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21.
Dingzhong Li Wensheng Zhang Dr. Longzhi Zhu Prof. Dr. Shuang-Feng Yin Prof. Dr. Nobuaki Kambe Prof. Dr. Renhua Qiu 《ChemistryOpen》2022,11(5):e202200023
An efficient hydrazine substitution of p-nitro-aryl fluorides with hydrazine hydrates catalyzed by FeO(OH)@C nanoparticles is described. This hydrazine substitutions of p-nitro-aryl fluorides bearing electron-withdrawing groups proceeded efficiently with high yield and selectivity. Similarly, hydrogenations of p-nitro-aryl fluorides containing electron-donating groups also smoothly proceeded under mild conditions. Furthermore, with these prepared aryl hydrazines, some phthalazinones, interesting as potential structures for pharmaceuticals, have successfully been synthesized in high yields. 相似文献
22.
Alternating polymers, poly[(disilanylene)ethynylene]s and poly[(1, 2-diethynylenedisilanylene)(1-silacyclopenta-2, 4-diene-3, 4-diyl)]s were prepared by the anionic ring-opening polymerization of 1, 2, 5, 6-tetrasilacycloocta-3, 7-diynes and 4, 5, 10-trisilacyclo[6.3.0]undeca-1(11), 8-diene-2, 6-diynes, respectively. Poly[(disilanylene)butenyne-1, 4-diyl]s were synthesized by the reaction of 1, 2-diethynyldisilanes with a catalytic amount of RhCl(PPh3)3. Photochemical and conducting properties of the polymers are described. 相似文献
23.
Yuzuru Uchida Katsumi Onoue Nobuaki Tada Fumio Nagao Hideaki Kozawa Shigeru Oae 《Heteroatom Chemistry》1990,1(4):295-306
Phosphine oxides bearing two or three 2-pyridyl groups react with organometallic reagents affording 2,2′-bipyridyl, 2-substituted pyridines and pyridine in good yields. Phosphonium salts and phosphine oxides, bearing at least two 2-pyridyl or substituted 2-pyridyl groups also give the corresponding 2,2′-bipyridyls and pyridines upon treatment with acid or neutral solvents such as water and alcohols in substantial yields. The 2,2′-bipyridyls are considered to be formed by ligand coupling within the pentacoordinated phosphorus intermediate formed incipiently during the reaction. 相似文献
24.
Tian XC Ban Y Abe K Abe K Aihara H Arinstein K Asano Y Aulchenko V Aushev T Bakich AM Banerjee S Barberio E Barbero M Bay A Bedny I Bitenc U Bizjak I Blyth S Bondar A Bozek A Bracko M Brodzicka J Browder TE Chang P Chao Y Chen A Chen KF Chen WT Cheon BG Chistov R Choi SK Choi Y Choi YK Chuvikov A Dalseno J Danilov M Dash M Dong LY Drutskoy A Eidelman S Enari Y Fang F Fratina S Gabyshev N Gershon T Gokhroo G Golob B Gorisek A Haba J Hara T Hayasaka K Hayashii H Hazumi M Hokuue T Hoshi Y Hou S 《Physical review letters》2005,95(23):231801
Using 281 fb-1 of data from the Belle experiment recorded at or near the (4S) resonance, we have measured the rates of the "wrong-sign" decays D0 --> K+ pi- pi0 and D0 --> K+ pi- pi+ pi- relative to those of the Cabibbo-favored decays D0 --> K- pi+ pi0 and D0 --> K- pi+ pi+ pi-. These wrong-sign decays proceed via a doubly Cabibbo-suppressed amplitude or via D0-D0 mixing; the latter has not yet been observed. We obtain R(WS)(K pi pi0) = [0.229 +/- 0.015(stat)(+0.013)(-0.009)(syst)]% and R(WS)(K3pi) = [0.320 +/- 0.018(stat)(+0.018)(0.013)(syst)]%. The CP asymmetries are measured to be -0.006 +/- 0.053 and -0.018 +/- 0.044 for the K+ pi- pi0 and K+ pi- pi+ pi- final states, respectively. 相似文献
25.
