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非水溶液浸渍法制备TiO2—Al2O3 总被引:1,自引:0,他引:1
二氧化钛用作石油炼制的加氢脱硫(HDS)或加氢脱氮(HDN)催化剂载体具有高的活性,其缺点是比表面小,机械强度差。为克服这些缺点,近年来研究了用共胶法、浸渍法和交替成胶法制备TiO_2-Al_2O_3载体。本文报道了以TiCl_4的CCl_4溶液作浸渍液,制备单层覆盖型TiO_2-Al_2O_3载体,并用多晶X光衍射(XRD)、X光光电子能谱(XPS)、透射电子显微镜(TEM)和选区电子衍射(HEED)等实验技术进行了表征。 相似文献
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本文研究了Pr1.27La0.7Ce0.03CuO4和Pr2CuO4单晶的低温热导率行为,在极低温下热导率(κ)随磁场的变化显示出低场下的凹陷和高场下的平台现象.这种现象很可能是顺磁离子散射声子的作用引起的,在Pr2CuO4单晶的比热测量结果中,肖特基峰随磁场的变化关系表明样品中确实含有少量的顺磁离子,并且其零场下基态能级存在劈裂.因此,这些顺磁离子很可能是Pr4+离子.该结果表明铜氧化合物高温超导体中声子与自旋的强烈耦合作用. 相似文献
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LU RuiJing & LIANG EnWei Physical Science & Technology College Guangxi University Nanning China 《中国科学:物理学 力学 天文学(英文版)》2010,(1)
Using time-resolved spectral data for a sample of 30 pulses in 27 bright GRBs detected with CGRO/BATSE, we investigate the luminosity-peak energy relation (L-E p relation) in the decay phases of these pulses. A tight L-E p relation is found for most of the pulses, but its power law index is various among pulses, which is normally distributed at 1.84±0.60(1σ) for the pulses in our sample, roughly consistent with the L-E p relation within a GRB and the isotropic gamma-ray energy-E p relation among GRBs. The large scatter of the power law index cannot be explained with both the statistical or observational effects and it may be an intrinsic feature, indicating that no universal L-E p relation would be expected among GRBs/pulses. This may strongly weaken the cosmological use of this relation. 相似文献
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The physico-chemical properties of organized assemblies (micelle or vesicle ) from sodium alkylcarboxylate - alkyltrimethyl -ammonium bromide mixture have been investigated systematically. In different mixed cationic-anionic surfactant systems, micelles and vesicles can coexist or be transformed into each other on different conditions. The experimental results are explained prelimilarily from the viewpoint of molecular packing geometry. The solubilization of organic compound in the mixed surfactant system was also studied in detail. 相似文献
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Kh.S.Karimov Khaulah Sulaiman Zubair Ahmad Khakim M.Akhmedov A.Mateen 《中国物理 B》2015,24(1):18801-018801
We report newly designed pressure and displacement capacitive sensors based on a flexible paper–CNT structure.The carbon nanotube(CNT)powder was deposited on a thin paper substrate and was pressed at an elevated temperature.The sheet resistance of the paper–CNT films was in the range of 2–4 kΩ/cm2.The paper–CNT films were used to fabricate pressure and displacement sensors.The sensitivities of the pressure and the displacement sensors were found to be17.3 p F·m2/k N and 0.93 10-3p F/μm,respectively.The experimental results were compared with the simulated data and they found good agreement with each other. 相似文献
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V. V. Lunin G. M. Kuramshina L. V. Vikov N. E. Kuz’menko The editorial board editorial staff of The Russian Journal of Physical Chemistry share in these wishes congratulations. 《Russian Journal of Physical Chemistry A, Focus on Chemistry》2006,80(8):1355-1355
Chronicle
Igor’ Alekseevich Myasnikov (1918–2005) 相似文献38.
V. V. Lunin G. M. Kuramshina L. V. Vikov N. E. Kuz’menko The editorial board editorial staff of The Russian Journal of Physical Chemistry share in these wishes congratulations. 《Russian Journal of Physical Chemistry A, Focus on Chemistry》2006,80(2):313-313
Chronicle
Ivan Pavlovich Bazarov (1916–2005) 相似文献39.
ZHUANG MuDe LIU Zheng REN Bin & TIAN ZhongQun State Key Laboratory of Physical Chemistry of Solid Surfaces 《中国科学:化学》2010,(2)
Tip-enhanced Raman spectroscopy (TERS) has been used to obtain the Raman signal of surface species on silicon single crystal surfaces without the necessity for surface enhancement by addition of Ag nanoparticles. By illuminating the hydrogen terminated silicon surface covered with a droplet of 4-vinylpyridine with UV light, a 4-ethylpyridine modified silicon surface can be easily obtained. By bringing a scanning tunneling microscope (STM) Au tip with a nanoscale tip apex to a distance of ca. 1 nm from the m... 相似文献
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XIAO TieJun & HOU ZhongHuai Hefei National Laboratory for Physical Sciences at the Microscale 《中国科学:化学》2010,(2)
Fluctuation theorem for entropy production in a mesoscopic chemical reaction network is discussed. When the system size is sufficiently large, it is found that, by defining a kind of coarse-grained dissipation function, the entropy production in a reversible reaction channel can be approximately described by a type of detailed fluctuation theorem. Such a fluctuation relation has been successfully tested by direct simulations in a linear reaction model consisting of two reversible channels and in an oscillat... 相似文献