predict the growth-limiting effects on thermophilic strains. The 22 inhibitors included furfural, levulinic
acid, acetic acid, and cinnamaldehyde. Neutralizing reagents and additional treatment steps have been tested. 相似文献
992.
R. Bugoi V. Cojocaru B. Constantinescu F. Constantin D. Grambole F. Herrmann 《Journal of Radioanalytical and Nuclear Chemistry》2003,257(2):375-383
Several fragments of ancient gold objects coming from an Eneolithic hoard and from Pietroasa Cloca cu Puii de Aur (The Golden Brood Hen with Its Chickens) hoard, unearthed on Romanian territory, and two Romanian native gold nuggets samples were analyzed using micro-PIXE technique. The purpose of the study was to clarify the metal provenance. Trace and minor elements (Cu, Te, Sn, Pb, Ti, Cr, V, Mn, Ta) and platinum group elements (PGE) concentrations were estimated. The presence of inclusions (micrometer size areas of composition different from the surroundings) was investigated. We found Si and Ca inclusions on two Eneolithic samples, and Ta inclusions on two samples from Pietroasa hoard. The measurements suggested an alluvial origin of gold for the Eneolithic samples and give indications for the possible gold ore sources of Pietroasa hoard. 相似文献
993.
Andreas Hofer und Rudolf Heidinger 《Fresenius' Journal of Analytical Chemistry》1969,246(2):125-126
Zusammenfassung Eine für die Bestimmung von 0,05–0,25% Vanadium in Eisenerzen geeignete Methode wird beschrieben. Vanadium wird in der Siedehitze in etwa 1,8 N schwefelsaurer Lösung mit 0,1 N Kaliumpermanganat vollständig zur fünfwertigen Stufe oxydiert. Anschließend wird zur selektiven Extraktion von Vanadium(V) mit einer 0,1%igen Lösung von N-Benzoyl-N-phenylhydroxylamin in Chloroform ausgeschüttelt. Die Extinktion des violett gefärbten Extraktes wird bei 530 nm spektralphotometrisch gemessen.
Contribution to the extractive-photometric determination of small amounts of Vanadium in iron ores employing N-benzoyl-N-phenylhydroxylamine
A method suitable for the determination of 0.05–0.25% of vanadium in iron ores is described. Vanadium is quantitatively oxidised to the pentavalent state in a boiling solution approximately 1.8 N in sulphuric acid by 0.1 N potassium permanganate. Vanadium(V) is then selectively extracted from the sample solution by a 0.1% solution of N-benzoyl-N-phenylhydroxylamine in chloroform. The extinction of the violet coloured extract is measured spectrophotometrically at 530 nm.相似文献
994.
Brigitte Gutsche und Roland Herrmann 《Fresenius' Journal of Analytical Chemistry》1971,253(4):257-262
Zusammenfassung Der von früheren Untersuchungen her bekannte In-Brenner für den spezifischen Chlor(359,9 nm) und Brom-(327,7 nm)Nachweis wird in dieser Arbeit für den spezifischen Jod-Nachweis bei 409,9 nm benützt. Es wird gezeigt, daß man mit einem solchen Detektor in günstigen Fällen das Auflösungsvermögen eines GC verbessern kann. Nach vorangegangener Eichung sind Aussagen darüber möglich, wieviel Jod in den einzelnen GC-Fraktionen enthalten ist. Die Nachweisgrenzen des Verfahrens liegen zwischen 0,01–1,4 g Jod.
Unterstützt mit Mitteln der Deutschen Forschungsgemeinschaft. 相似文献
Iodine-specific detector for a gas chromatograph
The In-flame detector earlier applied to the specific chlorine (359.9 nm) and bromine (372.7 nm) analysis has now been employed for the iodine determination at 409.9 nm. It is shown that the resolution power of a GC column can be improved by such a specific detector. After calibration quantitative measurements of the iodine contents of the GC fractions are possible. The detection limits are 0.01–1.4 g of iodine.
Unterstützt mit Mitteln der Deutschen Forschungsgemeinschaft. 相似文献
995.
(DAPM). The use of DAPM as a spectrophotometric reagent for the determination of titanium in aluminium and aluminium alloys was investigated. To the solution, 0.5 N in hydrochloric acid, a 2% solution of DAPM in 0.5 N hydrochloric acid is added to form the yellow complex of titanium(IV) with DAPM. The addition of 20% solution of tin(II)chloride in 0.5 N hydrochloric acid yields a yellow precipitate, which is extracted by chloroform. The absorbance of the extract is measured at 390 nm. 0.01–0.1% of titanium have been determined in pure aluminium and Al-Mg-Zn alloys by the method suggested (standard deviation ±0.0004 to 0.0008%). 相似文献
996.
997.
998.
999.
Let (A,M) be a noetherian local ring. For certain equimultiple ideals I in A we try to relate the Gorenstein property of the Rees algebran and of A itself. In particular we n0 treat the case of equimultiple prime ideals of height two and the case I=M. The results underscore a natural conjecture, s. Thm. 2.6. and 3.2. 相似文献
1000.
Rudolf Scharlau 《Geometriae Dedicata》1987,24(1):77-84
Following earlier work of Tits [8], this paper deals with the structure of buildings which are not necessarily thick; that is, possessing panels (faces of codimension 1) which are contained in two chambers, only. To every building , there is canonically associated a thick building
whose Weyl group W(
) can be considered as a reflection subgroup of the Weyl group W() of . One can reconstruct from
together with the embedding W(
) W(). Conversely, if
is any thick building and W any reflection group containing W(
) as a reflection subgroup, there exists a weak building with Weyl group W and associated thick building
. 相似文献