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81.
82.
Hong Ming ZHANG Xian Hong WANG Xiao Jiang ZHAO Ji LI Fo Song WANG 《中国化学快报》2006,17(4):437-440
A novel method for the preparation of oligothiophene molecular wires is described via a bi-directional solid-phase synthesis. Using an alternating sequence of bromination and Stille coupling reactions, oligomers were obtained up to the heptamer in excellent yield and purity. 相似文献
83.
A Hybrid Multiobjective Evolutionary Algorithm for Solving Vehicle Routing Problem with Time Windows 总被引:2,自引:0,他引:2
Vehicle routing problem with time windows (VRPTW) involves the routing of a set of vehicles with limited capacity from a central
depot to a set of geographically dispersed customers with known demands and predefined time windows. The problem is solved
by optimizing routes for the vehicles so as to meet all given constraints as well as to minimize the objectives of traveling
distance and number of vehicles. This paper proposes a hybrid multiobjective evolutionary algorithm (HMOEA) that incorporates
various heuristics for local exploitation in the evolutionary search and the concept of Pareto's optimality for solving multiobjective
optimization in VRPTW. The proposed HMOEA is featured with specialized genetic operators and variable-length chromosome representation
to accommodate the sequence-oriented optimization in VRPTW. Unlike existing VRPTW approaches that often aggregate multiple
criteria and constraints into a compromise function, the proposed HMOEA optimizes all routing constraints and objectives simultaneously,
which improves the routing solutions in many aspects, such as lower routing cost, wider scattering area and better convergence
trace. The HMOEA is applied to solve the benchmark Solomon's 56 VRPTW 100-customer instances, which yields 20 routing solutions
better than or competitive as compared to the best solutions published in literature. 相似文献
84.
强混合样本下回归加权估计的一致渐近正态性 总被引:5,自引:0,他引:5
在强混合样本下,讨论固定设计回归模型的加权函数估计的一致渐近正态性,给出一致渐近正态性的收敛速度,这个速度接近n-1/6. 相似文献
85.
We report viscometric data collected in a Couette rheometry on dilute, single‐solvent polystyrene (PS)/dioctyl phthalate (DOP) solutions over a variety of polymer molecular weights (5.5 × 105 ≤ Mw ≤ 3.0 × 106 Da) and system temperatures (288 K ≤ T ≤ 318 K). In view of the essential viscometric features, the current data may be classified into three categories: The first concerns all the investigated solutions at low shear rates, where the solution properties are found to agree excellently with the Zimm model predictions. The second includes all sample solutions, except for high‐molecular‐weight PS samples (Mw ≥ 2.0 × 106 Da), where excellent time–temperature superposition is observed for the steady‐state polymer viscosity at constant polymer molecular weights. No similar superposition applies at a constant temperature but varied polymer molecular weights, however. The third appears to be characteristic of dilute high‐molecular‐weight polymer solutions, for which the effects of temperature on the viscosity curve are further complicated at high shear rates. The implications concerning the relative importance of hydrodynamic interactions, segmental interactions, and chain extensibility with increasing polymer molecular weight, system temperature, and shear rate are discussed. © 2006 Wiley Periodicals, Inc. J Polym Sci Part B: Polym Phys 44: 787–794, 2006 相似文献
86.
Using kinetic Monte Carlo method, we have simulated a pulsed energetic growth process in pulsed laser deposition. During the growth of film, substrate temperature mainly influences upon film morphology by directly enhancing the adatom mobility through the temperature-dependent thermal vibration. By contrast, the effect of incidence kinetic energy on film growth is complex resulting from the collisions between the incident particles and the adatoms. The results show that improving incident kinetic energy cannot significantly accelerate the migration rate of adatom but change surface microstructure and promote single adatom formation resulting in more island aggregation density. Moreover, since pulse-influx characterizes pulsed laser deposition, the intensity per pulse contributes to the evolvement of nucleation density and the results illustrate that a general scaling law different from ordinary power law still exists in energetic growth of pulsed laser deposition. 相似文献
87.
采用多靶磁控溅射法制备了一系列具有不同Al2O3调制层厚度的TiN/Al2O3纳米多层膜.利用X射线能量色散谱、X射线衍射、扫描电子显微镜、高分辨透射电子显微镜和微力学探针表征了多层膜的成分、微结构和力学性能.研究结果表明,在TiN/Al2O3纳米多层膜中,单层膜时以非晶态存在的Al2O3层在厚度小于1.5 nm时因TiN晶体层的模板效应而晶化,并与TiN层形成共格外延生长,相应地,多层膜产生硬度明显升高的超硬效应,最高硬度可达37.9 GPa.进一步增加多层膜中Al2O3调制层的层厚度,Al2O3层逐渐形成非晶结构并破坏了多层膜的共格外延生长,使得多层膜的硬度逐步降低. 相似文献
88.
关于方程(1)的极限环唯多性问题,不少人作了研究,[1]引进“n重互相包含”曲线类,,经[2]的改进获得较好的结果,但这类曲线要求的条件较多。本文不从[1]的观点出发,不包含[1]的全部条件,独立地用①11。’,LtnnoB变换折叠相平面,据轨线与折叠线交点的位置,对(1)的等价方程按线性方程积分,将积分的正负项作成比值进行比较,得出一组充分条件。 相似文献
89.
90.
Vee Ming Ng 《Journal of multivariate analysis》2002,83(2):409
Bayesian inference is considered for the seemingly unrelated regressions with an elliptically contoured error distribution. We show that the posterior distribution of the regression parameters and the predictive distribution of future observations under elliptical errors assumption are identical to those obtained under independently distributed normal errors when an improper prior is used. This gives inference robustness with respect to departures from the reference case of independent sampling from the normal distribution. 相似文献