高压煤粉密相气力输送实验研究

在输送压力可达4 MPa的气力输送实验台上,进行不同平均粒径煤粉的密相输送实验。研究总输送差压、发送压力对煤粉的质量流量、固气比等输送参数的影响。结果表明;煤粉质量流量随总输送差压的增加而增加;相同总输送差压下,煤粉平均粒径越大,煤粉质量流量越低;煤粉质量流量随发送压力的增加而增加。研究表明,相同煤粉质量流量下固气比随着表观气速的增加而降低;相同表观气速下,煤粉质量流量的增加会导致固气比的增加。     

Mn助剂对K-Co-Mo催化剂结构及CO加氢合成低碳醇性能的影响

通过溶胶-凝胶法合成了一系列Mn掺杂K-Co-Mo催化剂,并利用X射线衍射、N₂吸脱附、NH₃程序升温脱附、原位漫反射红外光谱以及X射线吸收谱等技术对催化剂的结构进行了表征.活性测试结果显示Mn掺杂催化剂比未掺杂催化剂表现更高的合成低碳醇的催化活性,尤其是C₂₊醇的选择性得到了明显的提高.醇产物分布偏离了ASF分布规律,甲醇的含量显著减少,乙醇成为主要醇产物.表征结果表明Mn助剂的加入增强了Co和Mo之间的相互作用,促进了醇生成活性中心Co-Mo-O物种的生成.显著减少了催化剂强酸性位的数量,促进了弱酸性位的产生,有利于醇产物的生成.助剂的加入有利于催化剂对CO的线性和桥式吸附,促进了醇产物的生成和碳链的增长,提高了催化剂对C₂₊醇的选择性.     

Heat treatment effects on microstructure and magnetic properties of Mn-Zn ferrite powders

Mn-Zn ferrite powders (Mn_0.5Zn_0.5Fe₂O₄) were prepared by the nitrate-citrate auto-combustion method and subsequently annealed in air or argon. The effects of heat treatment temperature on crystalline phases formation, microstructure and magnetic properties of Mn-Zn ferrite were investigated by X-ray diffraction, thermogravimetric and differential thermal analysis, scanning electron microscopy and vibrating sample magnetometer. Ferrites decomposed to Fe₂O₃ and Mn₂O₃ after annealing above 550 °C in air, and had poor magnetic properties. However, Fe₂O₃ and Mn₂O₃ were dissolved after ferrites annealing above 1100 °C. Moreover, the 1200 °C annealed sample showed pure ferrite phase, larger saturation magnetization (M_s=48.15 emu g⁻¹) and lower coercivity (H_c=51 Oe) compared with the auto-combusted ferrite powder (M_s=44.32 emu g⁻¹, H_c=70 Oe). The 600 °C air annealed sample had the largest saturation magnetization (M_s=56.37 emu g⁻¹) and the lowest coercivity (H_c=32 Oe) due to the presence of pure ferrite spinel phase, its microstructure and crystalline size.     

High-spin yrast and yrare structures in 112In

Up to now, no experimental cross-section data exist for the ⁶⁷Zn (n,a \alpha) ⁶⁴Ni reaction in the MeV neutron energy region. In the present work, the cross-section of the ⁶⁷Zn (n,a \alpha) ⁶⁴Ni reaction was measured at E _n = 6.0 MeV. Experiments were performed at the Van de Graaff accelerator of Peking University, China. Fast neutrons were produced through the D (d, n) ³He reaction using a deuterium gas target. Absolute neutron flux was determined by a small ²³⁸U fission chamber and a BF₃ long counter was used as a neutron flux monitor. A twin gridded ionization chamber was employed as the a \alpha -particle detector and two back-to-back ⁶⁷Zn samples were used for a \alpha events measurement. Background was measured and subtracted from foreground. The measured cross-section of the ⁶⁷Zn (n,a \alpha) ⁶⁴Ni reaction was 7.3 (1±15%) mb at 6.0MeV. The present result was compared with existing evaluations and TALYS code calculations.     

