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91.
Two methods for multi-element preconcentration from copper by reductive matrix precipitation are presented. In systematic investigations on the coprecipitation behaviour of Ag, Al, Au, Bi, Cd, Co, Cr, Fe, Ga, In, Mn, Mo, NJ, Pb, Sb, Se, Sn, Te and Zn during precipitation of the copper matrix as Cu2O or CuSCN, the separation parameters were optimized. By combination with a hexamethyleneammonium hexamethylenedithiocarbamate collector precipitation, a concentration of 8 elements (Cu2O precipitation) or 13 elements (CuSCN precipitation) in a small volume was achieved. The limits of detection of the procedures are, depending on the element, 0.1–5 μg g?1 for flame atomic absorption spectrometry (AAS) and 0.01–0.1 μg g?1 for graphite furnace AAS. The relative standard deviations are about 3%. The analytical performance of the procedures is compared with that of an electrolytic copper separation. 相似文献
92.
M. Heusler 《General Relativity and Gravitation》1991,23(2):189-207
The field equations for homogeneous models in an arbitrary number of dimensions form a Hamiltonian system with constraint forces. Due to the monotonic behavior of the determinant of the induced metric, the evolution of the system can be interpreted as the motion of a particle in an explicitly time-dependent potential. Considering vacuum models, we show that this explicit time-dependence can be eliminated. Using the scaling properties of the Ricci tensor we obtain an autonomous system, for which we can also find a Liapunov function in terms of the n-dimensional Ricci curvature. 相似文献
93.
The variational problem of contact equilibrium of a punch and an elastic body is considered. An equivalent formulation of the problem is given in variational inequality form. Existence and uniqueness of the solution is investigated in a particular case. A penalty method is proposed for approximate solution of the problem.Translated from Vychislitel'naya i Prikladnaya Matematika, No. 56, pp. 97–103, 1985. 相似文献
94.
E. V. Zakharov A. G. Davydov Yu. V. Pimenov G. M. Tikhonov 《Computational Mathematics and Modeling》1991,2(1):79-84
Translated from Chislennye Metody Resheniya Obratnykh Zadach Matematicheskoi Fiziki, pp. 119–127. 相似文献
95.
I. L. Davies K. E. Markides M. L. Lee M. W. Raynor K. D. Bartle 《Journal of separation science》1989,12(4):193-207
Although coupled liquid chromatographygas chromatography (LC-GC) was first demonstrated ten years ago, only in the last few years has there been a sudden surge of interest in the technique. Approximately 70% of the total number of LC-GC applications have been published in the last two years (1987–88) alone. This review categorizes LC-GC publications into four main application areas: fossil fuels, foods, environmental samples, biologiical/pharmaceutical samples, and miscellaneous samples. Multidimensional separations carried out using other coupled-column chromatographic techniques (such as supercritical fluid chromatography (SFC) with GC, and on-line trace enrichment-GC) have also been included in this review. 相似文献
96.
Translated from Zhurnal Prikladnoi Spektroskopii, Vol. 51, No. 2, pp. 212–217, August, 1989. 相似文献
97.
E. Dror Farjoun 《Israel Journal of Mathematics》1989,66(1-3):132-142
Using a new group of singular chains on polyhedra, a transfer map is defined on the chain level for fibrations with singularities.
These include usual transfer on homology as well as Oliver transfer and other cases. 相似文献
98.
99.
Palle E. T. Jorgensen 《Mathematische Zeitschrift》1989,201(4):455-476
Work supported in part by the NSF 相似文献
100.
A. M. Vinogradov 《Acta Appl Math》1989,15(1-2):3-21
The main notions and results which are necessary for finding higher symmetries and conservation laws for general systems of partial differential equations are given. These constitute the starting point for the subsequent papers of this volume. Some problems are also discussed. 相似文献