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941.
Tiantian Si Lei Liu Xiaojing Liang Huixiao Duo Licheng Wang Shuai Wang 《Journal of separation science》2019,42(12):2148-2154
A zirconium(IV)‐based metal–organic framework material (MOF‐808) has been synthesized in a simple way and used for the extraction of phenoxyacetic acids in complex samples. The material has good thermal and chemical stability, large specific surface area (905.36 m²/g), and high pore size (22.18 Å). Besides, it contains a large amount of Zr‐O groups, easy‐to‐form Zr‐O‐H bond with carboxyl groups of phenoxyacetic acids, and possesses biphenyl skeleton structure, easy to interact with compounds through π‐π and hydrophobic interactions. These characteristics make the material very suitable for the extraction of certain compounds with a high extraction efficiency and excellent selectivity. The extraction conditions were optimized, and then an analytical method was successfully established and applied for analysis of actual samples. The solid‐phase extraction method based on prepared material had a wide linear range of 0.2–250 μg/L and a low detection limit of 0.1–0.5 μg/L for four phenoxyacetic acid compounds including 2,4‐dichlorophenoxyacetic acid, 2‐(2,4‐dichlorophenoxy) propionic acid, 4‐chlorophenoxyacetic acid, and dicamba. The relative standard deviations of intra‐ and interday precision were 1.8–3.8 and 4.3–6.9%, and the recoveries after spiking were between 77.1 and 109.3%. The results showed that the material is a desired substituent for the extraction of compounds with benzene ring structure containing carboxyl groups. 相似文献
942.
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944.
HE Min-Hua ZHANG Duan-Ming PAN Gui-Jun YIN Yah-Ping CHEN Zhi-Yuan 《理论物理通讯》2008,50(12):1351-1354
Through using the methods of finite-size effect and short time dynamic scaling, we study the critical behavior of parasitic disease spreading process in a diffusive population mediated by a static vector environment. Through comprehensive analysis of parasitic disease spreading we find that this model presents a dynamical phase transition from disease-free state to endemic state with a finite population density. We determine the critical population density, above which the system reaches an epidemic spreading stationary state. We also perform a scaling analysis to determine the order parameter and critical relaxation exponents. The results show that the model does not belong to the usual directed percolation universality class and is compatible with the class of directed percolation with diffusive and conserved fields. 相似文献
945.
The optically stimulated luminescent (OSL) radiation dosimeter technically surveys a wide dynamic measurement range and a high sensitivity. Optical fiber dosimeters provide capability for remote monitoring of the radiation in the locations which are difficult-to-access and hazardous. In addition, optical fiber dosimeters are immune to electrical and radio-frequency interference. In this paper, a novel remote optical fiber radiation dosimeter is described. The optical fiber dosimeter takes advantage of the charge trapping materials CaS:Ce, Sm that exhibit OSL. The measuring range of the dosimeter is from 0.1 to 100 Gy. 相似文献
946.
2004—2007年BEPC高频系统从常温腔改建到超导腔, 逐渐解决了改频的物理问题和超导技术的工程难题, 实现了与国际先进技术接轨, 并按期保质完成了工程、调束任务. 高频系统是BEPCⅡ工程首个吸收国外超导技术、自主完成集成和调试成功的大型装置; 2006年7月国内首次超导高频大功率试验成功; 2006年11月完成系统联调, 按期投入BEPCⅡ首轮调束; 同年12月首次投入同步辐射运行; 2007年2至5月, 东、西两套超导高频系统在1MV以上的加速电压均已实现正/负电子1.89GeV注入积累和110/114mA对撞; 在同步辐射运行中, 逐渐达到2.5GeV/250mA、束流功率100kW, 接近国外同类机器水平; 束流试验证明两套高频系统的 相似文献
947.
Establishment of Configuration with Optimized Current Profile in Pellet Fuelled Discharge on HL-2A
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A sawtooth-free period is produced following the pellet injection in the pellet fuelled discharge of qa = 3.4 (where qa is the safety factor at the plasma boundary) in the HL-2A tokamak. Establishment of the current profile such as in the hybrid scenario is studied under the condition of pellet injection in HL-2A. It is shown that a q-profile of weak negative shear is produced immediately after the pellet injection, and it then evolves to a broad flat profile with q0 〉 1 (where qo is the safety factor at the centre). The measured MHD mode structures evidence consistencies of the evaluated q-profile with locations of the q = 1 surface in the sawtoothing period and of the q = 2 surface in the sawtooth-free period. TRANSP analysis indicates that the energy confinement is enhanced substantially during and after pellet injection, which is resulted from the q-profile optimization and the plasma density peaking. 相似文献
948.
Electronic Curves Crossing in Methyl Iodide by Spin--Orbit Ab Initio Calculation 总被引:1,自引:0,他引:1
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An ab initio investigation of electronic curve crossing in a methyl iodide molecule is carried out using spin-orbit multiconfigurational quasidegenerate perturbation theory. The one-dimensional rigid potential curves and optimized effective curves of low-lying states, including spin-orbit coupling and relativistic effects, are calculated. The spin-orbit electronic curve crossing between ^3Qo+ and ^1Q1, and the shadow minimum in potential energy curve of ^3Qo+ at large internuclear distance are found in both sets of the curves according to the present calcu- lations. The crossing position is in the range of Re-1 = 0.2370 3:0.0001 nm. Comparisons with other reports are presented. 相似文献
949.
Experimental Characterization of Sub-picosecond Electron Bunch Length with Coherent Diffraction Radiation 总被引:1,自引:0,他引:1
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XIANG Dao YANG Xing-Fan HUANG Wen-Hui TANG Chuan-Xiang LIN Yu-Zheng LI Wei-Hua PAN Qing LI Ming 《中国物理快报》2008,25(7):2440-2443
Diffraction radiation is one of the most promising candidates for electron beam diagnostics for the International Linear Collider, x-ray free electron lasers and energy recovery linac due to its non-intercepting characteristics. We report the non-intercepting measurement of sub-ps electron bunch length with coherent diffraction radiation. The bunch length is measured with a Martin--Puplett interferometer and the detailed longitudinal bunch shape is reconstructed with the Kramers--Kronig relation. The rms bunch length is found to be about 0.73ps, which confirms a successful commissioning of the bunch compressor and the interferometer. 相似文献
950.
Growth Mechanism and Optimized Parameters to Synthesize Nafion-115 Nanowire Arrays with Anodic Aluminium Oxide Membranes as Templates
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Nation-115 nanowire arrays are synthesized with an extrusion method using AAO membranes as templates. It is indicated that the vacuum treating of AAO templates before surface decoration plays an important role in obtaining high filling rate of the Nation-115 nanowires in the AAO templates, vchile the concentration of Nafion-115 DMSO solutions does not affect the flling rate greatly. The optimized parameters to synthesize the Nation-115 nanowire arrays are studied. The filling rate of the Nadion-115 nanowires in the AAO templates synthesized with the optimized parameters is about 95% discussed to qualitatively explain the experimental results The growth mechanism of Nafion-115 nanowires is 相似文献