Chao Y Chang P Abe K Abe K Aihara H Akai K Akatsu M Akemoto M Asano Y Aushev T Bahinipati S Bakich AM Bay A Bedny I Bitenc U Bizjak I Bondar A Bozek A Bracko M Brodzicka J Browder TE Chen A Chen KF Chen WT Cheon BG Chistov R Choi SK Choi Y Chuvikov A Dalseno J Danilov M Dash M Dragic J Drutskoy A Eidelman S Eiges V Enari Y Fang F Flanagan J Fratina S Furukawa K Gabyshev N Garmash A Gershon T Gokhroo G Golob B Haba J Hastings NC Hayasaka K Hayashii H Hazumi M Hinz L Hokuue T Hoshi Y Hou S Hou WS 《Physical review letters》2005,94(18):181803
We report the observation of the decay B0-->pi(0)pi(0), using a 253 fb(-1) data sample collected at the Upsilon(4S) resonance with the Belle detector at the KEKB e(+)e(-) collider. The measured branching fraction is B(B0-->pi(0)pi(0))=(2.3(+0.4+0.2)(-0.5-0.3))x10(-6), with a significance of 5.8 standard deviations including systematic uncertainties. We also make a measurement of the direct CP violating asymmetry in this mode. 相似文献
26.
K. Ishikawa H. Nakano H. Masuda C. Kusano Y. Takahashi T. Hamagishi N. Endo 《Fiber and Integrated Optics》1992,11(4):385-394
A 10-Gbit/s optical receiver is developed using low-capacitance HBT IC technology. The HBT allows a cutoff frequency of 45 GHz and a maximum oscillation frequency of 70 GHz. The receiver contains an automatic gain-control amplifier IC with a gain of 16 dB, a bandwidth of 10.7 GHz, and a decision-circuit IC with an ambiguity of 66 mVp-p at a data rate of 10 Gbit/s. The sensitivity of this receiver is -26.5 dBm at a bit error rate of 10-9. Transmission over a 140-km fiber was achieved successfully. 相似文献
27.
E. V. Sampathkumaran K. Hirota I. Das M. Ishikawa 《Zeitschrift für Physik B Condensed Matter》1993,90(2):195-196
Experimental observations for possible presence of 4f quadrupolar Kondo effect in PrCu2Si2 are critically discussed. A comparison of the low temperature properties of the alloys, Pr
x
Y1–x
Cu2Si2 (x=0.05, 0.2 and 0.4), seems to signal the existence of 4f electric quadrupolar glass phenomenon around 4K forx=0.2. 相似文献
28.
N. Nishida R.S. Hayano K. Nagamine T. Yamazaki J.H. Brewer D.M. Garner D.G. Fleming T. Takeuchi Y. Ishikawa 《Solid State Communications》1977,22(4):235-239
In recent positive-muon spin rotation experiment at TRIUMF on single crystal Fe, a clear temperature dependent change has been observed, for the first time, both in frequency and depolarization rates from 300 K down to 23 K. The μ+ depolarization was explained by the μ+ diffusion through inhomogeneous dipolar fields and the diffusion constant was found to obey an Arrhenius law (activation energy 17 meV) above 70 K but surprisingly deviated from this at lower temperatures, indicating quantum diffusion. We have also found that the μ+ hyperfine field has a temperature dependence slightly stronger than that of the magnetization. 相似文献
29.
Neutron scattering measurements have been made of phonons in a Fe65Ni35 crystal at several temperatures. Marked softening of the [110] acoustic shear modes and a dip in the dispersion relation are found at low temperatures. Above the magnetic ordering temperature Tc, the frequency shift is removed completely, which suggests phonon perturbation by magnetoelastic coupling. 相似文献
30.