Characterization and properties of ZnO1−xSx alloy films fabricated by radio-frequency magnetron sputtering

A series of ZnO_1−xS_x alloy films (0 ≤ x ≤ 1) were grown on quartz substrates by radio-frequency (rf) magnetron sputtering of ZnS ceramic target, using oxygen and argon as working gas. X-ray diffraction measurement shows that the ZnO_1−xS_x films have wurtzite structure with (0 0 2) preferential orientation in O-rich side (0 ≤ x ≤ 0.23) and zinc blende structure with (1 1 1) preferential orientation in S-rich side (0.77 ≤ x ≤ 1). However, when the S content is in the range of 0.23 < x < 0.77, the ZnO_1−xS_x film consists of two phases of wurtzite and zinc blende or amorphous ZnO_1−xS_x phase. The band gap energy of the films shows non-linear dependence on the S content, with an optical bowing parameter of about 2.9 eV. The photoluminescence (PL) measurement reveals that the PL spectrum of the wurtzite ZnO_1−xS_x is dominated by visible band and its PL intensity and intensity ratio of UV to visible band decrease greatly compared with undoped ZnO. All as-grown ZnO_1−xS_x films behave insulating, but show n-type conductivity for w-ZnO_1−xS_x and maintain insulating properties for β-ZnO_1−xS_x after annealed. Mechanisms of effects of S on optical and electrical properties of the ZnO_1−xS_x alloy are discussed in the present work.     

光泵铯蒸气激光的动力学模型

建立了一个物理模型描述了光泵铯蒸气激光的动力学过程和激光机理.结合实验参量,经数值求解该模型,定量分析了抽运光参量、缓冲气压和输出镜反射率等对激光输出功率和光光效率产生的影响,得到了与实验基本一致的模拟结果.表明该模型较好地反映了光泵銫蒸气激光的动力学机理和发射过程,为该类激光的优化设计提供了借鉴和参考.     

6.1 MW, 10 kHz Side-Pumped Burst-Mode Nd:YAG Laser

We present a compact high-peak-power, high-repetition-rate burst-mode laser from a master-oscillator power amplifier (MOPA) at 1064 nm for laser-based measurement applications. The oscillator is an 808 nm pulsed laser diode side-pumped acousto-optical (A-O) Q-switched Nd:YAG laser at repetition rates ranging from 10–100 kHz, producing a pulse train with a pulse number of 2–25. The maximum output energy of the oscillator is 15.6 mJ at 10 kHz, whereas it is 1.7 mJ at 100 kHz. After twostage amplifiers, a single-pulse energy of 85.2 mJ with a pulse-width of 14.5 ns is achieved at 10 kHz, which produces a peak power of 6.1 MW. At 100 kHz, the total burst energy reaches 220 mJ with a single-pulse energy of 8.8 mJ in the pulse burst laser system.     

多倍脉宽输出的螺旋重入脉冲形成线

提出了一种螺旋线重入结构的脉冲形成线,可实现多倍脉宽输出。该结构由储能外线和重入内线组成;重入内线的外屏蔽圆筒内表面呈阶梯状,内筒为均匀螺旋线结构,实现简单;储能外线与Tesla变压器一体化。结合采用螺旋重入和二级重入结构,给出了一组10 GW功率、百ns脉宽的重入型脉冲形成线设计,形成线采用Midel 7131合成酯绝缘介质,外筒内径1 m,长度2 m。     

高精度组合脉冲激光时序控制系统设计

在激光等离子体机理的研究中,为实现灵活的界面配置和多路脉冲激光器高精度的时序延时,设计了一种基于微控制器STM32和FPGA的多路时序延时控制系统。重点介绍了基于FPGA的多路ns级时序信号和基于ucGUI的触摸屏界面的设计。另外,采用高速光电隔离技术和高速FET开关电路技术,对驱动电路进行了设计,缩短了输出脉冲上升沿的时间,提高了系统延时精度、驱动能力和抗干扰性能。测试结果表明,该设计每路延时可调,调节范围为5 ns~10 ms,最小可调步进为5 ns,延时误差小于1 ns。