On the role of mechanical effects during dynamic fatigue of PbTiO3 single crystals

The details of the mechanical effects (twinning and microcracking) are clarified at various stages of dynamic fatigue of PbTiO₃ crystals using a polarization microscope and selective etching.     

Possibility of observing chiral-symmetry effects in ferromagnetic nanoparticles

The statistics of left-and right-handed vortical magnetization states in a system of submicron-sized ferromagnetic disks is studied experimentally. Lattices of elliptic cobalt particles with a planar size of 750 × 450 nm and a thickness of 25 nm were formed using high-resolution electronic lithography. To visualize the magnetization distributions in the disks, magnetic force microscopy was used. The experimental results indicate the conservation of magnetic chiral symmetry in cobalt ferromagnetic particles of the above size and shape.     

Electrochemical procedure for express evaluation of the corrosion effect of aqueous glycol solutions on metals

Electrochemical procedure for express evaluation of the corrosion effect of aqueous glycol solutions on the metallic construction materials for cooling systems was studied. This procedure was used to develop new coolant formulations.     

Preparation of ultrapure calcium formate

Crystallization of Ca(HCOO)₂ from aqueous solutions was studied and conditions under which an ultrapure product can be obtained were determined.     

One-pot diastereoselective synthesis of α-aminonitriles from aldehydes, chiral amines, and trimethylsilyl cyanide under solvent-free conditions

Treatment of aliphatic and aromatic aldehydes with chiral amines and trimethylsilyl cyanide in the absence or in the presence of Lewis acids (including lithium perchlorate) under solvent-free conditions afforded the corresponding α-aminonitriles in good yields and with a diastereoselectivity of 68 to 86%. Published in Russian in Zhurnal Organicheskoi Khimii, 2006, Vol. 42, No. 1, pp. 56–59. The text was submitted by the authors in English.     

The role of readily hydrolyzable polysaccharides of larch wood in manufacture of board materials

Role of readily hydrolyzable polysaccharides of larch wood in production of board materials is studied.     

Properties of Josephson junctions in the inhomogeneous magnetic field of a system of ferromagnetic particles

The effect of an array of ferromagnetic nanoparticles on the field-dependent critical current of the short overlap Josephson junction is experimentally studied. Large reversible variations of the maximum critical current are observed depending on the magnetic state of the particles. The pronounced commensurability effects are detected which are proved by the additional peaks of magnetic field induced diffraction pattern.     

Applications of fast atom bombardment mass spectrometry (FAB MS) to organometallic and coordination chemistry

This article describes the technique of fast atom bombardment mass spectrometry (FAB MS) and its applications to the analysis of organometallic and coordination complexes. Sections on ion generation and matrices are followed by a Periodic Group-based review of FAB MS results obtained from Transition Metal and Main Group compounds, organometallic cluster carbonyls and their derivatives, and salts of poly-oxo-anions. The literature has been surveyed from 1981 to approximately mid-1986.